• Title/Summary/Keyword: 체화인지

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A Study of Tensile Strength in 18% Ni Maraging Steel Sheet Welded with Electron Beam (E.B 용접된 18% Ni 마르에이징강 박판의 인장이음강도에 관한 연구)

  • 정병호;김무길;김원녕
    • Journal of Advanced Marine Engineering and Technology
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    • v.21 no.2
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    • pp.157-165
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    • 1997
  • The strength level of welded joint in room temperature and elevated temperature up to $600^{\circ}C$ was investigated in 250 and 300 grade 18% Ni maraging steel sheet welded with electron beam. The results obtained in this study are as follows; 1. Optimum welding heat input was 600J/cm in 1.0mm thickness and the room temperature tensile strength, joint efficiency of welded joint treated with optimum aging condition were found to be about 166kg/$mm^2$, 95% in 250 grade, 189kg/$mm^2$, 92% in 300 grade maraging steel sheet, respectively. 2. Tensile strength of welded joint in room temperature increased slightly by aging after repeated solution heat treatment, but the fracture mode showed a shear. 3. Joint efficiency at a temperature between $540^{\circ}C$and $600^{\circ}C$ found to be about 72% to 55%, but the joint efficiency exceeded about 90% below $300^{\circ}C$. 4. The fracture occurred in most weld metal, and the fracture surface showed a shallow dimple.

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UV-HPLC Determination of Carbowyl Group Using 2-Bromoacetyltriphenylene as a Pre-labeling Reagent - The isolative determination of prostaglandin $E_2$ and $F_2{\alpha}$ by HPLC (2-Bromoacetyltriphenylene 유도체화제를 이용한 카르복실기 함유성분의 분석법 (I) - 프로스타글란딘 $E_2$$F_2{\alpha}$ 혼합물의 HPLC에 의한 분리정량)

  • 이왕규;정해수;김박광
    • YAKHAK HOEJI
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    • v.30 no.6
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    • pp.311-316
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    • 1986
  • A new UV labeling reagent was developed and used in HPLC for the determination of prostaglandin $E_2$ which have weak UV light-absorbing property. This reagent, 2-bromoacetyltriphenylene, was synthesized by the bromination of 2-acetyltriphenylene which was obtained from triphenylene by Friedel-Crafts reaction. The wave length maximum (${\lambda}_{max}^{CH_3CN}$ of this reagent was 268nm. Prostaglandin E$_2$ was extracted from prostaglandin E$_2$-$\beta$-cyclodextrin using a Sep-pak $C_{18}$ cartridge. The prostaglandin E$_2$ was labeled with 2-bromoacetyl-triphenylene in aectonitrite using 18-crown-6-ether as catalyst. Derivatized prostaglandins were separated on a reversed-phase column (Radial-pak) $\mu$-Bondapak $C_{18}$ using acetonitrile: water=60:40 as mobile phase. The effluent was monitored by UV detector at 254nm filter kit. Linearity of calibration curve was obtained between 30ng and 140ng, and the lower limit of detection was 5ng.

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A Study on the Flexural Behaviors of RC Slabs of Widened Bridges (확폭교량 RC 상판의 휨거동에 관한 연구)

  • 홍순길;장동일
    • Magazine of the Korea Concrete Institute
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    • v.6 no.3
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    • pp.152-161
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    • 1994
  • Most widened bridges have been constructed by the joining-construction method that makes new and existing bridges structurally a single structure. Since the joining-construction method has several problems in design and construction viewpoint, this study is conducted in order to investigate the structural behaviors of RC slabs, which are widened and influenced by traffic-induced vibration of existing bridge during placing and curing of new concrete, with the prototype flexural strength test and FEM analysis. It was found that cracks are generated in construction joint at low applied load and that stress concentration at the joints and slips between steel bar and concrete are occured. But, the decreasing of load carrying capacity is negligible according to the traffic-induced vibration as well as the difference of construction method.

A Study of Annealing Heat-treatment for Ti(Grade 2) by Electrochemical Methods (전기화학적 방법을 이용한 Ti(Grade 2)재의 최적 어닐링 열처리에 대한 연구)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.90-98
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    • 2002
  • In this paper, the annealing heat treatments for the best corrosion resistant of Ti(Grade 2) were studied in a 3.5% NaCl solution by electrochemical methods. The annealing heat treatments were accomplished at 650, 700 and $750^{\circ}C$ with different time of 30min., 1hour and 2 hours in a vacuum condition. The obtained results are: 1) in the case of solution heat treated $930^{\circ}C$ for 2 hours in a vacuum and air, the corrosion potentials were -348.7 and -567. 1mV, and current densities 2.32 and $22.62\mu\textrm{A}$, respectively, 2) as increase both annealing heat treatment temperature 650, 700, $750^{\circ}C$ and time 30min., 1 hour, 2 hours, the corrosion potential were decreased, whereas corrosion current density increased, 3) in the case of cyclic polarization, the measured charges were increased as increasing solution heat treatment temperature and time, 4) on the bases of corrosion potential, current density and charge, the best annealing temperature and time were measured as $700^{\circ}C$ and 30min. for Ti(Grade 2) material.

Constructive Artificial Intelligence (구성적 인공지능)

  • Park Choong Shik
    • Korean Journal of Cognitive Science
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    • v.15 no.4
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    • pp.61-66
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    • 2004
  • I think constructivism can be considered as the new count proposal for understanding human to Cartesian rationalism. Constructivism has the common area not only with recent results of evolutionary biology, evolutionary psychology. brain science, system theory, and complex adaptive system but also with recent trends of humanities, and social science. In artificial intelligence, the studies which can be considered as constructivistic methods is going on. In this paper, from a constructivistic pint of view, to broaden the concept of intelligence in artificial intelligenve, I will examine constructivistic methodologies to intelligent machine and look about the artificial intelligence techniques which are constructivistic. Throughout such a discussion I want to promote the integral understanding of various kinds of mind theories and techniques, and pave the way of general intelligence in artificial intelligence.

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Application and Optimization of the IsoButoxycarbonyl Derivatization method to the Analysis of Trace Level Phenols in Environmental Samples (환경시료로부터 미량 페놀류의 분석을 위한 isoButoxycarbonyl 유도체화 분석방법 적용 및 최적화)

  • Kim, Hyub;Hong, Jong-Ki;Kim, Yong-Hwa;Kim, Kyoung-Rae
    • Environmental Analysis Health and Toxicology
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    • v.17 no.1
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    • pp.37-51
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    • 2002
  • Eleven phenols including two chlorophenols, eight alkylphenols and bisphenol A were derivatized with isobutylchloroformate to form their isobutoxycarbonyl derivatives. Standard phenol mixture was concentrated for the isobutoxycarbonyl (isoBOC) derivatization and analysed by gas chromatography/mass spectrometry (GC/MS). The recoveries of the derivatization method of alkylphenols, chlorophenols, and bisphenol A were calculated by gas chromatography/mass spectrometry-selected ion monitoring mode using two work-up methods for comparison; shaking and heating method. The linear detector responses were obtained in the concentration range of 5∼400 ng, with correlation coefficients varying from 0.9755∼0.9981. Recoveries of the alkylphenols, chlorophenols, and bisphenol A were determined by gas chromatography/mass spectrometry-selected ion monitoring mode using two work-up methods for comparison ; the US-EPA method and the isoBOC derivatization method, Eleven phenols in water samples were extracted with dichloromethane and then concentrated. Also, solid-phase extraction (SPE) with XAD-4 and subsequent conversion to isobutoxycarbonyl derivatives for sensitive analysis with the selected ion-monitoring (SIM) mode. The recoveries were 85.1∼109.9% and 90.3∼126.6% for the US-EPA method and the isoBOC.

Determination of total iodide in seawater by gas chromatography-mass spectrometry (Gas chromatography-mass spectrometry를 이용한 해수 중 총 요오드 정량분석)

  • Shin, Ueon-Sang
    • Analytical Science and Technology
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    • v.15 no.5
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    • pp.445-450
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    • 2002
  • A sensitive gas chromatographic method has been established for the determination of total iodide in seawater as their volatile organic derivative. The method is based on the formation of 4-iodo-2,6-dimethylphenol with 2,6-dimethylphenol in matrix and a single-step extraction of the derivative with ethyl ether, which are then measured by gas chromatography-mass spectrometry (selected ion monitoring). Iodate in sea water was completely reduced to iodide with ascorbic acid and acetic acid. The detection limit was 0.1 ng/mL in seawater and the calibration curve showed good linearity with r=0.9997. The method was sensitive, reproducible and simple enough to permit the reliable routine analysis of total iodide in seawater. Total iodide in sea water was found about 30 ng/ml.

A Study on Wisdom Management through Theoretical Research and Empirical Analysis (이론연구 및 실증분석을 통한 지혜경영)

  • Oh, Sang-Young
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.9 no.2
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    • pp.508-514
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    • 2008
  • Knowledge management has been spread rapidly since Knowledge is regarded as a crucial asset in future. Once, Knowledge had been obtained freely but hard to be shared. Studies on importance and share of knowledge have been taking place and it leads to development of knowledge management systems. However, decision makers still have problems even though they are using knowledge management systems. Eventually, for the decision makers are needed concentrated knowledge which is unconscious and embodied, when they make a decision. This is wisdom. Thus, wisdom is superior to knowledge for the decision makers. There are some researches on wisdom but wisdom management were overlooked. This study presents differences between knowledge and wisdom with theoretical research and empirical analysis on the wisdom management.

Creep Behaviour of Solution Treated Alpha Titanium Alloy for Automotive Parts (자동차부품 소재개발을 위한 알파 티타늄 합금의 용체화 처리후 정적 크리프 거동)

  • Hwang Kyungchoong;Yoon Jongho
    • Transactions of the Korean Society of Automotive Engineers
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    • v.13 no.1
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    • pp.153-158
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    • 2005
  • Titanium alloy has widely been used as material for automotive parts because it has high specific strength. It is also light and harmless to human body. But, we have little design data about the creep behaviors of the alloy. Therefore, in this study, creep tests under four constant stress conditions have been conducted with low different temperature conditions. A series of creep tests had been performed to get the basic design data and life prediction of titanium products and we have gotten the fallowing results. First, the stress exponents decrease as the test temperatures increased. Secondly, the creep activation energy gradually decrease as the stresses became bigger. Thirdly, the constant of Larson-Miller parameter on this alloy was estimated as about 7.5. And for the last, the fractographs at the creep rupture showed the ductile fracture due to the intergranullar rupture.

Analysis of Cyclofenil and its Metabolites in Human Urine using GC/MS (GC/MS를 이용한 소변중의 Cyclofenil 및 그 대사체의 분석)

  • Myung, Seung-Woon;Min, Hye-Ki;Cho, Hyun-Woo;Kim, Dong-Hyun;Kim, Myungsoo
    • Analytical Science and Technology
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    • v.15 no.3
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    • pp.185-189
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    • 2002
  • International Olympic Committee (IOC) prohibits the use of cyclofenil for male. To prove whether cyclofenil product was taken or not, the analytical method in urine using GC/MS was established. The extraction recoveries of cyclofenil and its metabolites were higher in the range of pH 5-9. Because the parent drug (cyclofenil) was not excreted in urine, metabolites were detected and theses were used as a criteria of cyclofenil dose. Therefore the metabolites were hydrolyzed, extracted at pH 9.6, derivatized with MSTFA and analyzed by GC/MS.