• Title/Summary/Keyword: 유약

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Application of Zn2TiO4 for nucleation and control of willemite crystalline glaze (아연결정유약의 결정 생성 및 제어를 위한 Zn2TiO4 활용 연구)

  • Lee, Hyun-Soo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.27 no.4
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    • pp.154-161
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    • 2017
  • $Zn_2TiO_4$, which is a progenitor of zinc crystallization, plays a significant role in controlling the crystallization of willemite ($Zn_2SiO_4$) in forming glaze at low temperatures. Thus, $Zn_2TiO_4$ was used to formulate stable willemite and to gain structural control. When synthesized 15 wt% of $Zn_2TiO_4$ is added to engobe and then applied, it can manipulate its crystallization and location. Additionally, when colorant is added to $Zn_2TiO_4$ and then applied to engobe, the mixture's colorant effect can be shown at crystallization. Certain characteristics of synthesized $Zn_2TiO_4$ enable various engobes to be applied to clay bodies. With a single glazing, the crystallization, location, and color of the crystals can be discretionarily regulated.

Effects of Juvenile Hormone and Molting Hormone on Diapausing Adults of the Alder Leaf Beetle, Agelastica coerulea Baly (휴면중인 오리나무잎벌레 (Agelastica coerulea Baly) 성충에 미치는 유약호르몬과 탈피호르몬의 영향)

  • 최진우;부경생
    • Korean journal of applied entomology
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    • v.30 no.4
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    • pp.258-264
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    • 1991
  • Studies were carried out to investigate effects of temperature and photoperiod on diapause induction and of juvenile hormone III and 20-hydroxyecdysone treatment on diapausing adults of the alder leaf beetle, Agelastica coerulea Baly(Chrγsomelidae: Coleoptera). Its life cycle and ovarian development in adults were also observed. The beetle had one year life cycle with egg, larval, pupal and adult periods being 7-10, 19-21, 14-15 days and about 10 months, r respectively. All adults showed a diapause syndrome when the larvae were reared at $20^{\circ}C$ or $25^{\circ}C$ in combination of photoperiods of 16L/8D, 12L/12D, or 8L/16D. Their ovarioles did not s show any development of vitellogenesis before or during diapause and even when exposed at $15^{\circ}C$ after overwintering. When diapausing adults were treated with JH III they resumed feeding and laid several eggs and broke diapause condition temporally. But diapausing adults treated with 20-hydroxyecdysone did not show any response.

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Compositional and Microstructural Study of Punchong from Hakbongni, Kongju (공주 학봉리 분청에 대한 성분과 미세구조의 분석)

  • Lee, Young Eun;Koh, Kyongshin
    • Journal of Conservation Science
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    • v.6 no.1 s.7
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    • pp.3-14
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    • 1997
  • Twelve Punchong sherds collected in Hakbongni, Kongju where the well known iron-painted on white slip were manufactured from late 15C to early 16C were analyzed for their composition and microstructure. The composition of the body was analyzed by X-ray fluorescence and that of glaze by electron probe micro-analyzer. Microstructure was observed by optical microscope, polarizing microscope, EPMA, and X-ray diffractometer. The results of composition of body and glaze of Hakbongni were compared with those of Punchong from Yongsuri, Boryong which was close to Hakbongni. The composition of body and glaze of these two areas were compared by principal component analysis using SPSS program. Hakbongni bodies have higher silica and flux materials but lower alumina and their glaze have higher silica, soda, iron oxide but lower alumina, calcia. Hakbongni punchong itself is divided into two groups. Their glaze is lime type. There are many remnant minerals, such as quartz, large feldspar mass with partially melted surrounding area, albite, biotite, and iron-oxide. From such a microstructure we can assume that preparation of raw material was rather crude and firing temperature quite low. Iron-painted material is identified as Mg/Fe/Al spinel by composition analysis and XRD pattern.

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Antigenic localities in the tissues of the young adult worm of Paragonimus westermani using immunogold labeling method (면역황금표식법을 이용한 폐흡충의 유약함충 조직내 항원성 부위에 관한 연구)

  • 권오성;이준상
    • Parasites, Hosts and Diseases
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    • v.29 no.1
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    • pp.31-42
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    • 1991
  • In order to observe the antigenic localization in the tissues of the young adult Paragenimus westermani, immunogold labeling method was applied using serum immunoglobulins (IgG) of the dog which infected with isolated metacercariae from Cambaroides similis. The sectioned worm tissue was embedded in Lowicryl HM 20 medium and stained with infected serum IgG and protein A gold complex(particle size; 12 nm) It was observed by electron microscopy at each tissues of the worm. The gold particles were not observed on the basal lamina of the tegument, interstitial matrix of the parenchyma, the muscle tissue and mitochondria of the tegument. The gold particles were specifically labeled in the secretory granules in the vitelline cells. They were predominantly labeling on the epithelial lamela and lumen of caecum. The above finding showed that antigenic materials in young adult worm tissue were specifically concentrated on the tegumental syncytium as well as cytoplasm of tegumental cells.

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Hydration Characteristics and Chemical Composition of Lead-glazed Paving Bricks Excavated from the Beopgwangsa Temple Site, Pohang (포항 법광사지 납유 전돌의 수화 양상과 화학조성)

  • Jeon Sangeun;Kim Gyuho
    • Conservation Science in Museum
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    • v.29
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    • pp.65-80
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    • 2023
  • This study investigated seven specimens of lead-glazed paving bricks in order to identify the materialistic characteristics of the lead glaze used for paving bricks during the late Unified Silla period in Korea. The samples were excavated from the Beopgwangsa Temple site, Pohang. As a result of observing the surface and cross-section of the glaze with a microscope, the study confirmed that the lead glaze demonstrates various traits of hydration, which were classified into four layers: Surface layer, hydration layer A, hydration layer B, and green layer. After measuring the composition of each layer with SEM-EDS analysis, the green layer was found to have been less affected by the external environment, which renders it highly reasonable to view the green layer as the original composition of the lead glaze. The green layer is a low-temperature glaze composed mainly of PbO and SiO2 at a ratio of 8:2, with approximately 2% CuO acting as the main colorant. Comparing the green layer composition with those from Gyeongsang-do, it was confirmed that the mixture ratio of lead glaze materials was similar to other sites such as the Sacheonwangsa Temple site, the Cheonryongsa Temple site, and the Buseoksa Temple site.

Purification and Characterization of a Juvenile Hormong Binding Protein from Whole Body Homogenates of the Wax Moth, Galleris mellonella Final Instar Larvae (꿀벌부채명나방 종령유충에서 유약호르몬 결합단백질의 정제와 특성)

  • 안기흥;전상학;이경로
    • Korean journal of applied entomology
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    • v.37 no.1
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    • pp.59-64
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    • 1998
  • A juvenile hormone binding protein (JHBP) has been isolated from the whole body homogenate of Galleria rnellonella final instar larvae by gel filtration. The isolated protein is homogenous as judged by column chromatography and gel electrophoresis in the presence and absence of denaturing agent. The JHBP has a relative molecular weight of 32 k by denaturing gel electrophresis and 28 k by gel filtration. The protein exhibits a dissociation constant of 3.9 x M for JH 111.

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The Effect of Micro Constituent Element on the Development of Unique Color of Koryo Celadon (고려 청자 유약 발색에 미량 성분이 미치는 영향)

  • 김형태;이세용;함청순;최의석
    • Journal of the Korean Ceramic Society
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    • v.38 no.6
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    • pp.522-530
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    • 2001
  • 발굴된 과거 고려청자의 화학성분조성과 물리적 특성에 대한 평가를 하고 미량성분의 청자의 발색에 미치는 영향을 고찰한 결과, 고려 청자 태토는 Fe$_2$O$_3$가 2%, TiO$_2$가 0.8% 함유되어 있었으며, 청자유는 석회.장석유로서 Fe$_2$O$_3$가 1.0~1.2%, TiO$_2$가 0.16% 포함되어 있었다. 비색청자의 경우 미량성분인 MnO$_2$가 P$_2$O$_{5}$의 함량이 0.37%와 0.76%, CuO는 300~500ppm 정도 함유하고 있었다. 반사율 측정 결과 일반적인 청자가 540~570nm의 장파장대에서의 반사율이 급격히 떨어지는데 반하여, 13세기 비색 청자의 것은 적색 파장대에서 10%이상 높았다. CoO는 미량 첨가로도 유약의 청색 파장대 반사율이 높고, 적색 파장대의 반사율이 급격히 떨어지며 청자 발색에 부정적인 영향을 미쳤다. CuO는 0.05%를 첨가했을 경우 적색 파장대에서 반사율 곡선이 높게 나타나고 있어 비색 청자발색에 효과적이었다. 또한 명도를 나타내는 L*값도 CuO가 첨가된 유약이 가장 높았고, 비색청자의 색상은 녹청자에 비해 맑고 깊은 색감을 보였다.

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Effect of Korean Earthenware Container (Onggi) on Preservation of Fresh Fruits and Vegetables (신선 과일과 채소의 보관에 사용된 옹기의 저장성 향상 효과)

  • Jeong, Mi-Jin;Kim, Nam-Yong;An, Duck-Soon;Lee, Dong-Sun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.16 no.2_3
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    • pp.35-42
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    • 2010
  • The effect of different containers on preservation of the fresh produces of banana, non-astringent persimmon, strawberry, cherry tomato and enoki mushroom was evaluated by storage test at controlled chilled temperature. Korean earthenware containers (onggi) glazed and/or unglazed were compared with plastic box and chinaware (or glass bottle). Glazed onggi was effective in preserving banana, persimmon and cherry tomato, while there was only marginal or little benefit with strawberry and enoki mushroom. The positive effect of glazed onggi on the freshness keeping for these ethylene-sensitive commodities is reasoned to come from adsorption of ethylene by the onggi, which needs to be tested by further study.

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Effects of Methoprene on Embryo Development in the Gypsy moth, Lymantria dispar (Methoprene이 짚시나방(Lymantria dispar)의 배자 발생에 미치는 영향)

  • 강정호;오세원;이경로
    • Korean journal of applied entomology
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    • v.32 no.4
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    • pp.450-456
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    • 1993
  • We investigated effects of a topical treatment of methoprene(0.5-5.0$\mul$/egg), a juvenLle horm mane analogue, on embryo development in the gypsy moth, Lymantri$\alpha$ dispar. Methoprene lowered egg hatching rate, and also reduced the mean wet weights of hatched 1st instar larvae w with the most effect shown at the highest concentration. The differences in protein(p < 0.01) and carbohydrate(p < 0.05) contents between control and methoprene(5$\mul$/ egg) treatment g groups were observed during embryo development.

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A Study of the Chemical Composition of Korean Traditional Ceramics (I): Celadon and Kory$\v{o}$ Whiteware (한국 전통 도자기의 화학 조성에 대한 연구 (I): 고려청자와 고려백자)

  • Koh, Kyong-Shin Carolyn;Choo, Woong-Kil;Ahn, Sang-Doo;Lee, Young-Eun;Kim, Gyu-Ho;Lee, Yeon-Sook
    • Journal of Conservation Science
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    • v.26 no.3
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    • pp.213-228
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    • 2010
  • The composition of Chinese ceramic shards has been the subject of analysis in Europe, beginning in the 18th century, and in China from the 1950s. Scientific studies of traditional Korean shards commenced in the United States and Germany in the 1980s, and studies within Korea began in the 1990s. From analysis of a large systematically collected dataset, the composition of porcelain produced during the Kory. dynasty, including 21 celadon and 10 whiteware groups, was characterized and compared with that of Chinese ceramics. The average composition of the body and glaze of several shards (usually three to five) from each group was determined, enabling comparisons between groups. The results show that the majority of groups were derived from mica-quartz porcelain stone, which was commonly used in Yuezhou, Jingdezhen, and other southern Chinese kilns. The composition of glazes includes clay and flux components; the latter were typically wood ash and limestone, initially as burnt but later as crushed forms. The earliest of the Kangjin glazes contained substantially less titanium oxide than did the Yuezhou glazes, which were typically formulated from body material and wood ash. The present study provides a comparative framework for the growing number of analytical investigations associated with excavations occurring in Korea.