• Proceedings of the Korean Fiber Society Conference
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• 2001.10a
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• pp.452-455
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• 2001

고분자/실리케이트 나노복합체란 고분자 매트릭스에 층상 구조의 점토 광물을 나노 스케일의 시트상의 기본 단위로 박리(exfoliation)ㆍ분산시켜 얻어진 복합체를 말한다. 실리케이트를 구성하는 두께 1nm 정도의 판으로 박리ㆍ분산시키기 때문에 5wt% 정도의 첨가량만으로도 고분자의 획기적인 물성 개선이 가능하다는 장점을 가지고 있다[1]. (중략)

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.13 no.5
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• pp.217-221
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• 2003

In this work, chemical-solution derived silicate fibers were prepared by mixing tetraethyl orthosilicate, ethanol, distilled water, and hydrochloric acid in order to investigate surface roughness of fiber. Silicate fibers were drawn by using a viscous solution after evaporation at $80^{\circ}C$. The dried gel fibers were finally annealed at $1000^{\circ}C$, $1100^{\circ}C$, $1200^{\circ}C$ and $^1300{\circ}C$ for 60 min in dried air (flow rate = ∼200 ml/min). The crystallinity of the heat-treated silica fiber was analyzed by the X-ray diffraction $\theta$-2$\theta$ scan. A field emission-scanning electron microscope and an atomic force microscope were used to evaluate surface properties. The silicate fiber annealed at $1300^{\circ}C$ showed high value of root mean square roughness and had a relatively inhomogeneous surface structure.

• Journal of the Korea institute for structural maintenance and inspection
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• v.28 no.3
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• pp.59-65
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• 2024

In this study, in order to improve the mechanical properties and durability of asphalt mixtures, a modifier (CSM, Cationized Silicate Modifier) was applied to asphalt to derive optimal mixing ratio conditions. Design of asphalt mixture using modified asphalt binder was conducted, and moisture resistance and dynamic stability were evaluated for optimal mixing conditions. The evaluation results showed that it exceeded the standards stipulated in the relevant guidelines, and as a result of conducting a water permeability test on the optimal mixing condition, it was confirmed that impermeable performance was secured. As a result of examining the noise reduction performance through field test, a noise reduction performance of about 10 dB was secured compared to before paving. It will be necessary to secure reliability through continuous noise generation evaluation in the future.

• Proceedings of the Korean Ceranic Society Conference
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• 2000.04a
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• pp.20.1-20.1
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• 2000

• Composites Research
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• v.35 no.3
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• pp.201-215
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• 2022

This paper presents the development of thin and lightweight ultra-high temperature radar-absorbing ceramic composites composed of an aluminosilicate ceramic matrix-based geopolymer reinforced ceramic fiber and sendust magnetic nanoparticles in X-band frequency range (8.2~12.4 GHz). The dielectric properties with regard to complex permittivity of ceramic/sendust-aluminosilicate composites were proportional to the size of sendust magnetic nanoparticle with high magnetic characteristic properties as flake shape and its concentrations in the target frequency range. The characteristic microstructures, element composition, phase identification, and thermal stability were examined by SEM, EDS, VSM and TGA, respectively. The fabricated total thicknesses of the proposed single slab ultra-high temperature radar absorber correspond to 1.585 mm, respectively, exhibiting their excellent EM absorption performance. The behavior of ultra-high temperature EM wave absorption properties was verified to the developed free-space measurement system linked with high temperature furnace for X-band from 25℃ to 1,000℃.

• Proceedings of the Korean Fiber Society Conference
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• 2003.04a
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• pp.352-353
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• 2003

Clay 분산 유/무기 나노복합재 제조기술은 실리케이트 층상구조의 점토광물을 나노 스케일의 시트상의 기본 단위로 박리(exfoliation)하여 고분자수지에 분산시킴으로써 범용 고분자의 낮은 기계적 물성의 한계를 엔지니어링 플라스틱 수준으로까지 올리고자 하는 것으로서, 기존의 무기 충진재 및 강화재의 입자크기(〉1 $\mu\textrm{m}$)를 나노 스케일까지 분산시켜 기존 무기물 충진 복합재의 단점을 한층 보완하는 것을 목표로 하고 있어 성능 및 원가 면에서 매우 유리한 방법으로 21세기의 복합재료 생산시장의 판도에 상당한 변화를 가져오게 할 수 있는 핵심기술이라 할 수 있다. (중략)

• Journal of the Korea Concrete Institute
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• v.17 no.3 s.87
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• pp.427-434
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• 2005

An experimental investigation was carried out in order to verify the compressive strength, flexural strength, equivalent bending strength, rebound rate of shotcrete according to silicate accelerator, aluminate accelerator, cement mineral accelerator respectively and to especially evaluate the performance of shotcrete using cement mineral accelerator for high quality. The test result of compressive strength was showed that all accelerators were satisfied the required test value for each age, for the requirement of having the $75\%$ or higher compressive strength ratio to plain concretes at 28 days, cement mineral accelerator with $87\%$ compressive strength ratio was only satisfied. In flexural strength test, cement mineral accelerator was satisfied the flexural strength requirement in steel fiber reinforced shotcrete for each age. Aluminate type was conformed to the requirement for 28 days, but not at 1 day, silicate type was failed to satisfy standard requirement. Rebound rate was measured between $11{\~}19\%$ and cement mineral accelerator was showed comparatively lower rebound rate. Based on the test results, cement mineral accelerator exhibited excellent strength improvement and lower rebound rate compared to the conventional accelerator, its result is showed the possibility of making high performance shotcrete.

• Resources Recycling
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• v.25 no.6
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• pp.73-81
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• 2016

Geopolymers produced from aluminosilicate materials such as metakaolin and coal ash react with alkali activators and show higher fire resistance than portland cement, due to amorphous inorganic polymer. The percentage of thermal shrinkage of geopolymers ranges from less than 0.5 % to about 3 % until $600^{\circ}C$, and reaches about 5 ~ 7 % before melting. In this study, geopolymers paste having Si/Al = 1.5 and being mixed with carbon nanofibers, silicon carbide, pyrex glass, and vermiculite, and ISO sand were studied in order to understand the compressive strength and the effects of thermal shrinkage of geopolymers. The compressive strength of geopolymers mixed by carbon nanofibers, silicon carbide, pyrex glass, or vermiculite was similar in the range from 35 to 40 MPa. The average compressive strength of a geopolymers mixed with 30 wt.% of ISO sand was lowest of 28 MPa. Thermal shrinkage of geopolymers mixed with ISO sand decreased to about 25 % of paste. This is because the aggregate particles expanded on firing and to compensate the shrinkage of paste. The densification of the geopolymer matrix and the increase of porosity by sintering at $900^{\circ}C$ were observed regardless of fillers.

• Composites Research
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• v.30 no.2
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• pp.84-93
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• 2017

This study investigates thermal and mechanical characterization of environmental barrier coating on the $SiC_f-SiC$ composites. The spherical environmental barrier coating (EBC) powders are prepared using a spray drying process for flowing easily during coating process. The powders consisting of mullite and 12 wt% of Ytterbium silicate are air plasma sprayed on the Si bondcoat on the LSI SiC fiber reinforced SiC composite substrate for protecting the composites from oxidation and water vapor reaction. We vary the process parameter of spray distance during air plasma spray of powders, 100, 120 and 140 mm. After that, we performed the thermal durability tests by thermal annealing test at $1100^{\circ}C$ for 100hr and thermal shock test from $1200^{\circ}C$ for 3000 cycles. As a result, the interface delamination of EBC never occur during thermal durability tests while stable cracks are prominent on the coating layer. The crack density and crack length depend on the spray distance during coating. The post indentation test indicates thermal tests influence on the indentation load-displacement mechanical behavior.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.16 no.4
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• pp.2344-2349
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• 2015

In Korea, summer is hot and humid, and air-conditioners consume too much electricity due to large amount of latent heat. Simultaneous usage of dehumidifier may reduce the latent heat and save the electricity. In this study, dehumidification performance was measured in a constant temperature and humidity chamber for a small-sized dehumdification rotor made of inorganic fiber impregnated with metallic silicate. Variables were rotor speed, room temperature, regeneration temperature, room relative humidity and frontal velocity to the rotor. Results showed that there existed optimum rotor speed (1.0 rpm), and optimum regeneration temperature ($100^{\circ}C$). Above the optimum rotor speed, incomplete regeneration is responsible for reduced dehumidification. Above the optimum regeneration temperature, increased temperature difference between regeneration and dehumidification process is responsible for reduced dehumidification. The amount of dehumidification also increases with the increase of relative humidity, dehumidification temperature and flow velocity into the rotor.