• Title/Summary/Keyword: 저온충격성

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A Study on the Activity of Metal Filter Pt Coated on Soot Oxidation (백금 코팅 메탈필터소재의 Soot 산화반응에 대한 활성 연구)

  • Kim, Sung Su;Lee, Sang Moon;Jang, Du Hun;Bae, Se Hyun;Hong, Sung Chang
    • Applied Chemistry for Engineering
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    • v.22 no.4
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    • pp.400-404
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    • 2011
  • The activity and stability of the metal filter material Pt coated on NOx and soot oxidation were examined. The catalytic reaction test for NOx and soot were also performed independently and simultaneously. As a result, it showed the NO to $NO_2$ shift reaction with 20% conversion, NOx decomposition (about 10%) and perfect soot oxidation on the material Pt coated proceeded. Onset temperature of soot oxidation shift to lower temperature (about $30^{\circ}C$) by generated $NO_2$. The material also was less affected by thermal shock than $Pt/Al_2O_3$ or $Pt/TiO_3$ catalysts due to its stability of surface structure.

Study on microstructure and mechanical properties of friction stir welded 9% Ni steel (마찰교반접합된 9% Ni 강의 미세조직 및 기계적 특성에 관한 연구)

  • Choi, Don-Hyun;Ahn, Byung-Wook;Choi, Jung-Hyun;Lee, Chang-Yong;Yeon, Yun-Mo;Song, Keun;Lee, Jong-Seop;Jung, Seung-Boo
    • Proceedings of the KWS Conference
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    • 2009.11a
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    • pp.49-49
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    • 2009
  • 마찰교반접합법은 특정한 회전수로 회전하는 용접 툴을 이용하여 접합하고자 하는 피접합재의 맞댄면에 삽입시킨 후 툴을 이동시키거나 혹은 시편을 견고하게 고정시킨 장치(backing plate)가 움직여 고상 상태에서 접합이 이루어진다. 알루미늄, 마그네슘 등 비교적 융점이 낮은 저융점 재료의 재료에 처음 적용이 되어 많은 연구가 활발히 진행되었고 타 용접방법에 비해 우수한 접합특성을 나타내었다. 최근 이러한 마찰교반접합은 이러한 저융점 재료를 넘어서 스틸, 타이타늄, 니켈 등과 같은 고융점 재료 등에 대한 적용이 늘어나고 있다. 마찰교반접합을 이용하여 이러한 고융점 재료의 접합 경우 내마모성 및 내열성 등의 내구성이 갖추어진 툴과 이러한 툴을 냉각시킬 수 있는 냉각 장치 등이 필요로 하나 경제적 측면이나 접합부의 우수한 특성 등을 고려 할 때 그 적용 및 발전 가능성이 매우 높다고 볼 수 있다. 최근 무공해 연료로 각광받고 있는 액화천연가스 (LNG)의 수요가 급증함에 따라 LNG 저장탱크 소재로 널리 사용되고 있는 9% Ni강의 수요 또한 증가하고 있는 상황이다. 하지만 9% Ni 강은 극저온용 소재로 용접부의 저온인성 ($-196^{\circ}C$)이 가장 중요하기 때문에 저온인성을 확보하고자 Inconel 계나 Hastelloy계 등의 니켈 기 합금을 용접재료로 사용하고 있으나 이러한 용접재료는 가격이 매우 고가이며 또한 용접 후 용접부의 강도가 낮다는 문제가 제기되고 있다. 또한 LNG 탱크 제작시 사용되는 용접법은 GTAW, SAW 및 SMAW 이지만 국내에서는 주로 SMAW에 의존하고 있는 실정인 관계로 보다 더 경제적인 용접 프로세스의 적용 가능성이 검토되고 있는 상황이다. 본 연구에서는 마찰교반용접을 이용하여 두께 4mm의 9% Ni 강에 대해 맞대기 마찰교반접합을 실시하였다. 툴 회전 속도 및 접합 속도를 고정한 상태에서 접합을 실시 하였으며 접합 시 툴은 $Si_3N_4$로 제작된 툴을 사용하였다. 접합 후 외관상태 점검, 미세조직 관찰, 경도, 인장 강도 및 저은 충격 측정 등의 실험을 실시하였고, 이러한 결과를 이용하여 미세조직과 기계적 특성과의 관련성을 조사하였다.

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Experimental Study on Fretting Wear of Inconel 690 Under High Temperatures and Pressures (고온 고압 환경에서 인코넬 690 재료의 프레팅 마모 특성에 관한 실험적 연구)

  • Lee, Coon-Yeol;Lee, Ju-Suck;Bae, Joon-Woo
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.36 no.6
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    • pp.637-644
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    • 2012
  • In a nuclear power plant, fretting wear due to impact motion between U-tubes and support structures located in steam generators can cause serious problems. In order to guarantee the reliability of the steam generator, the damage due to fretting wear should be thoroughly investigated. The purpose of this study is to elucidate the fretting wear mechanism qualitatively and quantitatively. Hence, fretting wear simulation is performed for the environments to which the actual steam generators in nuclear power plants are exposed. Initial experimental results are obtained for various experimental parameters, and the effect of the work rate and temperature on fretting wear is evaluated. In water, the wear coefficients for $90^{\circ}C$, $200^{\circ}C$, and $340^{\circ}C$ are found to be $9.051{\times}10^{-16}\;Pa^{-1}$, $3.009{\times}10^{-15}\;Pa^{-1}$, and $2.235{\times}10^{-15}\;Pa^{-1}$, respectively. It is also found that the wear coefficient at room temperature is larger than that at low temperature in water because of the dynamic viscosity of water.

High functional biodegradable card through annealing (어닐링을 통한 고기능성 생분해성 카드)

  • Sim, Jae-Ho
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.21 no.2
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    • pp.280-286
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    • 2020
  • Cards made from PVC and PET materials do not oxidize or decompose readily, so they are generally incinerated or landfilled after use and cause pollution problems, such as environmental hormones and combustion gases during incineration. In addition, there is a problem of environmental pollution because they are discarded as semi-permanent refuse without being decomposed at landfill. This study attempted to solve this problem using polylactic acid (PLA), which is a representative biodegradable material as a substitute material that can solve the issues with these cards. On the other hand, when the thin card core sheet is made from only PLA material, the physical properties of the material are insufficient, such as the low temperature impact strength, high temperature stability, and poor bending properties, so its use is limited. To solve this problem, the compositional ratio of PLA was reviewed, and the optimal biodegradable compound composition was determined through an examination of the compositions, such as crystallization nucleating agents, additives, and nano compound technology. The high functionalization as a biodegradable card was verified through a laminating process using annealing technology.

Electroporation Conditions for DNA Transfer into Somatic Embryogenic Cells of Zoysia japonica (들잔디 체세포 배발생 세포로의 DNA 전입을 위한 Electroporation 조건 구명)

  • 박건환;안병준
    • Korean Journal of Plant Tissue Culture
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    • v.25 no.1
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    • pp.13-19
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    • 1998
  • We have reported previously that intact embryogenic cells can be used instead of protoplasts for electroporation-mediated transformation of zoysiagrass and rice. In this study, conditions of the tissue electroporation were examined to optimize the procedures. Embryogenic cell suspensions were established in liquid MS medium containing 2 mg/L of 2,4-D with embryogenic calluses induced from mature embryos of Z. japonica. The suspension-cultured cell clumps were electroporated with 35S-gusA expression vector DNA, and degrees of DNA introduction into the cells were determined by histological expression rates of the gusA marker gene. DNA transfer into the cell clumps occurred in wide range of voltage (100-400 V) and capacitance (10-1980 $\mu\textrm{F}$), but more in the ranges of 200-300 V and 330-800 $\mu\textrm{F}$ DNA concentrations higher than 6 $\mu\textrm{g}$/mL were adequate for GUS expression of the electroporated cells. DNA transfers were confirmed in all three embryogenic cell lines but only in one out of eleven non-embryogenic lines. Positive GUS expressions occurred with DNAs added even 20-40 h after pulse treatments. As a promoter of gusA, Act1 and Ubi1 were effective 7 and 5 times than 35S respectively in number of GUS expression units on electroporated cell clumps. Embryogenic cell clumps survived and regenerated into plantlets after pulse treatments of wide range of conditions.

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A Study on Properties of Pb-free Solder Joints Combined Sn-Bi-Ag with Sn-Ag-Cu by Conditions of Reflow Soldering Processes (리플로우 솔더링 공정 조건에 따른 Sn-Bi-Ag와 Sn-Ag-Cu 복합 무연 솔더 접합부 특성 연구)

  • Kim, Jahyeon;Cheon, Gyeongyeong;Kim, Dongjin;Park, Young-Bae;Ko, Yong-Ho
    • Journal of the Microelectronics and Packaging Society
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    • v.29 no.3
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    • pp.55-61
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    • 2022
  • In this study, properties of Pb-free solder joints which were combined using Sn-3.0Ag-0.5Cu (SAC305) Pb-free solder with a mid-temperature type of melting temperature and Sn-57Bi-1Ag Pb-free solder with a low-temperature type of melting temperature were reported. Combined Pb-free solder joints were formed by reflow soldering processes with ball grid array (BGA) packages which have SAC305 solder balls and flame retardant-4 (FR-4) printed circuit boards (PCBs) which printed Sn-57Bi-1Ag solder paste. The reflow soldering processes were performed with two types of temperature profiles and interfacial properties of combined Pb-free solder joints such as interfacial reactions, formations of intermetallic compounds (IMCs), diffusion mechanisms of Bi, and so on were analyzed with the reflow process conditions. In order to compare reliability characteristics of combined Pb-free solder joints, we also conducted thermal shock test and analyzed changes of mechanical properties for joints from a shear test during the thermal shock test.

Cultivation of cauliflower mushroom (Sparassis crispa) by use of coniferous sawdust-based media with wheat flour and molasses (소맥분과 물엿을 첨가한 침엽수 톱밥배지에서의 꽃송이버섯 생산)

  • Oh, Deuk-Sil;Park, Hyun;Park, Hwa-Sik;Kim, Myong-Seok;Chai, Jung-Ki
    • Journal of Mushroom
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    • v.4 no.1
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    • pp.39-42
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    • 2006
  • Cauliflower mushroom(Sparassis crispa) contains much amount of ${\beta}$-glucan, which make lots of farmer want to cultivate the mushroom. Since a practical cultivation method is not provided yet, the mushroom is considered as a difficult crop to deal with. In this study, we tried to develope a simple method to cultivate the mushroom by use of coniferous sawdust-based medium with wheat flour and molasses. There was no significant differences between the sawdust spawn and the liquid spawn for the mycelial growth of the mushroom. The cold shock in $4^{\circ}C$ for a day was thought to be the best way to seduce primordium formation. The sawdust medium of Pseudotsuga menziesii mixed with wheat flour, corn chip, cottonseed meal and 10% molasses was showed the best yield with 41% followed by that of Larix leptolepis mixed with the same additives with 37% of yield. There was good relations between the fruit-body production and the weight loss of the sawdust substrate.

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A study on the mechanical performance of impregnated polymer foam in cargo leakage of LNG carrier (LNG운반선의 화물 누출 시 함침된 고분자 폼의 기계적 성능에 관한 연구)

  • Park, Gi-Beom;Kim, Tae-Wook;Kim, Seul-Kee;Lee, Jae-Myung
    • Journal of Advanced Marine Engineering and Technology
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    • v.41 no.4
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    • pp.345-352
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    • 2017
  • In this study, the effect of cryogenic liquefied natural gas leakage and loading on liquefied natural gas cargo hold is investigated to observe the performance of the polymer foam material that comprises the cryogenic insulation of the cargo hold. The primary barriers of liquefied natural gas carrier that are in contact with the liquefied natural gas will leak if damage is accumulated, owing to fluid impact loads or liquefied natural gas loading / unloading over a long period. The leakage of the cryogenic fluid affects the interior of the polymer foam, which is a porous closed cell structure, and causes a change in behavior with respect to the working load. In this study, mechanical properties of polyisocyanurate foam specimen, which is a polymer material used as insulation, are evaluated. The performance of the specimens, owing to the cold brittleness and the impregnation effects of the cryogenic fluids, are quantitatively compared and analyzed.

Performance of OLED devices with the surface characteristics of TCO thin films (투명전도성 박막의 표면 특성에 따른 OLED 소자의 특성)

  • Lee, Bong-Kun;Lee, Yu-Lim;Lee, Kyu-Mann
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2009.06a
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    • pp.313-313
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    • 2009
  • OLED 소자는 직접발광, 광시야각, 그리고 빠른 응답속도 때문에 동영상에 적합하여 최근 각광받고 있는 디스플레이장치 중의 하나이다. OLED 소자의 양극재료로는 높은 광투과율과 $\sim10^{-4}{\Omega}\;cm$ 수준의 낮은 전기 비저항을 갖는 ITO (Sn-doped $In_2O_3$)가 널리 사용되고 있다. 하지만 원료 물질인 인듐의 수급량 부족으로 인한 문제점과 독성, 저온증착의 어려움, 스퍼터링시 음이온 충격에 의한 막 손상으로 저항의 증가의 문제점이 있고, 또한 액정디스플레이의 투명전극으로 사용될 경우 $400\;^{\circ}C$정도의 높은 온도와 수소 플라즈마 분위기에서 장시간 노출 시 열화로 인한 광학적 특성변화가 문제가 된다. 반면에 Al이 도핑 된 ZnO (AZO)박막은 넓은 밴드갭 (3.37eV)와 400nm에서 700nm 사이의 가시광 영역에서 80% 이상의 우수한 투과성을 지니고 있다. 특히 Al이 도핑된 ZnO는 박막의 전기적 특성이 크게 향상되어 디스플레이나 태양전지로의 응용이 가능하다. 또한 비교적 낮은 비용과 플라즈마에서의 안정성, 무독성, 그리고 전기전도성과 같은 많은 이점이 있다. 그 결과 AZO 박막은 ITO기판을 대안하는 지원물질로 활발히 연구가 진행되고 있다. 본 연구에서는 TCO 박막의 면 저항과 표면 거칠기에 따른 OLED 소자의 특성을 분석하였다. ITO와 AZO 박막은 챔버 내 다양한 가스 분위기(Ar, Ar+$O_2$ and Ar+$H_2$)에서 R.F Magnetron Sputtering방법으로 증착하였다. TCO 박막의 구조적인 이해를 돕기 위해서 X-ray diffraction 과 FESEM으로 분석하였다. 광학적 투과도와 박막의 두께는 ultraviolet spectrophotometer (Varian, cary-500)와 surface profile measurement system으로 각각 측정하였다. 면저항 charge carrier 농도, 그리고 TCO 박막의 이동도와 같은 전기적특성은 four-point probe와 hall effect measurement(HMS-3000)로 각각 측정하였다. TCO 박막의 표면 거칠기 조절을 위해 photo lithography 공정을 사용하여 TCO 박막을 화학에칭 하였다. 미세사이즈 패턴 마스크가 사용되었으며 에칭의 깊이는 에칭시간에 따라 조절하였다. TCO 박막의 표면 형태는 FESEM과 AFM으로 관찰하였다. 투명전극으로 사용되는 ITO 및 AZO 기판 상용화를 위해 ITO 및 AZO 기판 위에 ${\alpha}$-NPB, Alq3, LiF, Al 의 순서로 증착 및 패터닝함으로써 OLED 소자를 제작하였다. 전류밀도와 전압 그리고 발광휘도와 전압과 같은 전기적 특성은 spectrometer(minolta CS-1000A)를 이용하여 측정하였다.

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A Study on Partially Applied Color Image in Black and White Moving Imagery (흑백영상의 부분 색채화에 관한 연구)

  • Yeo, Myoung;Kim, Ji-Hong
    • Proceedings of the Korea Contents Association Conference
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    • 2006.11a
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    • pp.322-326
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    • 2006
  • Though human being has ability to percept a full colored vision, the technology of early photography only can produce black and white images. For cinema filming imagery also captured mono tone with black and white, until developed a color film technology. The desire for presenting color imagery and the technique for producing film and color ink, photography and print utilize color on it with noticeable color impact to viewers. It, however, abusing fun colors image each and every printed and filmed imagery, the freshness of eye catching power diminished now. On contrast, color becomes black and white or partially used for making discrepancy among full colored images. This image detected commercial and music video, and it spread to film. To use those bleached color images is for evoking a nostalgia and a visual differentiation. Especially, it can be provocative images brought to audience with that. such as "Anycall", "Dimchae" for CF, and "Schindler's list," and "Sin city" for movie. It is hard to investigate on the color studies for partially used images. Therefore, this study is to research that through CF and film, base on it, to investigate the application for this image. To collect data from survey, it will be established a basic concept for understanding the partial color applying.

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