• Journal of Conservation Science
• /
• v.33 no.2
• /
• pp.61-73
• /
• 2017

In order to identify the application techniques of wooden lacquerware artifacts, optical/polarized light microscopy, Fourier transform infrared (FT-IR) spectroscopy, and scanning electron microscopy (SEM) equipped with energy dispersive X-ray analysis (EDX) were conducted on the lacquer films of 61 wooden lacquerware artifacts excavated from the Imdang-dong site, Gyeongsan, Korea. Powdered soil, soot, and charcoal were used as a filler for the undercoat, and iron oxide ($Fe_2O_3$) was used as a red pigment. Five different applying techniques were identified for the undercoat according to the composition of the lacquer. Eight different application techniques were identified for the final coat (on the middle layer and surface layer). Totally seventeen application techniques were identified based on the combination methods of the undercoat and finalcoat. Consequently, the undercoating techniques of Imdang-dong lacquerwares were found to be similar to those of lacquerwares from excavated in other provinces. However, the use of iron oxide as a red pigment at Gyeongsang province is very characteristic compared with others.

• 한국문화재보존과학회:학술대회논문집
• /
• 2004.10a
• /
• pp.101-102
• /
• 2004

• Conservation Science in Museum
• /
• v.4
• /
• pp.79-88
• /
• 2003

The lacquer ware objects of Nangnang were treated for conservation and seven of them were studied on the manufacturing technic. When we examined them using microscopes and an SEM-EDS analysis, the lacquer layer was proved to consist of two parts: the ground and the upper lacquer. The ground coating was made of several mixed materials such as powdered bone and minerals. Many forms of powdered bone were observed. We could find out that HgS, PbO and AgS were used as pigments. We could also find out a specific process and materials were used for those objects, although we could not say definitely what they were because the number of the sample was not big enough.

• Conservation Science in Museum
• /
• v.15
• /
• pp.78-95
• /
• 2014

To examine the materials, production techniques, and key features of Goryeo wooden lacquerwares, scientific analysis was conducted on six relevant lacquerware items. All of the items, except for a lacquered bowl ^{duksu 4123}, were found to have been made by first covering the surface of the wood with cloth and then varnishing with lacquer. The wooden frames of flower-shaped lacquered case and pine leaves shape lacquered case were made by wrapping thin wood around either the lid or bottom panel. In most cases, microscopic analysis revealed a lower layer of lacquer mixed with bone ash and bone dust, followed by an upper varnish layer of lacquer. SEM-EDS analysis and μ-XRF ^{Micro-X-ray Fluorescence} analysis showed that vermilion lacquer mixed with cinnabar was used on the surface. A lid decorated with a dot pattern was made by first varnishing the surface with yellow lacquer mixed with orpiment, and then irregular dot pattern with a mixture of black lacquer and soot. The vermilion lacquer used to varnish the side of the lacquered bowls was composed of lacquer mixed with cinnabar and minium ^{Red Lead}.

• Conservation Science in Museum
• /
• v.8
• /
• pp.41-47
• /
• 2007

The wooden lacquer wares, which had excavated from the water reservoir in the Isong Sansung Fortress, were applied with vacuum freeze drying method and treated, after they had been substituted with tbutanol, and treated with PEG-pretreatment. The manufacturing technique, which had not been investigated in the past, was examined through the investigation of the wood and the lacquer used for wooden lacquer wares, and the pieces of the lacquer wares, which had been stored for a long time, were restored for the exhibition and conservation. As the result, the wooden lacquer wares were manufactured, using black alder belonging to the group of Alnus, and the lacquer was painted on the bottom-layer by mixing the powdered soil and lacquer, and it was confirmed that the lacquer mixed with the black pigment and the pure lacquer had been painted alternatively over 2 times, and that the wooden lacquer ware had been manufactured through total 5 times of being painted.

• Journal of Conservation Science
• /
• v.21
• /
• pp.49-58
• /
• 2007

Among the treatment results of test samples of the antique lacquer-ware, the treatment with PEG#3,350 40% solution displayed excellent effect with low shrinkage ratio; in weight gain the treatment with Sucrose 19%+Glycerin 1%(t-butanol 5% in water) solution showed consistent increase. However during the impregnation process of Sucrose, the weight of the testing samples decreased by dehydration because the inner part of the test samples and the treatment solution showed concentration gradient. Therefore, we concluded longer impregnation period should be necessary to prevent dehydration. Since both higher and lower molecular weight treatment chemicals could penetrate into the wood of the lacquer-ware, air drying and conditioning after impregnation treatment with high concentration chemicals would be possible, as well as vacuum freeze-drying.

• Journal of the Korean Chemical Society
• /
• v.34 no.2
• /
• pp.130-135
• /
• 1990

The title compound (C13H17NO2S) is monoclinic, space group P21/a, with a = 13.756 (3), b = 9.310(4), c = 21.305(3) $\AA$, $\beta$ = 95.0。, Z = 8, V = 2718.11 $\AA$3, Dc = 1.23$g·{\cdot}cm-3$, (Mo k$\alpha$) = 0.71069$\AA$,$\mu$ = 2.18 cm-1, F(000) = 1071.86, T = 298, R = 0.085 for 2935 unique observed reflections with I >2.0$\sigma$(I). The structure was solved by direct methods. The C-H bond lengths and the methyl groups are fixed and refined as their ideal geometry by allowing to ride on the parent atoms. Both molecules A and B have almost same structures except for two terminal ethyl groups. The ethylene-like skeleton including the nitro group in one molecule is nearly perpendicular to the plane of the methylbenzene group and two ethyl groups form a cis-type structure which has the dfferent orientations between two molecules; in the molecule A, two terminal methyl groups being the opposite directional arrangement against the plane of its skeleton, while in the B, with the same directional structure from its plane. The molecules in the crystal are packed together by non-bonded van der Waals forces.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2000.11a
• /
• pp.489-493
• /
• 2000

Turbine blade has trouble of cracking at root region. Fracture surface of blade root is surveyed by SEM and AFM to clear relation between fracture mechanical parameter and surface parameter (striation width and surface roughness). Service stress is predicted by maximum height roughness $R_{max}$, on fractured surface and stress analysis on turbine blade. It is to thought that turbine blade is fractured by abnormal condition such as incorrect fittings between pin and pin hole but isn't fractured by normal service conditions such as steam pressure, centrifugal force and torsional force.

• Journal of Life Science
• /
• v.30 no.5
• /
• pp.460-467
• /
• 2020

Hepatocellular carcinoma (HCC) is one of the most commonly diagnosed cancers in the word. Although radiation and chemotherapy are generally effective, there are various side effects that greatly limit the effectiveness of these treatments. Therefore, traditional herbs may have potential as important resources for the discovery of liver cancer therapeutics. In this study, we selected three Korean herbal medicine formulas from the Donguibogam, namely Bigihwan (BGH), Daechilgithang (DCGT), and Mokwhyangbinranghwan (MHBRH), and evaluated their anti-cancer effects on HCC cells. According to our results of three ethanol extracts, BGH was more effective at suppressing HCC growth than DCGT or MHBRH. Furthermore, flow cytometry analysis showed that inhibition of HCC proliferation by the three extracts was associated with the induction of apoptosis and autophagy. In particular, BGH significantly increased mitochondrial impairment and showed the possibility of inducing mitophagy in comparison with the other two extracts. BGH prominently upregulated the levels of microtubule-associated protein light chain-3 which was accompanied by a decrease in the expression of anti-apoptotic Bcl-2 without altering the expression of pro-apoptotic Bax. In addition, the levels of PTEN-induced kinase 1 were also markedly increased in BGH-treated HCC cells. Moreover, autophagy blocking improved cell viability and reduced apoptosis after the three treatments, indicating that autophagy by these extracts enhances HCC cells against cytotoxicity. In conclusion, our findings show that BGH demonstrates the highest anti-cancer activity among the three formulas and inhibits the proliferation of HCC cells through autophagy induction.

• Journal of Conservation Science
• /
• v.33 no.1
• /
• pp.17-24
• /
• 2017

Studies were conducted on manufacturing techniques by applying microscopy and conservation treatments on the annals of Joseon dynasty storage box at the National Museum of Korea. The results revealed that lime tree wood(Tilla spp.) was used to make the annals of Joseon dynasty storage box. Lacquering techniques were used to coat the box with a layer of lacquer and bone ash and then cover it with traditional Korean paper. After being covered with traditional Korean paper, more layers were applied in the following sequence: mud ashes, black lacquer, pure lacquer, and black lacquer. Before conservation treatments, some components and lacquer layers were missing in addition wood joint were loose. Therefore, conservation and restoration should be conducted based on the identified wood and by observing the shape of the remaining components.