• Analytical Science and Technology
• /
• v.12 no.2
• /
• pp.125-129
• /
• 1999

Portable-type two electrode system for the determination of highly concentrated hydrogen peroxide (10-75%) has been studied. The electrode body was made with teflon rod (length=10 cm, diameter=1.5 cm) to withstand the highly corrosive power of hydrogen peroxide. Glass carbon rod (diameter=3 mm) was used as the working electrode and a carbon cylinder (i.d.=5 mm; o.d.=9 mm) was used as counter electrode. The applied voltage for the determination of $H_2O_2$ was 0.8 V. Diluting the highly concentrated samples taken from the industrial batch to 10% or less, it was possible to make quantitative determinations, while eliminating the interference from the stabilizer contained in the sample and preventing the surface of the electrode from oxidative corrosion. Employing hydrogen peroxide permeable membrane (teflon membrane${\leq}100{\mu}m$) for the electrode system, it was possible to measure the content of $H_2O_2$ in highly concentrated samples directly, quantitatively and reproducibly with no extra dilution step. However, it was necessary to change the internal electrolyte frequently to maintain the analytical performance of the electrode.

• Journal of Chest Surgery
• /
• v.29 no.5
• /
• pp.510-516
• /
• 1996

Cardiopulmonary bypass cannulas are usually characterized by the French number. However this de- scription provides only the external diameter of the cannula, which gives no information about the press- ure-flow characteristics of the cannula itself. A standardized system to describe the pressure-flow characteristics of a given cannula has recently been proposed and has been termed the M-number It is reported that the pressure-flow characteristics of a particular cannula can be determined from a novo- gram or chart, if the experimentally derived M-number of the cannula is known. In this regard, we conducted an investigation to analyze correlation between experimentally and clinical y derived M-numbers using three different sizes of pediatric aortic cannulas in fifty cardiac patients on cardiopulmonary bypass. The clinical and experimental M-numbers showed a strong correlation. The clinical M-numbers were typically 0.)5 to 0.55 greater than the experimental M-numbers. The clinical M-numbers also showed an inverse relationship to the temperature change of the patient, most probably due to an increase in blood viscosity from hypothermia. This inverse clinical M-numbersltemperature re- lationship was more marked in higher M-number cannulas. The clinical data obtained in this study suggest that the experimentally derived M-numbers correlated strongly with the clinical performance of the cannula with the significant influence of the temperature.

• Korean Journal of Soil Science and Fertilizer
• /
• v.33 no.1
• /
• pp.15-23
• /
• 2000

RC oscillation method was applied to study the condenser characteristics of two metal sticks insulated by vinyl tube and used in the dielectric constant determinations of most soils. Its capacitance as influenced by the contacted ambient materials was measured as relative capacitance of the sensor sticks compared with the standard one on the RC oscillation circuit. According to the equivalent circuit of the sensor stick set, the measured capacitance was composed of a basic capacitance connected in parallel with sensor stick capacitance, which was composed of lineally connected vinyl tube capacitances and the sensing part capacitance. The dielectric constant (U) of the contacted ambient moist soil located in the sensing part around the sticks interrelated with the other parameters as following equation. $$\frac{1}{C-B}=\frac{k}{U}+Z$$ where C is the output total relative capacitance, B is the hidden and fixed basic relative capacitance, k is a constant related with U, and Z is a constant for the insulating vinyl tube capacitances determined by its thickness and dielectric constant. The constant k is determined by the spacing and length of sensor sticks. The Z value is theoretically an invariable constant, but it may become considerably bigger than the determined in lab if air tube is formed on the surface of sensor sticks by some shocks on them after their installation in soil. Due to the unstability of lab Z value, it may be better to revise it after sensor stick's installation in soil and no shaking shocks should be applied on them.

• Journal of the Korean Society for Nondestructive Testing
• /
• v.18 no.6
• /
• pp.455-463
• /
• 1998

RCCA(rod cluster control assembly) End-Tip suffers from neutron irradiation and constant vibration due to high-speed internal flow of primary coolant during plant operation. Such operating conditions cause the RCCA end-tip crackings around tile circumferential weldment of the end-tip, and in some cases, the defective end-tips were completly broken loose. However, no reliable inspection techniques for end-tip crackings were developed in the past, although some techniques exist for inspecting RCCA control rod wears. Therefore, NDE group at KEPRI has developed an ECT technique for the detection and the sizing of the end-tip crackings. The technique uses a specially designed surface-riding probe that can detect size of circumferential crackings with an accuracy of ${\pm}5.31%$ RMS error. This paper describes the ECT instrumentation including the ECT probes, calibration bars, as well as technical approaches.

• Journal of Energy Engineering
• /
• v.25 no.4
• /
• pp.103-109
• /
• 2016

Polyethylene pipes has useful benefits which are anti-corrosive and flexible material, so it is used to gas pipes but also class 3 water pipes of nuclear power plant, process pipes of petrochemical plant and chemical plant. So the usage of polyethylene pipes is widely increased. But it has been limited for the usage of polyethylene, because it can not be directly detected to fusion joints by using non destructive evaluation. Polyethylene pipes are connected by two methods, one is butt fusion and the other is electrofusion. Butt fusion is widely used to connecting the pipes. It is proposed to method for determining the reliability of joints in this study that is detection of the melt flow zone at fusion joints. In this study, middle density polyethylene is used, outside diameter of the test specimen is 225mm and thickness is 20.5mm. Speed of ultrasonic of this test specimen is 2,200m/s. Test specimens were fabricated by varying the heating time which means from 0% to 130% applying time through heating plate to polyethylene for detecting melt flow zone. Also 4 additional test specimens were made, one was made that not scrapping attached surface of pipes but applying 100% of the proper heating time and the others were made to include of soil, gravel and vinly tape paper at fusion joints, that were also applied 100% of proper heating time. Ultrasonic testing to measure the melt flow zone of 20 test specimens was conducted by using 3.5MHz and 5.0MHz ultrasonic probes and melt flow zone measuring was conducted to three times at different point to one specimen. To differentiate the melt flow zone signal, post image processing was equally conducted to all test results and image levels, contrast, sharpen, threshold were adopted to all teat results and the test results were displayed gray scale. From the results, for the shorter heating times the reflection area of multiple echo have been increased, so the data was obtained from the position where it can be eliminated as much as possible. At 80% of proper heating time(168 sec.), the signal of melt flow zone was obtained clearly, so measuring could be conducted. From 7% of proper heating time(15 sec.) to shorter heating times. we could not obtain the signal because test specimen was not fused. From the result, we can verify that measuring of melt flow zone by using phased array ultrasonic imaging method is possible. And we can verify to complete and incomplete butt fusion by measuring the melt flow zone.

• The korean journal of orthodontics
• /
• v.37 no.6
• /
• pp.400-406
• /
• 2007

The purpose of this experimental study was to evaluate the effect of immediate orthodontic loading on the stability at the bone-implant interface of titanium miniscrews in a rabbit model. Methods: Forty titanium miniscrews (1.6 mm diameter, 8 mm length) were inserted in the tibiae of 10 rabbits. Twenty test group miniscrews were subjected to continuous orthodontic forces of 200g immediately after implantation for a period of 6 weeks. The remaining 20 control group miniscrews were left unloaded for the same follow-up interval. Removal torque values were recorded using a digital torque gauge. An independent t-test was performed. Results: All the miniscrews were stable, and exhibited no mobility or displacement throughout the experimental period. Histologically, miniscrews were well-integrated into bone. No statistically significant differences in removal torque data were found between the loaded test and the unloaded control groups. Conclusions: These findings suggest that titanium miniscrews can be used as anchoring units for orthodontic tooth movement immediately after insertion.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2009.06a
• /
• pp.208-208
• /
• 2009

최근 광섬유 센서기술의 수요는 전 산업분야에 걸쳐 높아지고 있으며, 이에 비례하여 기업 간, 국가 간 경쟁이 첨예화되고 있다. 또한 소형화, 경량화, 고성능화 센서에 대한 요구도 높아지고 있어 종래의 각종 센서들의 형태와 개선을 위한 연구개발이 매우 활발하게 전개되고 있으므로 이를 대체할 수 있는 광섬유 센서의 수요가 급격히 늘어날 전망이다. 기존 침입자 감지 시스템은 태풍, 낙뢰, 폭설, 폭우 등의 기상변화나 지반 흔들림, 통행차량 진동 및 전자기 간섭 등에 영향을 받아 오작동, 오경보가 빈번히 발생된다. 이러한 문제의 해결책으로 광섬유 센서 케이블을 이용한 시스템이 대안으로 부각되고 있다. 현재 국내에서 군부대, 공항을 중심으로 펜스와 휴전선 철책에 힘입자 감지를 위하여 도입되고 있다. 광섬유 센서 케이블을 사용하는 광망경비시스템은 광섬유 센서 케이블을 그물망 형태(광망)로 만들어 경계 지역에 설치된다. 광망경비시스템의 원리는 광섬유에 광펄스를 입사시켜 순환시키는데 침입자가 광망을 절단하거나 외력을 가할 경우 발생되는 레일리 산란에 기인하는 후방산란과 접속점과 파단점에서 생기는 반사광을 OTDR(Optical Time Domain Reflectometer)로 검출하여 침입상황 및 침입위치를 탐지한다. 그러나 이러한 침입자 감지를 위한 광망경비시스템의 핵심부품인 광섬유 센서 케이블은 기존에 전량 해외수입에 의존하고 있는 실정이며, 지금까지 국내에서 생산하기 위한 제작 기술과 노하우가 초보단계에 머물러 있다. 이러한 광섬유 센서 케이블 제작에 있어서 중요한 부분이 패키징 기술이라 할 수 있다. 이는 광섬유 센서를 일반적인 피복 구조로 패키징하게 되면, 센서 고유의 특성이 패키징 과정과 운반과정, 포설과정에서 변하게 되고 센서로써의 신뢰성이 크게 저하된다. 본 연구에서는 힘입자 감지용 광섬유 센서 케이블의 설계와 제작을 위한 제조공법을 확립하고, 이를 이용해 제작된 광섬유 센서 케이블의 신뢰성 특성을 평가하였다. 설계 제작된 광섬유 센서 케이블의 구조는 멀티모드광섬유(MMF) 에 0.9 mm Tight buffer를 코팅하고, 광심선 주위에 아라미드 얀을 삽입시킨 후 고문자 수지를 적용하여 외부 피복 (jacket)을 하였다. 제작된 광섬유 센서 케이블의 외경 측정결과 기준치 ($2.95\;{\pm}\;0.03$ mm)를 모두 만족하였고, 850 nm 파장에서의 광 손실 측정 결과 4.0 dB/km 이하였다. 또한 주요 항목의 신뢰성 특성 시험결과, 인장강도는 8~10 kg의 인장력을 갖으며 온도순환시험 ($-30^{\circ}C\;{\sim}\;+75^{\circ}C$)에서의 광 손실은 0.6 dB 이하로 나타나 침입자 감지용 광섬유 센서 케이블로 적합함을 확인할 수 있었다.

• Nuclear Engineering and Technology
• /
• v.19 no.1
• /
• pp.22-33
• /
• 1987

The confirmed integrity of nuclear fuel cladding materials is an important object during steady state and transient operations at nuclear power plant. In this context, the clad material yielding behavior is especially important because of pellet-clad gap expansion. During the steep power excursion, the in-pile irradiation behavior differences between uranium-dioxide fuel pellet and zircaloy clad induce the contact pressure between them. If this pressure reaches the zircaloy clad yield pressure, the zircaloy clad will be plastically deformed. After the reactor power resumed to normal state, this plastic permanent expansion of clad tube give rise to the pellet-clad gap expansion. In this paper, the simple mandrel expansion test method which utilizes thermal expansion difference between copper mandrel and zircaloy tube was adopted to simulate this phenomenon. That is, copper mandrel which has approximately three times of thermal expansion coefficient of zircaloy-4 (PWR fuel cladding material) were used in this experiment at the temperature range from 400C to 700C. The measured plastic expansion of zircaloy outer radius and derived mathematical relations give the yield pressure, yield stress of zircaloy-4 clad at the various clad wall temperatures, the activation energy of zircaloy tube yielding, and pellet-clad gap expansion. The obtained results are in good agreement with previous experimental results. The mathematical analysis and simple test method prove to be a reliable and simple technique to assess the yielding behavior and gap expansion measurement between zircaloy-4 tube and uranium-dioxide fuel pellet under biaxial stress conditions.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.38 no.12
• /
• pp.1240-1246
• /
• 2010

Enthalpy probe with the inner and outer diameters of 1.5 mm and 4.8 mm, respectively, is designed and used to measure the temperatures and velocities along the centerline of Ar arc plasma flow until the probe was destroyed. For this purpose, Ar arc plasma flow is generated by non-transferred type DC arc heater with the power level of 17 kW. From this experiment, it is shown that the designed enthalpy probe can measure the temperature and velocity of arc plasma flow up to 12,000 K and 600 m/s, respectively, without destroy of probe tip. In this extreme case, the arc plasma flow is calculated to transfer the heat flux of ${\sim}5{\times}10^7\;W/m^2$ to the probe based on the heat and thermal boundary equations near the forward stagnation point of a body immersed in arc plasma flow. Consequently, the designed enthalpy probe can measure the wide ranges of plasma temperatures, velocities and concentrations simultaneously, which are generated by various types of arc heaters within the heat flux ranges of $0{\sim}5{\times}10^7\;W/m^2$ on the probe tip.

• Journal of the Korean Magnetics Society
• /
• v.25 no.4
• /
• pp.129-137
• /
• 2015

The Cu(radius ra = $95{\mu}m$)/$Ni_{80}Fe_{20}$(outer radius $r_b$ = $120{\mu}m$) core/shell composite wire is fabricated by electrodeposition. The two diagonal components of impedance tensor for the Cu/$Ni_{80}Fe_{20}$ core/shell composite wire in cylindrical coordinates, $Z_{zz}$ and $Z_{{\theta}{\theta}}$, are measured as a function of frequency in 10 kHz~10 MHz and external static magnetic field in 0 Oe~200 Oe. The equations expressing the diagonal $Z_{zz}$ and $Z_{{\theta}{\theta}}$ in terms of diagonal components of complex permeability tensor, ${\mu}^*_{zz}$ and ${\mu}^*_{{\theta}{\theta}}$, are derived from Maxwell's equations. The real and imaginary parts of ${\mu}^*_{zz}$(f) and ${\mu}^*_{{\theta}{\theta}}$(f) spectra are extracted from the measured $Z_{zz}$(f) and $Z_{{\theta}{\theta}}$(f) spectra, respectively. It is presened that the extraction of ${\mu}^*_{zz}$(f) and ${\mu}^*_{{\theta}{\theta}}$(f) spectra from the diagonal impedance spectra can be a versatile tool to investigate dymanic magnetization process in the core/shell composite wire.