• Title/Summary/Keyword: 화학적 성분 분석

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Physical and Chemical Characterization of Soil in China (황사토양입자의 물리ㆍ화학적 특성)

  • 신선아;고준석;한진석;최덕일;여상진;박순웅;김신도
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.05b
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    • pp.179-180
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    • 2003
  • 황사가 발생하는 중국 지역의 토양 특성은 우리나라로 이동되어온 황사성분의 특성을 결정하는 중요한 요소중의 하나이다. 따라서, 황사토양입자의 특성과 지역적 차이에 대한 자료를 마련하기 위해 대표적인 황사 발생원으로 알려져 있는 중국 내륙의 황토지역과 북부 사막지역을 포함하는 총 37개의 토양 시료를 중국에서 채취하였으며, 채취한 각 토양시료의 분석을 통해 황사토양입자의 물리ㆍ화학적 특성을 파악하고자 하였다. (중략)

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Acidity and Chemical Composition of Precipitation Collected by Auto and Manual Sampling Method in Chonbuk Area (전북지역에서 시료채취방식에 따른 강수의 산성도 및 화학적 특성)

  • 강공언;오인교;전종남;유두철;유재웅;박경수
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.11a
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    • pp.372-373
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    • 2003
  • 오늘날 강수의 오염도는 대기오염의 중요한 지표가 되고 있으며, 특히 산성화된 강수는 생태계에 심각한 악영향을 주고 있어 전세계적으로 이에 대한 연구가 지속적으로 이루어지고 있다. 우리나라에서도 환경부 및 지방자치단체에서 산성비 측정망을 운영하면서 강수의 산성도 및 수용성 이온성분의 농도 측정을 수행하고 있으나 현재 강수자동채취장치와 수동채취장치를 같이 사용하고 있어 그 분석자료의 정도관리에 상당한 문제점이 있는 것으로 드러나고 있다. (중략)

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사상분진과 열연슬러지를 이용한 TCE, PCE의 제거

  • 이용재;박규홍;박준범;이재원
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 2003.04a
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    • pp.356-359
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    • 2003
  • 영화유기화합물의 제거에 있어서 일반적으로 이용되는 금속분말로는 아연, 주석, 니켈, 납, 철 등이 알려져 있으며, 경제성과 반응성이 좋고, 독성을 야기하지 않는다는 측면에서 영가 철이 가장 많이 연구·실용화되어 적용되고 있는 실정이다. 본 연구에서는 제철부산물들의 비표면적 측정, 화학적 구성성분 분석 및 pH의 변화를 통해 TCE, PCE 제거능력 평가 및 탈염소화반응을 확인하였으며, 제철부산물인 사상분진과 열연슬러지가 TCE 및 PCE의 제거효율적인 측면이나 산업폐기물의 재활용적인 측면에서 순수철보다 우수하다는 것을 확인하였다.

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A Study on change in thermal properties and chemical structure of Zr-Ni delay system by aging (노화에 따른 Zr-Ni계 지연관의 열 특성 및 화학적 구조 변화에 관한 연구)

  • Park, Byung Chan;Chang, Il Ho;Kim, Sun Tae;Hwang, Taek Sung;Lee, Seungho
    • Analytical Science and Technology
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    • v.22 no.4
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    • pp.285-292
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    • 2009
  • It has been observed that, after long term storage, some ammunitions are misfired by tamping (combustionstopping) due to aging of the chemicals loaded in the ammunitions. Used in ammunitions are percussion powder which provides the initial energy, igniter which ignites the percussion powder, and a delay system that delays the combustion for a period of time. The percussion powder is loaded first, followed by the igniter and then the delay system, and the ammunitions explode by the energy being transferred in the same order. Tamping occurs by combustion-stopping of the igniter or insufficient energy transfer from the igniter to the delay system or the combustion-stopping of the delay system, which are suspected to be caused by low purity of the components, inappropriate mixing ratio, size distribution of particulate components, type of the binder, blending method, hydrolysis by the humidity penetrated during the long term storage, and chemical changes of the components by high temperature. Goal of this study is to find the causes of the combustion-stopping of the igniter and the delay system of the ammunitions after long term storage. In this study, a method was developed for testing of the combustion-stopping, and the size distributions of the particulate components were analyzed with field-flow fractionation (FFF), and then the mechanism of chemical change during long term storage was investigated by thermal analysis (differential scanning calorimetry), XRD (X-ray diffractometry), and XPS (X-ray photoelectron spectroscopy). For the ignition system, M (metal)-O (oxygen) and M-OH peaks were observed at the oxygen's 1s position in the XPS spectrum. It was also found by XRD that $Fe_3O_4$ was produced. Thus it can be concluded that the combustion-stopping is caused by reduction in energy due to oxidation of the igniter.

Wine quality prediction analysis using machine learning (머신러닝을 이용한 와인 품질 예측분석)

  • Kim, Min-Seung;Jeong, Jae-hyeon;Kim, Jong-min
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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    • 2022.05a
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    • pp.690-693
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    • 2022
  • In this study, we used wine data to perform correlation analysis on factors that affect wine quality, and predicted wine quality standards based on the results. The dataset used in this study used data from 1599 red wines and 4898 white wines produced in Vinho verde, Portugal, for a total of 6497. The variable items are 12 kinds of component variables that represent wine components through physical and chemical analysis tests, a total of 1599 observations, and a total of one of the representative wines of the three major wine producing regions in the world (France, Italy, Spain). Added 3 pieces. Analysis was made by applying national climate change data.

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Mass Balance on the Pulping Extracts of Maple Hardwood using High Performance Liquid Chromatography (HPLC 분석기를 이용한 펄프용 단풍나무의 펄핑 추출액에 관한 물질수지)

  • Um, Byung-Hwan
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.4
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    • pp.102-108
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    • 2008
  • At the University of Maine, a hemicellulose pre-extraction technology is now being investigated to improve pulp yields, reduce the organic and inorganic load for liquor recovery, and create a feed stream for the generation of new biomaterials. It is important to understand the composition of unextracted wood, extracted wood, and pulping extracts in the design of an economically viable pilot-scale ethanol plant. For analysis of wood pulp composition, the total analytical mass balance closure was 100.6, 100.3, and 81.6% for unextracted chips, extracted chips, and pulping extracts from HPLC-H column analysis. Meanwhile, the total analytical mass balance from the HPLC-P column was 97.8, 86.3, and 80.7%, respectively. This slight variability between H- and P-column results for analytical mass balance may be within the experimental error of the measurement. The data generated by this analysis are important to further design work in commercializing this process.

Analysis and Conservation Treatment of Gilt-bronze Standing Buddha and Bronze Standing Buddha Statues Excavated from Yeongguksa Temple in Yeongdong (영동 영국사 출토 금동여래입상, 동제여래입상 분석 및 보존처리)

  • Yoo, Jayoung;Yang, Seulgi;Lee, Minhee
    • Conservation Science in Museum
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    • v.19
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    • pp.69-82
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    • 2018
  • The gilt-bronze standing Buddha and bronze standing Buddha statues excavated from Yeongguksa Temple in Yeongdong, currently held in the collection of the Cheongju National Museum, underwent conservation treatment after scientific study. Materials analysis showed that the gilt-bronze statue was made with a ternary alloy of copper, tin, and lead, while the bronze statue is of a binary alloy of copper and tin. The analysis also revealed that the bronze statue contains gold, and it is therefore recommended to change its description to gilt-bronze standing Buddha. The gilt-bronze statue appears to have been made with lead produced in Korea. The material observed on the surface that is presumed to have been used as an adhesive for the gold coloring is thought to be lacquer. For conservation treatment, the statues were minimally cleaned using physical and chemical methods and were treated through consolidation and protective coating.

Multivariate Statistical Analysis and Prediction for the Flash Points of Binary Systems Using Physical Properties of Pure Substances (순수 성분의 물성 자료를 이용한 2성분계 혼합물의 인화점에 대한 다변량 통계 분석 및 예측)

  • Lee, Bom-Sock;Kim, Sung-Young
    • Journal of the Korean Institute of Gas
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    • v.11 no.3
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    • pp.13-18
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    • 2007
  • The multivariate statistical analysis, using the multiple linear regression(MLR), have been applied to analyze and predict the flash points of binary systems. Prediction for the flash points of flammable substances is important for the examination of the fire and explosion hazards in the chemical process design. In this paper, the flash points are predicted by MLR based on the physical properties of pure substances and the experimental flash points data. The results of regression and prediction by MLR are compared with the values calculated by Raoult's law and Van Laar equation.

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Morphology and Thermal Properties of PPS/ABS Blends (PPS/ABS 블렌드의 형태학적/열적 특성)

  • 이영관;김준명;남재도;박찬석;장승필
    • Polymer(Korea)
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    • v.24 no.3
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    • pp.366-373
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    • 2000
  • In this study, the PPS/ABS blend system was investigated in order to collectively identify the relationship among blend morphology, chemical compatibilization and thermal property. ABS resin was chemically modified by the incorporation of maleic anhydride through reactive extrusion for enhanced compatibilization, and PPS, ABS and the modified ABS were blend by a sing twin screw extruder. The effect of chemical modification of ABS on the morphological, mechanical, and thermal properities of the resulting blend was examined. A strong interaction was observed between PPS and MABS by optical microsopy as well as scanning electron microscopy, exhibiting a well-dispersed morphological feature. The PPS/MABS blend showing a single glass transition temperature was observed in dynamic mechanical analysis, demonstrating a pseudo-homogeneous phase morphology induced by chemical compatibilization. PPS/MABS blend also exhibited an enhanced thermal stability and heat distortion temperature compared with modified PPS/ABS blend.

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Influence of Reaction Temperature on the Pyrolytic Product of Rice Straw by Fast Pyrolysis using a Fluidized Bed (볏짚의 급속 열분해 생성물에 대한 반응온도의 영향)

  • Kang, Bo-Sung;Park, Young-Kwon;Kim, Joo-Sik
    • Proceedings of the Korean Institute of Resources Recycling Conference
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    • 2005.10a
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    • pp.47-58
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    • 2005
  • Rice straw is one of the main renewable energy sources in Korea, and bio-oil is produced from rice straw with a lab. scale plant equipped mainly with a fluidized bed and a char removal system. We investigated how the reaction temperature affected the production of bio-oil and the efficiency of a char removal system. To elucidate how the temperature depended on the production of bio-oil, experiment were conducted between $450^{\circ}C\;and\;600^{\circ}C$ with a feed rate of about 300g/h. The mass balance was established in each experiment, and the produced gas and oil were analyzed with the aid of GCs and a GC-MS system. The char removal system is composed of a cyclone and a hot filter. In the experiments, we observed that the optimum reaction temperature range for the production of bio-oil is between $450^{\circ}C\;and\;500^{\circ}C$.

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