• Korean Journal of Heritage: History & Science
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• v.53 no.1
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• pp.34-51
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• 2020

In order to clarify the lime-based building method used in the Joseon Dynasty, lime materials, production techniques, and mixing methods recorded in ancient literature were examined. In ancient Joseon Dynasty literature, the use of low grade limestone as a raw material was recorded, and the use of pozzolanic materials such as Hwangtoh, white clay, and roof tile powder as mixing aids to enhance the strength of lime was recorded. In addition, various lime hydration and mixing methods were recorded, and based on re-experiments carried out with regards to this, a physical property evaluation was deemed to be required in accordance with the various types of raw lime materials, lime hydration methods, and mixture ratios. In the early Joseon Dynasty, lime was used for various aspects, but frequent problems were experienced due to lack of supply and poor production techniques. In the late Joseon Dynasty, lime production techniques developed along with mass production. Based on analysis of the manufacturing techniques of Hoegwagmyo lime mortar in the 16^th and 18^th centuries during the Joseon Dynasty, it was found that mixing ratios and the methods described in the ancient literature had been applied. It was confirmed that the mixing ratio differed depending on mixing materials and lime quality. Since the mixing ratio of Hoegwagmyo lime mortar changed over time and it was produced strictly on the basis of a guidebook, it is believed that if continuous scientific analysis of the Hoegwagmyo lime mortar production method were carried out, this would be helpful for ascertaining the chronological methodology of Hoegwagmyo.

• 한국문화재보존과학회:학술대회논문집
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• 2003.09a
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• pp.42-47
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• 2003

• Journal of Conservation Science
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• v.28 no.1
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• pp.63-73
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• 2012

In this study, the 89 components of the gases emitted from grave goods at Sim Seol(1570-1630) tomb identified and quantitatively analyzed using a thermal desorption system integrated with gas chromatography-mass spectrometer. The concentration of major components show the levels of alpha-pinene 4,113ppbv, beta-pinene 2,510ppbv and limonene 2,424ppbv, that of the others orderly show p-menth-2-ene, acetone, isolongifolene and isoborneol. The functional groups of high concentration level cover 65% of terpenes and 25.8% of alcohols. The expected odor intensity orderly show 35.1% of terpenes, 33.4% of aldehydes and 8.8% of alcohols. Terpenes have generally effect of a perfume, antifungal and antimicrobial activity, and could come out of the pine(Pinus densiflora) coffin, aldehydes and alcohols could be come out of both the Sim Seol mirra and Pinus densiflora for a long time. The analyses of gases emitted from a excavated properties or a tomb are assessed that it can pc001 provide a scientific basis on a counterplan against harmful gases, a method of conservation treatments and a evaluation of effectiveness in conservation of cultural properties in a tomb.

• Korean Journal of Heritage: History & Science
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• v.41 no.1
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• pp.99-108
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• 2008

The paleogenetic analysis has become an increasingly important subject of archaeological, anthropological, biological as well as public interest. Recently, scientific research for human skeletal remains was more activated because of increasing awareness of the valuable archaeological information by the ancient DNA analysis. State of preservation of organic remains vary in different soil and burying environmental condition. Almost all available tissue disappear to analysis ancient DNA of bone in acidic soil caused by climate and geological features in Korea. Many preserved human remains excavated in the 'Heogwakmyo'(limelayered tomb of Chosun Dynasty Period) is able to explain through the relationship between burial conditions and bone survival form the burial method and ceremony. Ancient DNA analysis of excavated human bone form ancient tomb requires to remove contaminants such as microorganism's DNA and soil components that affect authentic results. Particularly, contamination control of contemporary human DNA is major serious problem and should verified by criteria of authenticity. In order to understand migration and culture of ancient population, when possible, ancient DNA studies needs to go abreast both radiocarbon and stable isotope studies because the dietary inferences will suggest ancient subsistence and settlement patterns. Also when the paleogenetic research supported with the arts and humanities research such as physical anthropology and archaeology, more valuable ancient genetic information is providing a unique results about evolutionary and population genetics studies to reconstruct the past.

• Journal of the Korean Wood Science and Technology
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• v.34 no.6
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• pp.12-20
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• 2006

The objectives of this study were to identify the species of coffin woods excavated at Ma-jeon relic in Jeonju and to date this coffin using tree-ring method. Al coffin woods were identified as red pines, most possibly, Pinus densiflora S. et Z. Tree-ring dating provides a calender year to each ring and produces the cutting date, if the bark presents. Due to the presence of bark and complete latewood present, the cutting date of the tree for coffin turned out between A.D. 1637 autumn and 1638 spring. However, due to the seasoning and storage periods, actual coffin manufacturing and burial time may be a little different from the tree-ring date.

• Journal of the Korean Wood Science and Technology
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• v.49 no.1
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• pp.67-81
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• 2021

This study aimed to conduct tree-ring dating and analysis of the materials used for the wooden coffins excavated from the ruins of Sipjeong-dong, Incheon. The tree species for the 10 wooden coffin materials was identified as pine. For accurate tree-ring measurement, the cross section was polished using sandpaper. The annual ring width was measured with an accuracy of 0.01 mm. Since the five materials were consistent with each other in dendrochronology, a representative annual ring chronology of 83 years was prepared. The prepared representative annual ring chronology was compared with the standard annual ring chronology, and the outermost ring of the wooden coffin was confirmed to correspond to the year 1575, suggesting that the wooden coffin was produced in the late 16th century. In addition, microscopic observation and FT-IR analysis revealed that the fibers attached to the surface of the wooden coffin were fibroin (Silk), and infrared spectroscopy (FT-IR) and Py-GC/MS analysis showed that the paint left on the surface of the wooden coffin was lacquer.

• Conservation Science in Museum
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• v.13
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• pp.37-44
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• 2012

White crystals on 46 costumes excavated from Shim Su-Ryun(1534 - 1589)'s tomb were examined their characterization and distribution. In 36 of such samples, white crystals with different shape and hardness were found. The formation of crystals did not correlated with a kind and use of textiles. However, crystals were found in the back side than the front of costume, specially around the marks of shrouding dead body. White crystals from 7 textiles were investigated by EPMA, XRD, or FT-IR. The composition of white crystal was analysed by EPMA and the structure characterization of crystals was used by X-ray diffraction. FT-IR spectroscopy was applied to check if non-crystalline compounds were also present. Mg and P were detected as the main element of white crystals and these compounds were identified a struvite and newberyite, the inorganic mineral magnesium ammonium phosphates. Struvite precipitation are influenced by many factors including concentration of Mg²⁺, NH₄⁺, and PO₄^3- ions, pH, and temperatures. It is assumed that magnesium, phosphorous, ammonia, a base material of struvite comes from decomposition product of human body. Tomb covered with lime, a unique triple-structure in Joseon period offering the basic condition, an anaerobe in a coffin, and high magnesium concentration of outer coffin with lime can be inferred as important factor for precipitation of crystals.

• Journal of Conservation Science
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• v.26 no.1
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• pp.95-107
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• 2010

Biochemical research was carried out on 4 human skeletal remains from historical lime-layered tombs assigned to the Joseon Dynasty in Oknam-ri, Seocheon. The preservation of femur was evaluated by stereoscopic microscopy and scanning electron microscopy. Most of specimens showed good histological preservation. The histological results proved to be a good potentiality for biochemical analysis using bio-molecules. The amelogenin gene and mitochondrial DNA (mtDNA) analyses revealed that three specimens perhaps have maternal consanguinity due to sharing with mtDNA haplogroup D4b1, and two specimens buried in the same tomb were a couple in Gatjaegol site. Carbon and nitrogen stable isotope analysis indicated that four deads diet were built around C3 plant as rice, barley, wheat and bean. In this study we characterized genetic and diet features from the social stratum who could make lime-layered tombs during period of the Joseon Dynasty. The results suggest that biochemical research using the human skeletal remains from the Joseon Dynasty has the great potential and reasonable value for archaeology, anthropology, and population genetics.

• Analytical Science and Technology
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• v.25 no.5
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• pp.300-306
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• 2012

This study reports the stable carbon and nitrogen isotope of mummy, the preserved human time capsule from Joseon Dynasty. The stable isotopic composition of biological tissue is expected to be a direct and constant function of diet because the stable isotope ratios do not decay or change in abundance through time. Over the past three decades, stable carbon and nitrogen isotope analysis has been extensively applied for archaeological topics. However, this is the first case in Korean mummy to extract palaeodietary information using stable isotope analysis. We extracted isotopic information from bone collagen and hair keratin, which reflects the lifetime average diet and short-term diet, respectively. The average values of ${\delta}^{13}C$ and ${\delta}^{15}N$ values are -19.0‰ and 11.4‰ (bone collagen), and -21.3‰ and 14.3‰ (hair keratin). Stable carbon isotope shows a mainly $C_3$-based diet from cradle to grave. On the other hand, there is significant difference in stable nitrogen isotope which implies a relatively enriched diet before death. We expect this study opens up a potential to understand the palaeodietary lifestyle in Joseon Dynasty.

• Economic and Environmental Geology
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• v.51 no.1
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• pp.49-65
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• 2018

The lime-soil mixture on tomb barrier (LSMB) is a type of tomb in Joseon Dynasty, which made with so-called 'Sammul' (three material compound) that mixture of lime, fine sand and yellow ocher. This study divided the tombs of the Gungri Site from Joseon Dynasty with layered wall and integrated wall according to the manufacturing types, and investigated on the basis of analysis to material characteristics and making techniques. Analytical samples were classified with lime-soil mixtures and soils, and interpreted the mixing characteristics of Sammul based on types of tomb barrier. The tomb barrier which is directly effect to control the inner environment was made with high content of lime. But the finishing or bottom layer were made with low content of lime. Overall the LSMB with integrated wall has higher content of lime and physical property than the LSMB with layered wall. The soil which was compounded as a Sammul and collected near the Gungri Site had similar with mineralogical and geochemical characteristics. Therefore, it is presumed that the fine sand and yellow ocher that made as a Sammul, were used with soil that was distributed around the site. Meanwhile, large scale limestone quarry is distributed near the site. Especially, Gungri Site has a possibility of material supply through water transport, due to the sea route from Asan bay is connected near the site. Thus, there is the possibility of transportation of lime materials from nearby quarry.