• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2006.05a
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• pp.81-85
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• 2006

Through-the-thickness properties of thick-walled cylindrical composites are required to determine structural performances because interlaminar tensile stress is primarily responsible for structural failure of the composites during their curing process. It is necessary for evaluating the tensile properties to find individual test methods to find appropriate methods because there are no recognised international standards(test methods and test specifications) available for generating reliable tensile properties in the direction. This paper has performed an experimental Study to measure that properties of carbon fabric/phenolic composites are produced by domestic company. Several test methods using an aluminum specimen were compared and evaluated. The best method, found out, was adopted to measure transverse through-the-thickness properties of composite materials. The results show that strain trends on four faces of composite specimen are the same.

• Journal of the Korean Society of Propulsion Engineers
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• v.10 no.3
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• pp.48-52
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• 2006

Through-the-thickness properties of thick-walled cylindrical composites are required to determine structural performances because interlaminar tensile stress is primarily responsible for structural failure of the composites during their curing process. It is necessary for evaluating the tensile properties to find individual test methods to find appropriate methods because there are no recognised international standards(test methods and test specifications) available for generating reliable tensile properties in the direction. This paper has performed an experimental study to measure that properties of carbon fabric/phenolic composites which are produced by domestic company. Several test methods using an aluminum specimen were compared and evaluated. The best test method to measure transverse through-the-thickness properties of composite materials was developed by the experimental results that strain trends on all faces of composite specimen are the same.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.35 no.1
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• pp.58-65
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• 2007

Mixed mode interlaminar fracture behaviors of carbon fabric/epoxy composites were investigated through MMF (Mixed Mode Flexural) test by varying mixed mode ratio ranging from 20% to 90%. Mixed mode interlaminar fracture criteria based on NL point and 5% offset point were also suggested in order to predict mixed mode interlaminar fracture behaviors. Fracture surfaces and crack propagating behaviors were examined through a travelling scope and a scanning electron microscope. According to the results, mixed mode interlaminar fracture behaviors can be predicted by mixed mode interlaminar fracture criterion with m=1.5 and n=0.5 on the basis of NL point or mixed mode interlaminar fracture criterion with m=2 and n=3 on the basis of 5% offset point. Fracture surfaces and crack propagating behaviors are sensitive to mixed mode ratios. MMF test can be successfully applicable in evaluating mixed mode interlaminar fracture toughness of carbon fabric/epoxy composites.

• Composites Research
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• v.26 no.2
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• pp.141-145
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• 2013

The mode II interlaminar fracture toughness was evaluated for CFRP laminates with different types of nonwoven tissues and the source of increased mode II interlaminar fracture toughness was examined by SEM analysis in this paper. The interlaminar fracture toughness in mode II is obtained by an end notched flexure test. The experiment is performed using three types of non-woven tissues: 8 $g/m^2$ of carbon tissue, 10 $g/m^2$ of glass tissue, and 8 $g/m^2$ of polyester tissue. On the basis of the specimen with no non-woven tissue, interlaminar fracture toughness on mode II at specimens inserted with non-woven carbon and glass tissues and polyester tissues increases as much as 166.5% and 137.1% and 157.4% respectively. The results show that mode II interlaminar fracture toughness of CFRP laminates inserted with nonwoven tissues increased due to the fiber bridging, fiber breakage, and hackle etc. by SEM analysis.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 1997.11a
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• pp.29-29
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• 1997

각광 받는 구조재료인 섬유강화 복합적층재에 대한 기계적 체결 거동은 본질적인 재료의 이방성에 의해서 파단강도가 파단 모우드와 매우 밀접한 관련을 갖는 것으로 알려져 있다. 따라서, 복합적층판 체결부의 정밀 구조 설계에서는 단순화에 따른 오차를 줄이고 정밀해에 의한 설계 및 해석이 요청된다. 특히, 층간응력 성분을 무시할 수 없는 두께를 갖는 복합적층 판의 기계적 체결부 해석이나 실제 구조물의 체결부에서 발생하는 굽힘이나 비틀림과 같은 하중 상태를 묘사하기 위해서도 정밀한 3차원 응력 해석은 필요하다. 하지만, 지금까지 기계적 체결부의 거동에 관한 연구는 층간응력 성분들을 어느정도 무시할 수 있는 얇은 평판에 대한 2차원 응력해석에 주로 국한되어 왔으며, 일부 수행된 체결부에 대한 3차원 응력 해석의 경우 여러 단점을 갖는 3차원 연속체 요소에 의한 유한요소 해석이 수행되었을 뿐이다.본 연구는 층간응력 성분들을 무시할 수 없는 두께를 갖는 복합적층판의 기계적 체결부 해석에 지금까지 사용되어온 3차원 연속체 요소에 의한 유한요소 방법이 갖는 단점들을 개선한 Layerwise 유한요소법을 이용하여 3차원 응력해석을 수행하였다. 특히, 선형상보성원리에 근거한 최적설계 기법을 응용하여, 기계적 체결시 핀과 적층판의 홀 사이에 발생하는 하중 전달 과정을 모사하고, 접촉력에 의한 홀 주위의 복잡하고 국부적인 응력 집중현상을 규명하여본다.

• Composites Research
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• v.28 no.3
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• pp.94-98
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• 2015

This paper reports the effects of nickel film interleaves on the interlaminar shear strength(ILSS) of carbon fiber reinforced epoxy composites(CFRPs). A nickel thin film was deposited onto the prepreg by radio frequency(RF) sputtering at room temperature. The ILSS of the nickel film interleaved hybrid composites was increased compared to that of the composites without interleaves. To understand the mechanism of enhancement of the ILSS, the fracture surface of the tested specimens was examined by scanning electron microscopy(SEM). The metal interleaves were acted as a reinforcement for the matrix rich interface and the shear property of their composites improved by enhancing the resistance to matrix cracking.

• Transactions of the Korean Society of Mechanical Engineers
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• v.10 no.2
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• pp.198-207
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• 1986

This study investigates interlaminar fracture characteristics of Graphite/Epoxy composite (HFG Graphite/Epoxy) under mode I (opening mode), mode II (sliding mode) and mixed mode loading conditions. The effects on interlaminar fracture toughness due to different fiber orientations on the crack surface are also investigated. The antisymmetric test fixture proposed by M. Arcan is used for this test. Both critical stress intensity foctors and critical energy release rates were determined and several mixed mode fracture criteria were compared to the experimental data. Also fracture surfaces were investigaed to obtain informations on the fracture behaviors of Graphite/Epoxy composite by means of a scanning electron microscope(SEM).

• Elastomers and Composites
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• v.34 no.1
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• pp.31-44
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• 1999

Interfacial adhesive strength between the fully-crosslinked and partially-crosslinked rubber layers were Investigated at the temperature range of $30{\sim}120^{\circ}C$ for four different rubbers(NR, SBR, EPDM, BIMS). The surfaces of interfacial failure were also investigated using a scanning electron microscopy(SEM). The physical interlinking played a major role in the adhesive strength between the fully-crosslinked rubber layers. When a partially-crosslinked rubber layer was bonded to the fully-crosslinked one, the chemical as well as the physical interlinking affected the adhesive strength. NR showed a "interfacial knotty tearing" pattern, while EPDM showed a typical "cross-hatched" one when the adhesive strength approached to the cohesive tear strength of each material.

• Proceedings of the KSR Conference
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• 2008.11b
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• pp.1668-1673
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• 2008

고분자 복합재 구조물의 경우 일반적으로 여러 층의 단층(laminar)이 적층된 구조로 이루어져 있으며, 모재균열, 층간분리 및 섬유파단과 같은 손상이 발생되어 파단에 이르게 된다. 자가손상 복구기법은 복합소재의 열경화성 수지 내에 손상복구액을 포함하고 있는 마이크로캡슐과 촉매를 투입하여 외부의 도움 없이 손상을 치료할 수 있는 방법으로, 소재의 디자인에 있어서 새로운 페러다임을 제공할 수 있는 것으로 현재 많은 연구가 진행되고 있다. 본 연구에서는 ENB(5-ethylidene-2-norbornene)와 DCPD(dicyclopentadiene)에 대하여 DMA(dynamic mechanical analysis)와 DSC(differential scanning calorimetry)를 이용하여 특성을 분석하였다. 또한 그들의 ROMP(ring-opening metathesis polymerization)반응과의 관계를 조사하였으며, ENB와 DCPD 블렌드에 대한 복구액으로서의 특성도 조사하였다. 본 연구실에서 합성된 두 가지 다른 종류의 ROMP 경화제에 대한 실제 자가손상복구에으로서의 적용상 특성도 연구하였다.

• Journal of the Korean Society of Propulsion Engineers
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• v.5 no.4
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• pp.20-30
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• 2001

This study represents the Nondestructive Test about impact damage of composite materials made by different lay-up patterns and degrees. For this study, they were examined by the drop test on composite materials of two type lap-up patterns with fabric and unidirectional prepreg and examined nondestructive test of those. Nondestructive methods were X-ray test with $ZnI_2$ penetrant and Ultrasonic C-scan. The defect detectability of X-ray and Ultrasonic test was compared according to defect species. And the amounts of damage on impacted zone wert compared according to impact energy on two type test specimens. At results, Ultrasonic test was more effective to detect delamination and Penetrant X-ray test was more effective to detect matrix crack and fiber fracture. There were some differences in defect shapes and grades according to lay-up patterns and degrees, and the trend appeared that matrix crack, delamination, fiber fracture occured and increasing defects sizes according to increasing impact energy.