• Journal of the Korea Concrete Institute
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• v.29 no.4
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• pp.361-369
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• 2017

Setting time of cement-based materials can represent a developing strength in early-age mixture, and it can be used a significant parameter of high-performance concrete having various mix-proportions. Generally, initial and final setting time of concrete is measured by penetration resistance method that used a wet-sieving mortar mixture, therefore, it hardly represents the setting time of sound concrete including coarse aggregate. Recently, several nondestructive methods, such as ultrasonic velocity and impendence measurement, are proposed to evaluate the setting time of fresh concrete. This study attempts to measure an electrical resistivity using four-electrode method for evaluation of setting time in early-age cement-based materials. For this purpose, total 10 mixtures are prepared as different mix-proportions including chemical admixture. Based on the experimental results, two electrical parameters, such as initial electrical resistivity and rising time, are proposed to reflect a microstructure development by hydration of cement-based materials. As a result, proposed parameter is also discussed with the measured setting time by penetration resistance method.

• Journal of the Korea Concrete Institute
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• v.17 no.6 s.90
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• pp.879-884
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• 2005

The setting time is a very important factor affecting the quality of tunnel lining and reinforcement of inclined slope etc. Currently, however, the quality criteria of accelerating admixture to improve it is not established well. In this study, evaluation on setting time measuring methods of cement mixed a accelerating admixture (AA) was performed using Gillmore and Vicat needle test methods. For both test methods, the setting time for addition at a time was better than post addition regardless of initial setting and final setting. For Gillmore needle test method, two types of measuring methods were selected and it is noted that setting time with cement type under the same accelerating admixture can be different. Accordingly, manufacturing company shall develop a less sensitive accelerating admixture to cement type. For Vicat needle test method, six types of measuring methods were used and a proper measuring method of the admixture were proposed as follows: (1) the temperature of materials used shall be controlled exactly and (2) to evaluate its properties, an admixture usage of $5\%$ (ratio of cement weight) is recommended.

• Journal of the Korea institute for structural maintenance and inspection
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• v.22 no.6
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• pp.9-15
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• 2018

According to the development and use of self-consolidating concrete in field, interest in material properties of early-age concrete is rising. Setting time with hydration process of cement is one of significant indicator to evaluate the early-age material properties of concrete, various nondestructive methods including penetration resistance measurement have been proposed to estimate setting time. This study performed an experimental approach to evaluate setting time delay in mortar adding superplasticizer using electrical resistivity measurement. For this purpose, total nine types of mortar samples were prepared, and its electrical resistivity was monitoring during 24h after mixing. From the experimental result, rising time of electrical resistivity was used to evaluate setting delay of mortar, and penetration resistance was also measured for comparison. In addition, dynamic elastic modulus and compressive strength of 1day mortar were measured to investigate a possibility the use of electrical resistivity measurement for evaluation of early-age material properties.

• Journal of the Korean Recycled Construction Resources Institute
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• v.12 no.2
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• pp.162-168
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• 2024

This study investigated the setting characteristics of cement paste with varying proportions of fly ash replacement using the electro-mechanical impedance (EMI) sensing technique. Cement paste samples were prepared with a water-to-binder ratio of 40 %, substituting fly ash for 10 %, 20 %, and 30 % of the cement weight. Piezoelectric (PZT) sensors were embedded in the center of each cement paste sample to continuously monitor the EMI signals. Vicat needle test and semi-adiabatic calorimetry test were conducted to validate the reliability of the EMI sensing technique in monitoring the setting of cement paste. Experimental results revealed notable changes in the magnitude and resonant frequency of the EMI resonant peaks during the setting time. It was confirmed that the setting times measured through the EMI sensing technique were correlated with those determined by the Vicat needle test and semi-adiabatic calorimetry test.

• Journal of the Korea institute for structural maintenance and inspection
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• v.26 no.4
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• pp.48-56
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• 2022

Controlling the setting time of cementitious materials is one of the most important factors in securing early-age performance of concrete structures. Recently, the use of retarding admixtures, which enable the inhibition of some hydration products to control the securing time due to average temperature rise is suggested. Although various non-destructive evaluation methods have been proposed to evaluate cement hydration and hardening of cement-based materials to overcome the limitations of Vicat needle test, experimental research is still required to use the non-destructive evaluation method with added retarding admixtures. In this study, measurements of electrical resistivity and ultrasonic wave velocity in early-aged cement pastes were performed according to the addition of retarding admixture(tartaric acid). The setting time of the cement pastes was evaluated by obtained rising time of the both non-destructive measurements. As a result, the possibility of evaluating the setting delay in cement pastes was confirmed through comparative analysis with the initial and final setting times by Vicat test. In addition, X-ray diffraction results at the rising time of electrical resistivity showed a key hydration product affecting the setting delay.

• Journal of the Korean Recycled Construction Resources Institute
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• v.5 no.4
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• pp.474-480
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• 2017

In this study, the evolution of electrical impedance of electric nodes was investigated to determine the setting time of cement paste using the electrical impedance spectroscopy method. The electric nodes were embedded in fresh cement paste and the electrical impedance signatures were continuously monitored. Vicat needle test and semi-adiabatic calorimetry test were also conducted to validate the electrical impedance spectroscopy method. During hydration period of cement paste, the magnitude of conductance gradually increased, and then started to decrease rapidly at a first certain time. After that, the magnitude of conductance gradually decreased at a second certain time. The times of turning point in the curves of magnitude of conductance seem to be related with the setting time by Vicat needle test. Also, the setting times by the electrical impedance spectroscopy method are well posed within the setting period estimated by the semi-adiabatic calorimetry test. Based on the results, it can be concluded that the setting time of cement paste can be effectively monitored through the electrical impedance spectroscopy method.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2022.11a
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• pp.65-66
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• 2022

In this study, the setting characteristics of the high range water reducing agent to minimize the retardation of UHPC were confirmed to minimize the setting time in the hardening of UHPC. As a result of the study, there was a slight change depending on the difference in the type of Superplasticizer, K > P > D = S > E in the order of condensation promotion, and E > S = D = K > P on the 28th day.

• Journal of the Korean Society for Nondestructive Testing
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• v.22 no.3
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• pp.292-303
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• 2002

This paper presents experimental results for early-age properties of concrete such as the setting time and strength, evaluated via the ultrasonic pulse velocity (UPV). Developing and using an automatically-recording monitoring system, the UPV's of mortar and concrete with various water to binder ratios (W/B) were measured during the first 24 hours. In addition, probe penetration and compression tests were conducted to measure the setting time and compressive strength, respectively. It was observed that the UPV's of mortar with high W/B remained constant during the first 6.5 hours and then abruptly began to increase at constant rates. On the other hand, the UPV of mortar with low W/B increased relatively slowly and gradually due to the setting retardation caused by the use of high range water reducing agent (HRWR). It was found that setting of concrete occurs when the UPV reaches a certain value. Moreover, it was concluded that the estimation formulas should incorporate the effects of W/B to more accurately estimate the early-age strength of concrete from the UPV.

• Journal of the Korean Recycled Construction Resources Institute
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• v.7 no.4
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• pp.358-366
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• 2019

The purpose of this study is to explore the possibility of estimating optimum surface finishing work time of the fresh concrete placed at the job site by applying a surface hardness test meter(Durometer). Tests are carried out by measuring and comparing the Proctor penetration resistance test and hardness test by Durometer. Correlations between Procter penetration test and hardness test by Durometer were obtained. Two different types Durometer were applied to estimate setting time. Test results indicate that the measurement of the Durometer and the test of the Proctor penetration resistance are highly correlated. When measuring the initial setting time with Durometer, initial setting time is reached when the hardness value by the type C Durometer is reached around 42HD, and when final setting is measured with the type D Durometer, the surface finishing work time limit and curing time can be estimated with 10HD of Durometer.

• Journal of the Korea Concrete Institute
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• v.29 no.1
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• pp.85-92
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• 2017

This study examines the characteristics of mortar mixed with various boron compounds. The adapted boron compounds, classified into acid, slightly alkaline and strongly alkaline with respect to the value of the pH are acid-based boron (AA), low-alkaline-based boron (AB), and high-alkaline-based boron (HB). The pH test, setting test and compressive strength test are performed to evaluate the physical and chemical properties of mortar, and SEM imaging is conducted to analyze the microstructure of mortar. The measured pH shows that the specimens mixed with boron compounds have lower pH than the basic mortar without boron and that loss of pH occurs according to time. The setting test reveals that the initial and final setting times of the specimens mixed with boron compounds occur later than the basic mortar, which disagrees slightly with the previous literature stating that the setting time can be shortened according to the alkalinity. From the compressive strength test and SEM imaging results, it is recommended to determine the optimal content of boron considering type and composition of the boron compounds.