• Polymer(Korea)
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• 제39권3호
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• pp.370-381
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• 2015

In the system of poly(vinyl alcohol) (PVA)/dimethyl sulfoxide, the refractive index of polymer was very well matched to that of solvent and thus its scattered intensity could be minimized. After adding small amount of polystyrene latex particle (nominal diameter 200 nm), diffusion behavior of only probe particle was investigated against the concentration of polymer matrix by means of dynamic light scattering. The polymer concentration dependence of its reduced diffusion coefficient was able to be analysed with the stretched exponential function of the reduced concentration $C[{\eta}]$. In very dilute concentration regime, the depletion layer kept constant but at the early semi-dilute regime of $1{\leq}C[{\eta}]{\leq}2.5$, the concentration-dependent exponent of depletion layer ${\delta}$ was appeared to be -0.8 which was very close to theoretical one of -0.85. However it was also observed at the higher concentration that its layer thickness decreased more abruptly than theoretical expectation and this phenomenon was ascribed to Oosawa type attractive interaction between adjacent latex particles.

• Korean Journal of Agricultural Science
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• 제5권1호
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• pp.29-34
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• 1978

In order to improve atomization of droplet of sprayers, gun-type nozzle equipped with swirl screw which could increase tangential velocity had been used in this study. The results obtained were as follow: The larger diameter of atomized droplet was, the longer it reached. Tile atomizing phenomenon while using swirl screw in the nozzle was more efficient. There was little difference of travelling distance in the both nozzles when the small diameter of disk hole was used, but thetravlling distance of the nozzle with swirl screw was evidently getting shorter with the increase of the hole diameter compared to that of the nozzle without swirl sorew. The size of sprayed particles was getting smaller owing to the phenomenon of air movement the one to two meters travelling distance of droplet from maximum travelling point.

• Water for future
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• 제26권1호
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• pp.63-69
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• 1993

Remediation technology becomes an issue in environmental engineering. The vibro-recovery technique is one of popular means to remove pollutants from contaminated soils and groundwater. Using Ultrasonic excitation in soil-fluid medium, it was found that removal efficiency in a mechanical effects was significant. In this paper, therefore, laboratory experiments were conducted on clayey sand soil columns using a probe-type ultrasonic processor. Ultrasonic treatment with simultaneous pumping enhances dislodgement of clay particles, and ultrasonic excitation reduced the proportions of finer particles and thus result in increased hydraulic conductivity significantly. Also, the results provided the changes in grain size distribution curve of the soil due to ultrasonic excitation. The results indicated that the maximum size of particles mobilized by Ultrasonic is about 0.004mm and particles in the size range from 0.04mm to 1.0mm were subjected to fracturing. The economic feasibility of Ultrasonic implementation is considered in power requirement of the generator and maintenance of the horn. At a specified amplitude of vibrations, the power requirement of the generator depends on overburden pressure of the horn, temperature and viscosity of fluid in the soil medium. For comparisons, the requirement of a one inch and two inch diameter horn sonicators are compared with the power required for pumping water from different depths.

• Korean Journal of Food Science and Technology
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• 제31권1호
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• pp.257-259
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• 1999

A molding of roasted glutinous rice powder by pressurized steaming was investigated in terms of steaming pressure and powder size. Roasted glutinous rice powders of $80{\sim}115,\;115{\sim}170,\;170{\sim}250$, and 250

• Journal of Adhesion and Interface
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• 제3권4호
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• pp.19-26
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• 2002

In order to study the toughening mechanism of rubber modified polycarbonate, the sequence of development of micro-voids was investigated by real-time small angle X-ray scattering with Synchrotron radiation (SR-SAXS). The used test method was wedge test. The scattering intensity increases with increasing penetration depth of wedge, i.e. applied strain. The increase is due to the micro-void formation during deformation. This micro-void was uniformly developed in matrix and was different from large-void due to internal cavitation of rubber particle and/or debonding between rubber particle and polycarbonate matrix. The micro-void was developed at the critical strain and the radius of micro-void is around $600{\AA}$. Above the critical strain the size of micro-void remains almost constant with increasing applied strain. However, the population of micro-void increased with applied strain.

• Journal of the Microelectronics and Packaging Society
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• 제25권4호
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• pp.155-161
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• 2018

A Si chip with the Cu/Au bumps of $100-{\mu}m$ diameter was flip-chip bonded using different anisotropic conductive adhesives (ACAs) onto the local stiffness-variant stretchable substrate consisting of polydimethylsiloxane (PDMS) and flexible printed circuit board (FPCB). The average contact resistances of the flip-chip joints processed with ACAs containing different conductive particles were evaluated and compared. The specimen, which was flip-chip bonded using the ACA with Au-coated polymer balls as conductive particles, exhibited a contact resistance of $43.2m{\Omega}$. The contact resistance of the Si chip, which was flip-chip processed with the ACA containing SnBi solder particles, was measured as $36.2m{\Omega}$, On the contrary, an electric open occurred for the sample bonded using the ACA with Ni particles, which was attributed to the formation of flip-chip joints without any entrapped Ni particles because of the least amount of Ni particles in the ACA.

• Journal of the Korean Society for Nondestructive Testing
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• 제26권2호
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• pp.69-76
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• 2006

TRISO(tri-isotropic)-coated fuel particle technology is utilized owing to its higher stability at a high temperature and Its efficient retention capability for fission products In the HTGR(high temperature gas-reeled reactor). The typical spherical TRISO fuel panicle with a diameter of about 1mm is composed of a nuclear fuel kernel and outer coating layers. The outer coating layers consist of a buffer PyC(pyrolytic carbon) layer, Inner PyC(1-PyC) layer, SiC layer, and outer PyC(O-PyC) layer Most of the Inspection Items for the TRTSO-coated fuel particle depend on destructive methods. The coating thickness of the TRISO fuel particle can be nondestructively measured by the X-ray radiography without generating radioactive wastel. In this study, the coaling thickness for the simulated TRISO-coated fuel particle with $ZrO_2$ kernel Instead of $%UO_2$ kernel was measured by using micro-focus X-ray radiography with micro-focus X-ray generator and flat panel detector The radiographic image was also enhanced by image processing technique to acquire clear boundary lines between coating layers. The coaling thickness wat effectively measured by applying the micro-focus X-ray radiography The inspection process for the TRISO-coated fuel particles will be improved by the developed micro-focus X-ray radiography and digital image processing technology.

• Proceedings of the Korean Vacuum Society Conference
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• 한국진공학회 1999년도 제17회 학술발표회 논문개요집
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• pp.214-214
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• 1999

다이아몬드를 반도체용 열방산용기판 등으로 사용하기 위해서는 수백 $\mu\textrm{m}$ 두께의 대면적 웨이퍼가 요구된다. 이를 위해서 DC are jet CVD, MW PACVD, DC PACVD 등이 개발되어, 현재 4"에서 8"까지의 많은 문제를 일으키고 있다. 본 연구에서는 multi-cathode DC PACVD법에 의한 4" 다이아몬드 웨이퍼의 합성과 합성된 막의 특성변화에 대한 연구를 수행하였다. 또한, 웨이퍼의 휨과 crack 발생거동과 대한 고찰을 통래 휨과 crack이 없는 웨이퍼의 제작방법을 고안하였다. 사용된 음극의 수는 일곱 개이며, 투입된 power는 각 음극 당 약 2.5kW(4.1 A-600V)이었다. 사용된 기판의 크기는 직경 4"이었다. 합성압력은 100Torr, 가스유량은 150sccm, 증착온도는 125$0^{\circ}C$~131$0^{\circ}C$, 수소가스네 메탄조성은 5%~8%이었다. 합성 중 막에 인가되는 응력은 합성 중 증착온도의 변화에 의해 제어하였다. 막의 결정도는 Raman spectroscopy 및 열전도도를 측정을 통해 분석하였다. 성장속도 및 다이아몬드 peak의 반가폭은 메탄조성 증가(5%~8%)에 따라 증가하여 각각 6.6~10.5$\mu\textrm{m}$/h 및 3.8~5.2 cm-1의 분포를 보였다. 6%CH4 및 7%CH4에서 합성된 웨이퍼에서 측정된 막의 열전도도는 11W/cmK~13W/cmK 정도로 높게 나타났다. 막두께의 uniformity는 최대 3.5%로 매우 균일하였다. 막에 인가되는 응력의 제어로 직경 4"k 합성면적에서 두께 1mm 이상의 균열 및 휨이 없는 다이아몬드 자유막 웨이퍼를 합성할 수 있었다.다이아몬드 자유막 웨이퍼를 합성할 수 있었다.active ion에 의해 sputtering 이 된다. 이때 plasma 처리기의 polymer 기판 후면에 magnet를 설치하여 높은 ionization을 발생시켜 처리 효과를 한층 높여 주었다. 이 plasma 처리는 표면 청정화, 표면 etching 이 동시에 행하는 것과 함께 장시간 처리에 의해 표면에서는 미세한 과, C=C기, -C-O-의 극성기의 도입에 의한 표면 개량이 된다는 것을 관찰할 수 있다. OPP polymer 표면을 Ar 100%로 plasma 처리한 경우 C-O, C=O 등의 carbonyl가 발생됨을 알 수 있었다. C-O, C=O 등의 carbynyl polor group이 도입됨에 따라 sputter된 Al의 접착력이 향상됨을 알 수 있으며, TEM 관찰 결과 grain size도 상당히 작아짐을 알 수 있었다.onte-Carlo 방법으로 처리하였다. 정지기장해석의 경우 상용 S/W인 Vector Fields를 사용하였다. 이를 통해 sputter 내 플라즈마 특성, target으로 입사하는 이온에너지 및 각 분포, 이들이 target erosion 형상에 미치는 영향을 살펴보았다. 또한 이들 결과로부터 간단한 sputtering 모델을 사용하여 target으로부터 sputter된 입자들이 substrate에 부착되는 현상을 Monte-Carlo 방법으로 추적하여 성막특성도 살펴보았다.다.다양한 기능을 가진 신소재 제조에 있다. 또한 경제적인 측면에서도 고부가 가치의 제품 개발에 따른 새로운 수요 창출과 수익률 향상, 기존의 기능성 안료를 나노(nano)화하여 나노 입자를 제조, 기존의 기능성 안료에 대한 비용 절감 효과등을 유도 할 수 있다. 역시 기술적인 측면에서도 특수소재 개발에 있어 최적의 나노 입자 제어기술 개발 및 나노입자를 기능성 소재로 사용하여 새로운 제품의 제조와 고압 기상

• Korean Chemical Engineering Research
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• 제55권5호
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• pp.646-651
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• 2017

Size and shape of carbon nanotube (CNT) agglomerates in the dilute phase of a bubbling fluidized bed ($0.15m\;i.d{\times}2.6m\;high$) have been determined by the laser sheet technique. Axial solid holdup distribution of the CNT particles showed S curve with dense phase and dilute phase in bubbling fluidization regime. Heywood diameter and Feret diameter of the CNT agglomerates in the dilute phase of bubbling fluidized bed increased with increasing gas velocity. The CNT particle number in the agglomerates increased with increasing of gas velocity. Aspect ratio increased and circularity, roundness and solidity decreased with increasing of gas velocity. A possible mechanism of agglomerates formation was proposed based on the obtained information.

• Transactions of the Korean Society of Mechanical Engineers B
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• 제38권1호
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• pp.17-24
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• 2014

We measured black carbon concentration in rural area to understand the characteristic of atmospheric aerosol by comparing the black carbon concentration and meteorological factors such as PM10 concentration, relative humidity, temperature and wind velocity. A MAAP (Multi Angle Absorption Photometer) which is one of filter based equipments was used to measure black carbon concentration. Black carbon concentration was measured to be high from April to May and low from June to September. Black carbon concentration was proportional to PM10 concentration. Black carbon concentration was correlated to relative humidity. Black carbon concentration was inversely proportional to wind velocity and temperature. Finally, we suggest that the volume fraction of black carbon in the atmosphere can be estimated from the size, number concentration and absorption coefficient measured using the MAAP.