• Title/Summary/Keyword: 표층강도

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SHEAR BOND STRENGTH OF COMPOSITE RESIN TO ENAMEL FOLLOWING ENAMEL MICROABRASION (Enamel Microabrasion을 시행한 법랑질과 복합레진의 전단결합강도)

  • Hong, Kee-Sang;Lee, Sang-Dae;Lee, Sang-Hoon
    • Journal of the korean academy of Pediatric Dentistry
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    • v.27 no.1
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    • pp.45-53
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    • 2000
  • Enamel microabrasion is a means by which superficial enamel discoloration is removed using hydrochloric acid and fine pumice. As enamel microabrasion alone may not be sufficient in cases of deeper discoloration, composite resin restoration is recommended in areas where there is remaining discoloration. The purpose of this study was to investigate the effects of different methods and number of applications of enamel microabrasion on the shear bond strength of composite resin to enamel. Untreated control was designated as group 1. 5-second applications of a mixture of 18% HCl and fine pumice were performed 5 and 10 times on groups 2 and 3, respectively. A commercially available mixture of 10% HCl and abrasives(PREMA) was applied using a 10 : 1 gear reduction handpiece 5 and 10 times on groups 4 and 5, respectively, with each application lasting 20 seconds. After etching with 37% phosphoric acid, composite resin was bonded. Thermocycling was performed and shear bond strength was measured. The following results were obtained : 1. Group 2 showed the highest bond strength$(24.36{\pm}3.34)$, while group 3 showed the lowest$(19.35{\pm}3.43)$, Shear bond strength decreased in the following order: 2>4>5>1>3. 2. Group 2 showed bond strength significantly higher compared to groups 1 and 3(p<0.05). 3. There were no significant differences between groups 2 and 3, which had been microabraded using HCl and pumice, and groups 4 and 5, to which PREMA had been applied, when bond strengths were compared(p>0.05). 4. When modes of fracture were examined, adhesive failure was observed in groups 3 and 4, while cohesive failure was observed in groups 1, 2, 3 and 4. Only mixed failures were found group 5. 5. When viewed using a SEM, groups 2 and 3, which had been microabraded using HCl and pumice, showed surface appearances similar to that of enamel etched with phosphoric acid. Groups 4 and 5, treated with PREMA, exhibited a smooth surface similar to that of group 1. All oops showed similar, typical surface characteristics following phosphoric acid etching.

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THE EFFECT OF OXYGEN INHIBITION ON INTERFACIAL BONDING BETWEEN COMPOSITE RESIN LAYERS (복합레진 적층계면에서 oxygen inhibition의 영향에 관한 연구)

  • Choi, Su-Mi;Park, Jae-Hong;Choi, Sung-Chul;Kim, Kwang-Chul;Choi, Young-Chul
    • Journal of the korean academy of Pediatric Dentistry
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    • v.37 no.3
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    • pp.298-307
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    • 2010
  • The purpose of this study was to assess the effect on oxygen inhibition layer(OIL) for the interfacial bonding between resin composite layers, including shear bond strength, fracture modes and degree of conversion. The first layer of specimen was filled with Z-250(shade A3) and was cured for 40s. The second layer of specimen was filled with same composite(shade A1) and was cured for 40s. The first layer of specimens for each group were prepared by methods as followings. Control(curing in atmospheric air), Group1(curing against Mylar strip), Group2(scrubbed with a acetone-soaked cotton), Group3(using Tescera light cup), Group4(using Tescera heat cup), Group5(stored in disti1led water for 30days at $37^{\circ}C$), Group6 (using bonding agent). The results were as follows: 1. There was no statistically significant different shear bond strength between control and group 1(p>0.05). 2. Group 2 showed significantly lower shear bond strength than control and group 1(p<0.05). 3. The observation of the fracture surface leads to the evidence that a major difference occurs in the case of control, group1 and group 3 samples which break mainly cohesively while the other groups break in majority adhesively. 4. The results of FTIR showed that the degree of conversion was the highest in group 2 and the lowest in control group(p<0.05). It can be concluded that an OIL is not necessary for bonding with composite resin. But if a reduced critical amount of the unreacted monomer is present, it was detrimental to bonding additional layers of composite. Further study, such as the quantitative analysis of the unreacted monomer are required.

COMPARISON OF MICROTENSILE BOND STRENGTH OF COMPOSITE RESTORATION TO ERODED ENAMEL BY SURFACE TREATMENT (접착제의 종류에 따른 침식치아에 대한 복합레진의 결합강도)

  • Lee, Soon-Young;Lee, Kyung-Ho;Noh, Hong-Seok;Jeong, Tae-Sung;Kim, Shin
    • Journal of the korean academy of Pediatric Dentistry
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    • v.38 no.4
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    • pp.348-354
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    • 2011
  • Composite resin has been widely used for eroded enamel. But, as there have been many reports about the differences in physicochemical characteristics of eroded enamel compared with sound enamel, an additional effort was thought necessary to obtain the optimal bond strength. As a possible answer, we came to think about the application of infiltrant resin which is known to have an excellent penetration capacity into enamel. This study was performed for the purpose of comparing the bond strength of composite restoration with or without infiltrant resin under adhesives on the artificially eroded enamel. 60 extracted sound maxillary primary incisors were selected and divided into group 1, 2, 3 according to the number of artificial erosion cycling for 5 minute duration in 1% citric acid of pH 3.2 at $37^{\circ}C$. And the labial surfaces were divided into 3 areas; group A, only resin adhesive was used, group I, only infiltrant resin, group IA, infiltrant resin followed by resin adhesive. Afterwards, every specimen was restored with composite resin. Microtensile bond strength was measured and failure modes were observed. The obtained results were as follows: 1. In comparing the bond strength by the degree of enamel erosion, it was revealed the highest bond strength in group 1, followed by group 2 and 3, showing the lowest bond strength in most eroded group(p<0.05). 2. In comparing the bond strength by surface treatment methods, group IA and I showed higher value than group A(p<0.05), with unsignificant difference between group I and IA(p>0.05). 3. In observation of failure mode, it was shown higher frequency of cohesive failure in order of 1-2-3 and IA-I-A. Conclusively, it was shown decreasing tendency of bond strength as the enamel is more eroded, and infiltrant resin was thought helpful to replace or add to the resin adhesive for optimal bonding with eroded enamel.

Effect of Annual Ring Angles on Static Bending Strength Performances of Cross-Laminated Woods Made with Spruce (연륜경사각이 가문비나무 직교형적층재의 정적 휨 강도성능에 미치는 영향)

  • Sung, Eun-Jong;Kwon, Chang-Bae;Ryu, Hyun-Soo;Byeon, Hee-Seop;Park, Han-Min
    • Journal of the Korean Wood Science and Technology
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    • v.42 no.3
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    • pp.290-300
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    • 2014
  • In this study, cross-laminated woods were made with spruce wood and the effects of annual ring angles of perpendicular direction laminae on static bending strength performance were investigated. Static bending strength performances of parallel laminated woods with all layers composed of laminae perpendicular to the grain ($P_{\bot}$ type) were in the order of $90^{\circ}$ > $0^{\circ}$ > $45^{\circ}$. The MOE and MOR for the $45^{\circ}$ annual ring angle were 0.0989 GPa and 3.25 MPa, and it showed the lowest values. By placing longitudinal-direction laminae in the core of $P_{\bot}$ type, the strength performances were markedly improved. In the case of cross-laminated woods with perpendicular-direction laminae in the faces ($C_{\bot}$ type), the bending strength performances were in the order of $90^{\circ}$ > $0^{\circ}$ > $45^{\circ}$, but the differences among annual ring angles were less than those of the parallel-laminated woods. In the case of cross-laminated woods with perpendicular-direction laminae in the core ($C_{\parallel}$ type), the bending strength performances were in the order of $45^{\circ}$ > $90^{\circ}$ > $0^{\circ}$ unlike $P_{\bot}$ type and $C_{\bot}$ type. The MOE and MOR for the $45^{\circ}$ annual ring angle were 12.0 GPa and 55.8 MPa, and it showed the highest values.

Consideration on Changes of Density Stratification in Saemangeum Reservoir (새만금호 내 밀도 성층 변화 고찰)

  • Oh, Chan-Sung;Choi, Jung-Hoon
    • Journal of the Korean Society for Marine Environment & Energy
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    • v.18 no.2
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    • pp.81-93
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    • 2015
  • The comprehensive master plan in November 2010 on Saemangeum internal development has been released, and there is a need for complementary measures related to in-situ monitoring methods in order to acquire water temperature (T) and salinity (S) data. Thus, these data are monitored and analyzed by Korea Rural Community Corporation continuously. The purposes of current study are to evaluate the distributions of seasonal T and S, sigma-t, and stratification parameter and to compare annual stratification system in 2011 and 2012. To achieve these objectives, monthly vertical changes of T, S, and sigma-t, which are reproduced by a kriging technique, have been analyzed. In summer, the temperature difference between surface and bottom layers varies from 2 to $3^{\circ}C$, and the stratification of T is considerably weak. The stratification of S occurs abruptly within depth of EL. (-)5 to EL. (-)10 m. Therefore, stratification is induced by sudden increasing of water inflow amount due to a localized downpour during the rainy season, and these stratification processes are strongly influenced by inflowing a fresh water from watersheds in estuary environment.

Floc Property of Yeongsan Cohesive Bed Sediment with Respect to Salinity and Sediment Concentration (점착성 퇴적물의 염분과 퇴적물농도에 따른 플럭 특성: 플럭카메라를 이용한 실험연구)

  • Shin, Hyun-Jung;Smith, S. Jarrell;Lee, Guan-Hong
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.18 no.3
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    • pp.122-130
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    • 2013
  • To examine floc characteristics of cohesive bed sediment of the Yeongsan River estuary, a floc camera system has been developed and utilized to observe flocs under varying conditions. In order to validate the floc camera system, sand particles were passed through 88-125 and $63-88{\mu}m$ sieves and observed within the laboratory. Mean grain size and settling velocities were found to be 102 and $56.2{\mu}m$ and 6.7 and 5.9 mm/s, respectively. Artifacts of particles estimated outside of the sieve range are attributed to being imaged out of the depth of focus. However, as mean grain size and settling velocity of each size class were within the confidence interval, the floc camera system was confidently used to examine cohesive bed sediments of Yeongsan River estuary. The bed sediment sample was prepared with a concentration of 0.1 g/L in 0 psu deionized water. The mean grain size, settling velocity and fractal dimension of flocs were $40.6{\pm}0.66{\mu}m$, 14 mm/s, and 2.86, respectively. Experiments were also conducted using different salinities (10 and 34 psu) and sediment concentrations (0.1 and 0.3 g/L). Despite changing these parameters, the mean observed grain size and settling velocities were found to be the same within the error range of the system. The relatively higher values of settling velocity and fractal dimension are considered a result of the sediment containing relatively small concentrations of organic matter. Moreover, consistent floc size over various grain sizes and concentrations may be the result of insufficient turbulence to aggregate flocs.

Characterization of Carbonized MDF by Scanning Electron Microscopy and X-ray diffraction (주사전자현미경 및 X선회절법에 의한 탄화 MDF의 특성)

  • Lee, Seon-Hwa;Park, Sang-Bum;Kwon, Sung-Min;Park, Jong-Young;Kim, Nam-Hun
    • Journal of the Korean Wood Science and Technology
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    • v.37 no.3
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    • pp.208-215
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    • 2009
  • As a fundamental study to develop absorbing materials on harmful volatile organic compounds (VOC) such as formaldehyde, structural and crystalline characteristics of MDF carbonized at different temperatures were examined by a scanning electron microscope and an X-ray diffraction method. Fibers in surface layer of MDFs showed more compressed morphology than those in middle layer of MDFs, but the porosity of MDFs increased with increasing the carbonized temperature. The wrinkle shape was frequently surfaces of cell walls was more severe than that at the lumina of cells. The shape of pits in the fibers of carbonized MDFs were hardly changed. The cell walls of MDFs carbonized at $400^{\circ}C$ and over showed an amorphous-like structure without cell layering. X-ray diffratograms from the MDFs carbonized at $400^{\circ}C$ showed a trace of crystalline cellulose. On the other hand, an amorphous diffraction pattern from carbons was obtained with the MDFs carbonized at $1,000^{\circ}C$.

CO2 net atmospheric flux estimation and influence factors analysis in a stratified reservoir (성층화된 저수지에서 CO2 NAF 산정 및 영향 인자 분석)

  • Park, Hyung Seok;Chung, Se Woong;Lee, Eun Ju
    • Proceedings of the Korea Water Resources Association Conference
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    • 2019.05a
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    • pp.73-73
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    • 2019
  • 지구 표면의 약 2%에 해당하는 담수에서 육상계 전체가 흡수하는 탄소의 50%가 배출되며, 이는 토양표면에서 배출되는 탄소량에 비해 더 큰 수치로 전 지구적 탄소순환 해석에 중요한 역할을 한다. 특히, 내륙수역과 대기의 경계면에서 $CO_2$ 이동은 전 지구적 탄소순환의 중요한 구성요소로 평가되고 있다. 호수와 저수지 같은 담수 저류시설은 육상에서 기인한 탄소의 운송 및 처리 역할을 한다. 하지만, 저수지에서 온실가스배출량을 평가할 수 있는 명확한 방법론이 부족하며, 전지구 규모 GHGs배출량에 대한 추정에 대한 불확실성이 상당히 큰 상황이다. 본 연구에서는 몬순기후대에 위치한 인공저수지를 대상으로 보다 신뢰도있는 온실가스 배출량 추정을 위해 $CO_2$ NAF 산정하고, 산정에 영향을 미치는 인자들을 분석 하였다. 분석을 위해 $CO_2$ NAF 산정에 필요한 수리 및 수질 인자들을 2017년부터 2018년까지 수집하고, 기초통계량 및 상관분석을 실시하였다. 또한, 주성분분석(PCA) 및 다중선형회귀모델(MLR)과 랜덤포레스트(RF) 기법을 사용해 변수 중요도를 평가하였으며, $CO_2$ NAF 산정 주요인자인 기체교환 계수를 경험적 모델 3종(Cole and Caraco, Crusius, Vachon), 표면갱신형 모델 4종(Heiskanen, Maclntyre, Read, Soloviev)을 비교, 검토하였다. 조사기간 동안 기체교환계수 산정 결과 Crusius 모델 예측값이 평균 $0.342(0.047{\sim}4.323)cm\;hr^{-1}$으로 검토한 모델중 가장 낮은 평균값을 보였으며, Heiskane 모델이 $2.135(0.337{\sim}5.152)cm\;hr^{-1}$으로 가장 큰 평균값을 보였다. 대상 수체는 연주기로 완전혼합되며 수온성층이 약화되는 시기에 저수지 표층 아래에 축적된 탄소가 표층으로 전달되어 높은 수준의 p$CO_2$를 보이며, 수표면에 큰 난류 강도가 작용하는 기간에 대기중으로 배출(pulse emission) 기작이 나타난다. NAF 산정결과 경험적 모델의 NAF값($-1246.0{\sim}6510.3mg-CO_2m^{-2}day^{-1}$)은 표면갱신형 모델 NAF값($-1436.1{\sim}8485.7mg-CO_2m^{-2}day^{-1}$)보다 낮은 수준을 보였으며, 풍속의 함수만을 이용하는 경험적 모델보다 부력 플럭스와 난류 혼합의 영향을 고려하는 Macintyre, Heiskanen모델이 성층 저수지의 $CO_2$ NAF 산정에 적합한 것으로 나타났다. $CO_2$ NAF 산정의 주요인자로 MLR모델은 Tw, EC, pH, Chla, TOC, Alk, RF모델은 EC, DO, TOC가 중요 변수로 평가되었다. PCA 분석결과, 수온이 낮고 성층이 약화되며 pH가 낮은 상태에서 NAF가 큰 것으로 나타났다.

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Early Age Behavior of Thin Bonded Continuously Reinforced Concrete Overlay on Aged Jointed Plain Concrete Pavement (노후 줄눈 콘크리트 포장 보수를 위한 얇은 연속 철근 콘크리트 덧씌우기 포장의 초기거동 평가)

  • Ryu, Sung-Woo;Nam, Jung-Hee;Kim, Ki-Heun;Cho, Yoon-Ho
    • International Journal of Highway Engineering
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    • v.11 no.2
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    • pp.121-132
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    • 2009
  • Thin bonded continuously reinforced concrete overlay(CRCO) was constructed on He existing jointed plain concrete pavement(HCP) surface at Seo-Hae-Ahn express highway in South Korea in order to evaluate its applicability and performance. Two sections of road were considered for this evaluation. In the first section, the concrete overlayer was placed and cut down to the existing layer to form transverse joints while CRCO was constructed on top of the existing layer in the second section. Early strength concrete(Type III) was utilized for both overlay sections. The depth of milling and the thickness of overlaid layer were 5 cm and 10 cm, respectively. Several vibrating wire gauges(VWG) were installed to evaluate the performance of CRCO with respect to curling, delamination, and crack propagation. As a result of the strength test, it was found that strength of the material reaches the design criteria within 1-3 days. Analysis with vibrating wire gauge(VWG) showed CRCO effectively restricts joint movement. High adhesive strength also was observed from the material regardless of length of aging. Meanwhile, transverse cracks were observed on the middle of the section where JPCP overlay was applied whereas arbitrarily cracks in transverse direction were observed on the section where CRCP was applied.

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Microstructural Realization of SD400 Rebar by Developing Tempcore Simulation Apparatus (템프코어 냉각모사 장치 개발을 통한 SD400 철근 미세조직 구현)

  • Park, Chun Su;Yi, Hyang Jun;Bae, Seh Wook;Kim, Gil-Su
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.39 no.5
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    • pp.543-547
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    • 2015
  • The cooling process referred to as Tempcore has been applied to produce a high-strength rebar. Excellent rebar with strength and weldability can be manufactured from mild steel without the addition of alloying elements by using the Tempcore process. However, there are limitations to evaluating the effect of various chemical compositions and cooling conditions within a site facility. In this study, we developed an apparatus to simulate the Tempcore process and obtained microstructures with a hardened surface layer, an intermediate region and a soft inner core. The experimental apparatus has been equipped with a cooler set that is the same as the site facility and consists of a pump line that supplies pressure of 12-13 bar and flow rate of up to $50m^3/h$. In accordance with the simulation result of steel grade SD400 that requires more than 400 MPa of yield strength, both the hardened area ratio and the hardness with respect to each cooling depth were found to agree well with the product.