• 제목/요약/키워드: 시효 처리

검색결과 166건 처리시간 0.032초

$Ti-50.1at\%$ Ni합금의 변태거동에 미치는 시효처리의 영향(I) (The Effect of Ageing on the Transformation Behavior of $Ti-50.1at\%$ Ni Alloy(I))

  • 우흥식;박성범;강봉수;김성진
    • 한국안전학회지
    • /
    • 제19권4호
    • /
    • pp.1-7
    • /
    • 2004
  • This study investigated the effects of aging on the transformation behavior of $Ti-50.1at\%$ Ni alloy by means of differential scanning calorimetry. It was found that aging in the temperature range of $350^{\circ}C\~550^{\circ}C$ induced complex transformation behavior, involving the R-phase and multiple-stage martensitic transformation. Usually aged Ni-rich NiTi alloys undergo martensitic transformation on cooling from high temperatures in two step : B2 to R and then R to Bl9'(normal behavior). But under certain ageing conditions, the transformation can also occur in three or more step(unusual multiple step behavior). In the present study we use differential seaming calorimetry(DSC) for a systematic investigation of the evolution of transformation behavior with ageing temperature and time.

음향방출법에 의한 SM45C 응력시효 처리재의 인장특성 평가 (An Evaluation of Tensile Characteristics of the Stress Aging Heat-treated SM45C Steel by Acoustic Emissions)

  • 이장규;박복남
    • 대한안전경영과학회:학술대회논문집
    • /
    • 대한안전경영과학회 2009년도 춘계학술대회
    • /
    • pp.413-421
    • /
    • 2009
  • This paper investigates tensile characteristics of the stress aging heat-treated SM45C steel which are aging temperature at $250^{\circ}C$, $300^{\circ}C$, aging time at 1, 3 hours, and applied load at 300, 400N conditions by using acoustic emission. Most suitable aging condition was aging temperature $300^{\circ}C$, aging time 1 hour, and aging applied load 300N. And increased yield load 28.3% than non-treatment specimen in this condition. AE energy in elastic limit increased about 16.7 times than non-treatment specimen. When aging time is 3 hours, yield load decreased than other conditions that possibility is high to have itself defect on inside the specimen or coarse grain size precipitation is different in happened over-aging phenomenon. Especially, in case of $300^{\circ}C$, 3 hours and 400N condition appeared AE energy in elastic limit fairly high about 30 times than non-treatment specimen. This is considered by emit a lot of energies when material causes plastic deformation because the ductility increases on specimen by over-aging phenomenon.

  • PDF

극저온 환경에 적용되는 INCONEL 718합금의 GTAW 기계적 특성 평가 (Mechanical Properties Evaluation of GTAW for INCONEL 718 alloy apply to Cryogenic Condition)

  • 김기홍;문인상;이병호;이수용
    • 한국추진공학회:학술대회논문집
    • /
    • 한국추진공학회 2009년도 제33회 추계학술대회논문집
    • /
    • pp.619-622
    • /
    • 2009
  • INCONEL 718합금은 상온, 고온 및 저온환경에서 기계적 특성이 아주 우수하다. 상온에서의 모재 강도는 약 900MPa이며, 열처리 후 시효경화처리에 의해 강도가 약 1300MPa까지 증가한다. 이러한 INCONEL 718합금의 기계적 특성은 시험결과에서도 유사한 값을 나타내었고, GTAW 용접부의 상온 기계적 특성도 모재보다 우수한 강도를 나타내었다. 또한 저온에서의 기계적 특성은 모든 시험조건에서 상온보다 높은 강도를 나타내었으며, 열처리 모재시편과 용접시편은 1400MPa에 달하는 고강도를 나타내었다. 이러한 결과를 바탕으로 INCONEL 718합금의 저온 기계적 특성이 우수한 것을 증명하였고, 용접성 또한 모재의 특성과 같이 상온 및 저온 특성이 우수한 것을 알 수 있었다. INCONEL 718 합금과 STS 316L의 이종접합의 경우에도 $-100^{\circ}C$환경의 인장강도가 상온보다 300MPa 이상 증가하는 것을 알 수 있었다. 따라서, INCONEL 718합금은 $100^{\circ}C$이하부터 일정온도까지는 기계적 특성이 계속 증가 할 것으로 사료되며, 극저온 고압 상태로 공급되는 산화제 배관 제작에 적합한 소재로 판단된다.

  • PDF

시효열처리 및 UNSM 처리에 따른 316L 스테인리스강의 입계부식거동 (Intergranular Corrosion of 316L Stainless Steel by Aging and UNSM (Ultrasonic Nano-crystal Surface Modification) treatment)

  • 이정희;김영식
    • Corrosion Science and Technology
    • /
    • 제14권6호
    • /
    • pp.313-324
    • /
    • 2015
  • Austenitic stainless steels have been widely used in many engineering fields because of their high corrosion resistance and good mechanical properties. However, welding or aging treatment may induce intergranular corrosion, stress corrosion cracking, pitting, etc. Since these types of corrosion are closely related to the formation of chromium carbide in grain boundaries, the alloys are controlled using methods such as lowering the carbon content, solution heat treatment, alloying of stabilization elements, and grain boundary engineering. This work focused on the effects of aging and UNSM (Ultrasonic Nano-crystal Surface Modification) on the intergranular corrosion of commercial 316L stainless steel and the results are discussed on the basis of the sensitization by chromium carbide formation and carbon segregation, residual stress, grain refinement, and grain boundary engineering.

시효처리된 연료전지 집전판용 Matte 주석도금 동판의 고온열화 거동과 비저항변화 (Degradation Behavior and Resistivity Changes After Thermal Aging of Matte Tin-Plated Copper Sheet for Current Collector in Fuel Cell)

  • 김주한;김재훈;구경완;금영범;정귀성;고행진;한상옥
    • 전기학회논문지
    • /
    • 제58권8호
    • /
    • pp.1559-1565
    • /
    • 2009
  • Resistivity changes and intermetallic growth after thermal aging of Matter tin-plated copper sheet for current collector in fuel cell were investigated to survey the diffusion of Cu into Sn in interface and surface. The results show that the intermetallic growth and resistivity depended on thermal aging temperature and dwell time. In Sn plate on a Cu substrate, Cu6Sn5(${\mu}$) and Cu3Sn(${\varepsilon}$) intermetallics layer were formed at plate/substrate interface. Cu6Sn5(${\mu}$) intermetallics layer gradually changed Cu3Sn(${\varepsilon}$). Moreover Cu get through Sn layer and it was diffused in the surface at $200^{\circ}C$. On the other hand, only Cu3Sn(${\varepsilon}$) intermetallics layer were formed at plate/substrate interface at $300^{\circ}C$. Consequently, the intermetallics formation, thermal condition and oxidation of surface, causes increase in the resistivity of Tin-plated copper sheet.

E.B 용접된 18% Ni 마르에이징강 박판의 인장이음강도에 관한 연구 (A Study of Tensile Strength in 18% Ni Maraging Steel Sheet Welded with Electron Beam)

  • 정병호;김무길;김원녕
    • Journal of Advanced Marine Engineering and Technology
    • /
    • 제21권2호
    • /
    • pp.157-165
    • /
    • 1997
  • The strength level of welded joint in room temperature and elevated temperature up to $600^{\circ}C$ was investigated in 250 and 300 grade 18% Ni maraging steel sheet welded with electron beam. The results obtained in this study are as follows; 1. Optimum welding heat input was 600J/cm in 1.0mm thickness and the room temperature tensile strength, joint efficiency of welded joint treated with optimum aging condition were found to be about 166kg/$mm^2$, 95% in 250 grade, 189kg/$mm^2$, 92% in 300 grade maraging steel sheet, respectively. 2. Tensile strength of welded joint in room temperature increased slightly by aging after repeated solution heat treatment, but the fracture mode showed a shear. 3. Joint efficiency at a temperature between $540^{\circ}C$and $600^{\circ}C$ found to be about 72% to 55%, but the joint efficiency exceeded about 90% below $300^{\circ}C$. 4. The fracture occurred in most weld metal, and the fracture surface showed a shallow dimple.

  • PDF

전기화학기법에 의한 슈퍼 오스테나이트 스테인리스강의 열화손상 평가 (An Evaluation of Degraded Damage for Superaustenitic Stainless Steel by Electrochemical Polarization Technique)

  • 권일현;이송인;백승세;이종기;;유효선
    • 대한기계학회:학술대회논문집
    • /
    • 대한기계학회 2001년도 추계학술대회논문집A
    • /
    • pp.143-148
    • /
    • 2001
  • This research was undertaken to clarify effects of thermal aging on electrochemical and mechanical properties of superaustenitic stainless steel. The steel was artificially aged at $300{\sim}650^{\circ}C$ for $240{\sim}10,000hrs$. and investigated at $-196{\sim}650^{\circ}C$ using small punch(SP) test. Also, the change in electrochemical properties caused by effects of thermal aging was investigated using electrochemical anodic polarization test in a KOH electrolyte. Carbides and ${\eta}-phase(Fe_2Mo)$ precipitated in the grain bounderies seem to deteriorate the mechanical properties by decreasing cohesive strength in the grain bounderies and promote the current density observed in electrochemical polarization curves. The electrochemical and mechanical properties of superaustenitic stainless steel was drastically decreased in the specimen aged at $650^{\circ}C$.

  • PDF

슈퍼 오스테나이트 스테인리스강의 열화손상에 대한 비파괴적 평가 (An Nondestructive Evaluation of Degraded Damage for Superaustenitic Stainless Steel)

  • 권일현;백승세;;유효선
    • 대한기계학회논문집A
    • /
    • 제26권7호
    • /
    • pp.1332-1339
    • /
    • 2002
  • This research was undertaken to clarify effects of thermal aging on electrochemical and mechanical properties of superaustenitic stainless steel and to detect the material degradation nondestructively. The steel was artificially aged at $300{\sim}650^{\circ}C$ for $240{\sim}10,000h$ and the mechanical properties were investigated at $-196{\sim}650^{\circ}C$ using small punch(SP) test. Also, the change in electrochemical properties caused by effects of thermal aging on superaustenitic stainless steel was investigated using electrochemical anodic polarization test in a KOH electrolyte. Carbides and ${\eta}-phase(Fe_2Mo)$ precipitated in the grain boundaries seem to deteriorate the mechanical properties by decreasing cohesive strength in the grain boundaries and to promote the current density observed in electrochemical polarization curves, The electrochemical and mechanical properties of superaustenitic stainless steel decreased significantly in the specimen aged at $650^{\circ}C$ corresponding to the sensitization temperature for conventional austenitic stainless steels.

열시효 처리된 무연 솔더 볼 연결부의 충격 전단강도 평가 (Evaluation of the Impact Shear Strength of Thermal Aged Lead-Free Solder Ball Joints)

  • 정진성;김호경
    • 한국안전학회지
    • /
    • 제30권6호
    • /
    • pp.7-11
    • /
    • 2015
  • The present study investigates the impact shear strength of thermal aged Sn-3Ag-0.5Cu lead-free solder joints at impact speeds ranging from 0.5 m/s to 2.5 m/s. The specimens were thermal aged for 24, 100, 250 and 1000 hours at $100^{\circ}C$. The experimental results demonstrate that the shear strength of the solder joint decreases with an increase in the load speed and aging time. The shear strength of the solder joint aged averagely decreased by 43% with an increase in the strain rate. For the as-reflowed specimens, the mode II stress intensity factor ($K_{II}$) of interfacial IMC between Sn-3.0Ag-0.5Cu and a copper substrate also was found to decrease from $1.63MPa.m^{0.5}$ to $0.97MPa.m^{0.5}$ in the speed range tested here. The degradations in the shear strength and fracture toughness of the aged solder joints are mainly caused by the growth of IMC layers at the solder/substrate interface.

페라이트 상을 갖는 12Cr 내열강의 기계적성질 및 감쇠능에 미치는 시효처리의 영향 (Effect of Aging Treatment on the Mechanical Properties and Damping Capacity of 12Cr Heat Resistant Steel with Ferrite Phase)

  • 강창룡;최한글;박형균;성장현;이도훈
    • 열처리공학회지
    • /
    • 제24권1호
    • /
    • pp.23-30
    • /
    • 2011
  • This study was carried out to investigate the effect of aging treatment on the mechanical properties and damping capacity of 12Cr heat resistant steel with ferrite phase. While hardness values in ferrite phase was not changed, that in martensite phase was dramatically dropped in early stage of aging treatment and then gradually decreased with increase of aging time. As aging treatment was carried out, the precipitation was not detected in ferrite phase, while carbides were precipitated in martensite phase. With increasing the aging time, tensile strength eventually decreased while impact toughness increased rapidly in the early stage of aging and then gradually increased. Besides, it was confirmed that damping capacity was not changed in the early stage of aging and then gradually increased with increase of aging time.