• Title/Summary/Keyword: 연화계수

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Processing of Bi-based glass for transparent dielectrics ($Bi_2O_3$계 투명유전체의 제조)

  • 유재륜;정경원;최승철
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2001.11a
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    • pp.189-194
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    • 2001
  • PDP(Plasma Display Panel)의 투명 유전체에 적용 가능한 저융점 유리 중에서 납성분이 포함 되어 있지 않는 Bi계 유리의 연구를 행하였다. 기판과의 일체화를 위한 유리의 응용으로, 소자와의 반응 억제와 열응력 완화를 위해 유리의 저융점화 및 열팽창 계수를 제어하였다. 본 연구에서 제조된 Bi계 유리는 DTA와 TMA의 열분석을 통해 50$0^{\circ}C$부근에서 연화점이 있고, 7.31~10.02$\times$$10^{-6}$$^{\circ}C$, 비유전을 11.1~13.3, 광투과도가 80%이상으로 PDP 투명유전체에 적용 가능한 Bi계 유리를 얻을 수 있었다.

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A Study on the Fatigue Characteristics of Accelerated Cooled TMCP Steel's Welded Joint with High Heat Input (가속냉각형 TMCP강재 대입열 용접부의 피로특성)

  • 윤중근;김희진
    • Journal of Welding and Joining
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    • v.6 no.1
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    • pp.28-34
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    • 1988
  • The fatigue test was carried out to evaluate the fatigue characteristics of the accelerated cooled (ACC) TMCP steel and its welded joint. From this study, it was confirmed that ACC TMCP steel has higher fatigue strength than conventional steels. After welding, however, the fatigue strength of ACC TMCP steel was deteriorated associated with HAZ softening when weld reinforcement was removed. On the other hand, with weld reinforcement, there is no effect of HAZ softening on the fatigue strength of welded joint because it is strongly dependant on the detail weld geometry i.e., stress concentration factor. Accordingly the fatigue strength of actual welded joint increases with decreasing the stress concentration factor of welded joint, regardless of HAZ softening.

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Thermal properties & crystallization of low melting Phosphate glasses (인산염계 저융점 유리의 열적 특성 및 결정화에 관한 연구)

  • 윤태민;윤영진;이용수;강원호
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.11a
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    • pp.191-194
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    • 2002
  • 본 연구는 친환경재료로서 생체, 전자, 환경재료로서 관심이 증가하고 있는 인산염계 저융점 유리의 열적특성 및 결정화에 대한 연구를 진행하였다. $K_2$O-CaO-P$_2$O$_{5}$ 삼성분계 인산염 유리에 대해 P$_2$O$_{5}$ 함량이 40~60mo1% 범위의 조성을 선정하여 전통 용융법에 의해 제조하였으며, 제조된 유리의 전자 패키징 및 저온소결 첨가제용 frit으로의 적용 가능성을 평가하기 위한 기초 연구로서, DSC, TMA를 통해 열적특성을 평가하였다. 제조된 유리의 연화온도는 320-5$50^{\circ}C$였으며, 열팽창 계수는 26~60$\times$$10^{-6}$/$^{\circ}C$의 범위였다. 제조된 유리의 열분석 결과로부터 최적 결정화 온도를 조사하였으며, 결정화 유리를 제조하여 XRD을 통해 결정상을 조사하였다.

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Preparation Pb free frit for Ag Paste in PDP application (PDP적용 Ag paste의 Pb free frit개발)

  • 김형수;최정철;최승철
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.11a
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    • pp.101-103
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    • 2002
  • PDP등의 각종 전자부품에 사용되는 Ag paste 의 frit은 주로 PbO를 주성분으로 하는 물질이 사용되어왔다. 그러나 이러한 Pb계 재료는 환경유해한물질로 규제대상이 되고 있다. 이에 대비하여 본 연구에서는 Bi$_2$O$_3$을 주성분으로 하여 B$_2$O$_3$, SiO$_2$, A1$_2$O$_3$가 함유된 새로운 frit을 개발하였다. TMA등을 이용하여 열적 특성을 관찰하였으며, 전극용 Ag-Paste를 제조한 후 스크린프린팅하여 인쇄성과 미세구조를 관찰하였고, 전기저항 및 소성두께를 측정하였다. 또한 전이온도, 연화점, 열팽창계수등을 조사하여 기존의 Pb함유 frit과 물성을 비교하였으며 PDP용 Ag전극에 적용하는 새로운 frit으로의 가능성을 검토하였다.

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Fabrication and Properties of Dielectric Materials used for Mobile Phone Antenna Chip Type (고주파 이동통신기기용 칩형 세라믹 안테나를 위한 유전체재료의 제조 및 특성 평가)

  • Lee H.K.;Lee Y.S.;Hwang S.J.;Kang W.H.
    • Proceedings of the KAIS Fall Conference
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    • 2004.06a
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    • pp.86-88
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    • 2004
  • 본 연구에서는 고주파 이동통신 기기용 칩형 세라믹 안테나의 사용을 위한 저유전율 및 저온동시소성이 가능한 CaO-B2O3-SiO2계 유리를 제조하고자 하였다. 제조된 CaO-B2O3-SiO2계 유리는 열분석을 통하여 낮은 연화온도를 갖는 안정한 유리조성을 선정하였다. 유리분말을 이용하여 성형된 샘플은 소결온도에 따른 특성을 조사하였다. 소결온도변화에 따라 유전율(${\epsilon}_r$)은 4-4.5값을 나타냈으며, 유전손실(tan$\delta$)은 <$0.1\%$ 보였으나, 품질계수(Q$\times$f)는 큰 변화폭을 보였다.

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A Study on Rheological Behavior of Korean Straight Asphalts (국내 스트레이트 아스팔트의 거동 특성 연구)

  • Kim, Nam-Ho;Hwang, Sung-Do;Park, Young-Cheol
    • International Journal of Highway Engineering
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    • v.1 no.2
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    • pp.121-133
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    • 1999
  • This study was based on the evaluation of 9 asphalts that were produced in five major Korean refineries. The study was concentrated to identify the problems of the current asphalt specification (KS M 2201) and to determine the ranges of visco-elastic asphalt behavior. As a conventional asphalt property. asphalt penetration, ring and ball(R&B) softening point, asphalt viscosity, and flash point of asphalt were measured. Also Dynamic Shear Rheometer (DSR) were used to evaluate visco-elastic properties of asphalts in the $-20^{\circ}C$ through $30^{\circ}C$ temperature range. These properties before and after the short-term (RTFO) and long-term (PAV) aging were compared and analyzed to achieve the research objectives. The conclusion from this study can be summarized by the followings. The low temperature rheological behavior of all the straight asphalt from five major Korean refineries is similar regardless of asphalt grade. In the mean while, the rheological behavior at high and intermediate temperature of Korean straight asphalt varies depending on asphalt grade.

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Determination of Steel-concrete Interface Parameters: Me chanical Properties of Interface Parameters (강-콘크리트 계면의 계면상수 결정 : 계면상수의 역학적 성질)

  • Lee, Ta;Joo, Young-Tae;Lee, Yong-Hak
    • Journal of the Korea Concrete Institute
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    • v.21 no.6
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    • pp.781-788
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    • 2009
  • Mechanical properties of steel-concrete interface were evaluated on the basis of experimental observations. The properties included bond strength, unbounded and bonded friction angles, residual level of friction angle, mode I fracture energy, mode II bonded fracture energy and unbonded slip-friction energy under different levels of normal stress, and shape parameters to define geometrical shape of failure envelope. For this purpose, a typical type of constitutive model of describing steel-concrete interface behavior was presented based on a hyperbolic three-parameter Mohr-Coulomb type failure criterion. The constitutive model depicts the strong dependency of interface behavior on bonding condition of interface, bonded or unbounded. Values of the interface parameters were determined through interpretation of experimental results, geometry of failure envelope and sensitivity analysis. Nonlinear finite element analysis that incorporates steel-concrete interface as well as material nonlinearities of concrete and steel were performed to predict the experimental results.

Effect of Particle Size of the Filler on the Thermal Properties of the Sealing Glass for Solid Oxide Fuel Cells (필러의 입자크기가 고체전해질 연료전지용 밀봉유리의 열적 특성에 미치는 영향)

  • Cho, Min-Young;Moon, Ji-Woong;Lee, Mi-Jae;Choi, Byong-Hyun;Park, Sun-Min;Hwang, Hae-Jin;Choi, Heon-Jin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2007.11a
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    • pp.305-305
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    • 2007
  • SOFC용 밀봉유리$({\sim}10.0{\times}10^{-7}/K)$의 열팽창 계수를 SUS430$({\sim}12.0{\times}10^{-7}/K)$ 인터커넥터에 매칭 시키기 위하여 모유리에 비하여 열팽창계수가 큰 $CaTiO_3\;({\sim}13.5{\times}10^{-7}/K)$ 입자를 필러로서 첨가하였다. 필러입자의 첨가량이 증가함에 따라 밀봉재의 열팽창 계수가 증가하고, 동일 함량의 필러를 첨가하는 경우 필러 입자의 크기가 작을 수록 밀봉재의 연화점 상승 폭이 커서 SUS430 기판과의 접합 상태가 불량해짐을 관찰하였다. 필 테스트, 접합시험, 미세구조 분석 등을 통하여 필러 입자 크기가 증가 할 수록 SUS430과의 접합이 가능한 범위 내에서 보다 많은 양의 필러를 첨가하는 것이 가능하기 때문에 열팽창 계수 제어가 용이하다는 것을 확인 할 수 있었다.

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Usefulness of Dual-Echo in Steady State (DESS) Image in Chondromalacia of Knee Joint: Comparison of DESS and Turbo Spin-Echo MR Images (슬관절 연골 연화증의 진단에서의 Dual Echo in Steady State (DESS) 영상의 유용성 : 급속 스핀에코 자기공명 영상과 비교)

  • 윤삼현;하두회
    • Investigative Magnetic Resonance Imaging
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    • v.3 no.1
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    • pp.66-72
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    • 1999
  • Purpose : To evaluate the usefulness of Dual Echo in Steady State(DESS) image in the diagnosis of chondromalacia of the knee compared with turbo spin-echo MR images Materials and Methods : We included 26 patients with chondromalacia of the knee. MR imaging was obtained with a 1.5T imager. Sagittal and coronal double echo T2 weighted images(TR/TE 3000-4200/16-96msec, FOV $140-160{\times}140-160mm$, matrix size $180{\times}256$, slice thickness 4.0mm, interslice gap 0.5mm), and sagittal DESS image(TR/TE 25.4/9.0msec, flip angle $35-45^{\circ}$, FOV $150-160{\times}150-160mm,{\;}matrix{\;}size{\;}192{\times}256$, effective slice thickness 1.5mm) were obtained. Cartilage lesions were staged according to a modified scheme proposed by Outerbirdge: grade 0, normal; grade 1, softening or/and swelling; grade 2, mild surface fibrillation or/and less than 50% of cartilage thickness; grade 3, severe surface fibrillation or/and loss of more than 50% of cartilage thickness but without exposure of subchondral bone; and grade 4, complete loss of cartilage with subchondral bone exposure. Gradings were determined by two readers with consensus, and patellofemoral, medial and lateral tibiofemoral compartments were evaluated. Results : Arthroscopic findings revealed grade 1 in seven cases, grade 2 in 21 cases, grade 3 in six cases, and grade 4 in 18 cases. Sensitivity of turbo spin-echo MR image was as follows; 0%, 14%, 0%, 61% in each grade, and sensitivity of DESS image was as follows; 0%, 33%, 50%, 67%, in each grade(p=0.001). In the detection of chondromalacic lesions regardless of gradings, sensitivity, specificity and accuracy of conventional MR image were 59.6% 88.6% 78.8%, and of DESS image, 73.1% 88.4%, 82.2%(p=0.007). Conclusion : For chondromalacia of knee joints, DESS images showed higher sensitivity than turbo spin-echo MR images. Therefore, DESS images will be helpful for diagnosis of chondromalacia of knee joints.

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Characteristics of velocity-dependent shear behavior of saw-cut rock joints at different shear velocities (편평한 암석절리면의 속도 의존적 전단거동 특성)

  • Park, Byung-Ki;Lee, Chang-Soo;Jeon, Seok-Won
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.9 no.2
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    • pp.121-131
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    • 2007
  • Recently, the probability of rock joints being exposed to free faces is getting higher for the scale of rock mass structures gets larger. Also, the frequency of occurring dynamic events such as earthquakes and blasting has been increasing. Thus, the shear behavior of rock joints under different conditions needs to be investigated. In this study, a series of direct shear tests were carried out under various conditions to examine the velocity-dependent shear behavior of saw-cut rock joints. Two types of direct shear test were carried out. The first was to examine the velocity-dependent shear behavior of saw-cut rock joints at seven different shear velocities, each with three different normal stresses. The second was to examine the shear behavior of saw-cut rock joints when three different instantaneous shear velocities changed. As a result, the coefficient of friction was affected by normal stress. The breakpoint velocity, the point when the change of shear velocity starts to affect the frictional behavior, became lower as normal stress increased. Also, as the shear velocity became lower, the degree of stress-drop on stick-slip behavior became larger. As a result of examining the changes of friction coefficient, velocity weakening (decrease of friction coefficient) was observed. The decrement of friction coefficient due to the changes of shear velocity under slow shear velocity was larger than that under fast shear velocity.

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