• Title/Summary/Keyword: 시효 열처리

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The Effect of Age Heat-treatment to the Electro-Chemical Corrosion Behavior on Ti-6Al-4V (Ti-6Al-4V재의 전기화학적부식 거동에 미치는 시효열처리의 영향)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.24 no.6
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    • pp.70-77
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    • 2000
  • In this paper, the effect of solution and age heat treatment to the corrosion behavior for the Ti-6Al-4V alloy were studied by cyclic polarization methods. Ti-6Al-4V was solution heat treated at $1,066^{\circ}C$ and $966^{\circ}C$ for 5 hours, and followed by age heat treated at $650^{\circ}C$, $600^{\circ}C$ and $550^{\circ}C$ with 1, 2, 4, 8 and 16 hours under vacuum environment. Test solution was 3.5% NaCl with temperature $25^{\circ}C$. The obtained results were as follows: 1. Base metal was exhibited higher electrical charge than that of solution and aged material. With decrease of solution-treatment temperature from 1066 to $966^{\circ}C$, the electrical charge was increased due to softening of micro structure. 2. The corrosion resistance of specimen that solution treated at $966^{\circ}C$ for 5 hours and age heat treated at 650, 660 and $550^{\circ}C$ were increased with increase of aging time to 4, 8 and 16 hours respectively, and then decreased. 3. In case of 316L stainless steel, measured charge and corrosion potential was 0.0627 coulomb and -614 mV respectively. Corrosion resistance of Ti-6Al-4V was higher than that of 316L.

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Grain Refining and Age Hardening of Mg-Zn Alloys by Addition of Cu and Si (Cu 및 Si첨가에 의한 Mg-Zn합금계의 입자미세화 및 시효경화)

  • Hwang, Jin-Hwan;Nam, Tae-Hyeon;An, In-Seop;Kim, Yu-Gyeong;Heo, Gyeong-Cheol;Heo, Bo-Yeong
    • Korean Journal of Materials Research
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    • v.5 no.6
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    • pp.682-689
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    • 1995
  • In order to refine the grain size of Mg-Zn alloy 0.5 to 6wt.%Cu or Si elements were added. Alloy ingot was made under vacuum atmosphere of 4 ${\times}$ 10$\^$-4/ Torr in the quartz tube coated by BN. Grain size and hardness were measured after solution treatment for 8 hours at 435$^{\circ}C$. Optimal condition for grain size refining effect was obtained at the minimum composition of 2wt.%Cu or 1.5wt.%Si addition to Mg-6wt%Zn alloy. Age hardening behavior was experimented at the optimal compositions of the Mg-6wt.%Zn, Mg-6wt.% Zn-2wt.%Cu and Mg-6wt.% Zn-1.5wt.%Si. The hardness increment due to fine grain size was higher at the Mg-Zn-Cu alloy system, but that due to age hardening was higher at the Mg-Zn-Si alloy system.

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The Effect of Aging Treatment on the High Temperature Fatigue Fracture Behavior of Friction Welded Domestic Heat Resisting Steels (SUH3-SUS 303) (마찰용접된 국산내열 강 (SUH3-SUS303 )의 시효열처리가 고온피로강도 및 파괴거동에 미치는 영향에 관한 연구)

  • Lee, Kyu-Yong;Oh, Sae-Kyoo
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.17 no.2
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    • pp.93-103
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    • 1981
  • It is well-known that nowadays heat resisting and anti-corrosive materials have been widely used as the components materials of gas turbines, nuclear power plants and engines etc. In the fields of machine production industry. And materials for engine components, like as the exhaust valve of internal combustion engine, have been required to operate under the high temperature range of $700^{\circ}C$-$800^{\circ}C$ and high pressured gas with repeated mechanical load for the high performance of engines. For these components, friction welding for bonding of dissimilar steels can be applied for in order to obtain process shortening, production cost reduction and excellent bonding quality. And age hardening recently has been noticed to the heat resisting materials for further strengthening of high temperature strength, especially high temperature fatigue strength. However, it is difficult to find out any report concerning the effects of age hardening for strengthening high temperature fatigue strength to the Friction welded heat resisting and anti-corrosive materials. In this study the experiment was carried out as the high temperature rotary bending fatigue testing under the condition of $700^{\circ}C$ high temperature to the friction welded domestic heat resisting steels, SUH3-SUS303, which were 10hr., 100hr. aging heat treated at $700^{\circ}C$ after solution treatment 1hr. at $1, 060^{\circ}C$ for the purpose of observing the effects of the high temperature fatigue strength and fatigue fracture behaviors as well as with various mechanical properties of welded joints. The results obtained are summarized as follows: 1) Through mechanical tests and micro-structural examinations, the determined optimum welding conditions, rotating speed 2420 rpm, heating pressure 8kg/mm super(2), upsetting pressure 22kg/mm super(2), the amount of total upset 7mm (heating time 3 sec and upsetting time 2 sec) were satisfied. 2) The solution treated material SUH 3, SUS 303, have the highest inclination gradient on S-N curve due to the high temperature fatigue testing for long time at $700^{\circ}C$. 3) The optimum aging time of friction welded SUH3-SUS 303, has been recognized near the 10hr. at $700^{\circ}C$ after the solution treatment of 1hr. at $1, 060^{\circ}C$. 4) The high temperature fatigue limits of aging treated materials were compared with those of raw material according to the extender of aging time, on 10hr. aging, fatigue limits were increased by SUH 3 75.4%, SUS 303 28.5%, friction welded joints SUH 3-SUS 303 44.2% and 100hr. aging the rates were 64.9%, 30.4% and 36.6% respectively. 5) The fatigue fractures occurred at the side of the base matal SUS303 of the friction welded joints SUH 3-SUS 303 and it is difficult to find out fractures at the friction welding interfaces. 6) The cracking mode of SUS 303, SUH 3-303 is intergranular in any case, but SUH 3 is fractured by transgranular cracking.

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Evaluation of Ultrasonic Nonlinear Characteristics in Artificially Aged Al6061-T6 (인공시효된 Al6061-T6의 초음파 비선형 특성 평가)

  • Kim, Jongbeom;Lee, KyoungJun;Jhang, Kyung-Young;Kim, ChungSeok
    • Journal of the Korean Society for Nondestructive Testing
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    • v.34 no.3
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    • pp.220-225
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    • 2014
  • Generally, the nonlinearity of ultrasonic waves is measured using a nonlinear parameter ${\beta}$, which is defined as the ratio of the second harmonic's magnitude to the power of the fundamental frequency component after the ultrasonic wave propagates through a material. Nonlinear parameter ${\beta}$ is recognized as an effective parameter for evaluating material degradation. In this paper, we evaluated the nonlinear parameter of Al6061-T6 which had been subjected to an artificial aging heat treatment. The measurement was using the transmitted signal obtained from contact-type transducers. After the ultrasonic test, a micro Vickers hardness test was conducted. From the result of the ultrasonic nonlinear parameter, the microstructural changes resulting from the heat treatment were estimated and the hardness test proved that these estimates were reasonable. Experimental results showed a correlation between the ultrasonic nonlinear parameter and microstructural changes produced by precipitation behavior in the material. These results suggest that the evaluation of mechanical properties using ultrasonic nonlinear parameter ${\beta}$ can be used to monitor variations in the mechanical hardness of aluminum alloys in response to an artificial aging heat-treatment.

The Effect of Solid Fraction on the Casting Formability in Vertical Type Squeeze Casting Process

  • Seo, Pan-Ki;Sohn, Sung-Man;Kang, Chung-Gil
    • Journal of Korea Foundry Society
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    • v.28 no.1
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    • pp.41-44
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    • 2008
  • 레오다이캐스팅 공정은 용탕상태의 원소재로부터 최종형상에 가장 가까운 정형제품(near-net shape)을 원하는 기계적 성질과 동시에 경제적으로 생산할 수 있는 제조방법으로 개발되어 왔다. 본 논문에서는 전자교반 시스템을 이용하여 결정립이 제어된 반용융 상태의 소재를 수직형 다이캐스팅기를 사용하여 리어파트(rear parts) 자동차 부품을 성형실험 하였다. 성형된 시제품들은 성형조건에 따른 조직 및 인장강도를 관찰하였으며, 시효경화 시간에 따른 T6 최적 열처리 조건을 조사하였다.

Weld Cracking of High Strength Al-Zn-Mg Alloy Weldment (용접구조용 7000 계열 고장력 Al-Zn-Mg 합금의 용접특성과 용접균열에 관한 고찰)

  • 김환태;황선효;남수우
    • Journal of Welding and Joining
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    • v.12 no.1
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    • pp.28-37
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    • 1994
  • 본 소고에서는 Al-Zn-Mg 계통의 고강도 알루미늄합금의 제조과정에서 실시하는 열처리 공정을 통해 얻어지는 시효경화 효과, 합금원소 첨가에 따른 석출물의 생성과 이에 따른 석출경화 효과와 용착금속의 응고균열 발생과의 상호관계를 조사하고 용접열영향부의 용질원자 확산과 입계의 liquid film에 의한 액화(liquation) 균열의 생성을 분석하여 설명하고자 한다.

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Evolution of Mechanical Properties through Various Heat Treatments of a Cast Co-based Superalloy (주조용 코발트기 초내열합금의 열처리에 따른 기계적 특성 변화)

  • Kim, In-Soo;Choi, Baig-Gyu;Jung, Joong-Eun;Do, Jeong-Hyeon;Jung, In-Yong;Jo, Chang-Yong
    • Journal of Korea Foundry Society
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    • v.38 no.5
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    • pp.103-110
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    • 2018
  • The effects of a heat treatment on the carbide formation behavior and mechanical properties of the cobalt-based superalloy X-45 were investigated here. Coarse primary carbides formed in the interdendritic region in the as-cast specimen, along with the precipitation of fine secondary carbides in the vicinity of the primary carbides. Most of the carbides formed in the interdendritic region were dissolved into the matrix by a solution treatment at $1274^{\circ}C$. Solutionizing at $1150^{\circ}C$ led to the dissolution of some carbides at the grain boundaries, though this also caused the precipitation of fine carbides in the vicinity of coarse primary carbides. A solution treatment followed by an aging treatment at $927^{\circ}C$ led to the precipitation of fine secondary carbides in the interdendritic region. Very fine carbides were precipitated in the dendritic region by an aging heat treatment at $927^{\circ}C$ and $982^{\circ}C$ without a solution treatment. The hardness value of the alloy solutionized at $1150^{\circ}C$ was somewhat higher than that in the as-cast condition; however, various aging treatments did not strongly influence the hardness value. The specimens as-cast and aged at $927^{\circ}C$ showed the highest hardness values, though they were not significantly affected by the aging time. The specimens aged only at $982^{\circ}C$ showed outstanding tensile and creep properties. Thermal exposure at high temperatures for 8000 hours led to the precipitation of carbide at the center of the dendrite region and an improvement of the creep rupture lifetimes.

The Effects of Solution Heat Treatment and Aging Treatment on the Electrical Conductivity and Hardness of Cu-Cr Alloys (크롬동합금의 도전율과 경도에 미치는 용체화처리와 시효처리의 영향)

  • Kim, Shin Woo
    • Journal of the Korean Society for Heat Treatment
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    • v.15 no.1
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    • pp.21-24
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    • 2002
  • The electrode materials for welding machine in automobile industry such as Cu-Cr, Cu-Zr and Cu-$Al_2O_3$ require the high electrical conductivity and the proper hardness. Therefore the effects of solution heat treatment and aging treatment on the electrical conductivity and hardness of Cu-0.8wt%Cr and Cu-1.2wt%Cr alloys have been investigated. Cu-0.8wt%Cr alloy showed the higher electrical conductivity and hardness than Cu-1.2wt%Cr alloy and both alloys showed the better electrical conductivity at $930^{\circ}C$ among 930, 980 and $1030^{\circ}C$ solution heat treatment temperatures. The electrical conductivity and hardness in both alloys were not affected by aging treatment but remarkably affected by solution heat treatment temperature. The final drawing process reduced electrical conductivity and increased hardness more in Cu-1.2wt%Cr alloy.

Age Hardening and Mechanical Property of Extruded Al-Zn-Mg-(Cu) Al Alloys with Sc addition (Sc 첨가된 Al-Zn-Mg-(Cu)계 알루미늄 합금 압출재의 시효 경화 거동과 기계적 성질)

  • Shim, Sung Yong;Lim, Su Gun
    • Journal of the Korean Society for Heat Treatment
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    • v.20 no.5
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    • pp.243-249
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    • 2007
  • The age hardening behavior and mechanical properties of an extruded Al-Zn-Mg-(Cu)-0.1 wt.%Sc alloy were investigated with the Sc addition and ageing temperature. The results showed that the $Al_3Sc$ compounds were formed by Sc addition and distributed preferentially along the extrusion direction. The age hardening of Al-Zn-Mg-Cu-0.1 wt.%Sc alloy which was treated by T6 process was more significant than that of Al-Zn-Mg-0.1 wt.%Sc alloy. The tensile property of Al-Zn-Mg-Cu+0.1 wt.%Sc alloy was also higher than that of Al-Zn-Mg-0.1 wt.%Sc alloy, which is 691 MPa and 584 MPa in strength and 9% and 11% in elongation, respectively.