• Title/Summary/Keyword: 순도

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Optimization of Precipitation Process for the Recovery of Lactic Acid (Lactic acid 회수를 위한 침전공정 최적화)

  • Choi, Kook-Hwa;Chang, Yong-Keun;Kim, Jin-Hyun
    • KSBB Journal
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    • v.26 no.1
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    • pp.13-18
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    • 2011
  • In this study, precipitation process was developed for the recovery of the lactic acid from calcium lactate fermentation broth. Calcium lactate yield was improved by decreasing the solubility of calcium lactate through the addition of ethanol (25%, v/v) as a co-precipitant. The optimal lime type, lime concentration, stirrer speed, precipitation time, temperature, and solvent amount for $Ca(LA)_2$ precipitation were CaO, 0.0175 g/mL, 220 rpm, 24 h, $5^{\circ}C$, ethanol 25% (v/v), respectively. Lactic acid was easily and efficiently recovered from precipitated $Ca(LA)_2$ by adding sulfuric acid ($Ca(LA)_2/H_2SO_4$ molar ratio=1:1). In the model solution of organic acids and fermentation broth, the overall yields of recovered lactic acid were 62% and 55%, respectively, under the aforementioned optimal conditions.

형광 발광층과 인광 발광층으로 구성된 하이브리드 발광층을 가진 청색 유기발광소자의 색 순도와 색안정성 증진

  • Bang, Hyeon-Seong;Chu, Dong-Cheol;Kim, Tae-Hwan;Seo, Ji-Hyeon;Kim, Yeong-Gwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.272-273
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    • 2011
  • 유기발광소자는 차세대 디스플레이 소자로서 빠른 응답 속도, 높은 색 재현성 및 매우 얇은 두께로 제작이 가능한 장점을 가지고 있어서 차세대 디스플레이 소자로서 많은 응용 가능성을 가지고 있다. 청색 유기발광소자는 적색 및 녹색의 유기발광소자의 발광 효율 특성보다 상대적으로 효율이 떨어지고, 색 순도가 낮으며 수명이 짧은 단점을 가지고 있어 소자 특성을 개선해야 한다. 본 논문에서는 청색 유기발광소자의 색 순도와 색 안정성 증진을 위하여 발광층을 2개의 층으로 나누어 15 nm 두께의 4,4'-Bis(2,2-diphenyl-ethen-1-yl)diphenyl (DPVBi) 형광 청색 호스트 물질에 4,4 '-Bis[4-(diphenylamino)stylyl]biphenyl (BDAVBi) 형광 청색 게스트 물질을 첨가하여 제 1 형광 발광층을 형성하고 15 nm 두께의 4,4'-Bis(carbazol-9-yl)biphenyl (CBP) 인광 호스트 물질에 bis(3,5-difluoro-2-(2-pyridyl)phenyl-(2-carboxypyridyl)iridium III (FIrpic) 인광 게스트 물질을 첨가한 제 2 인광 발광층으로 구성된 30 nm 두께의 하이브리드 발광층을 사용하여 청색 유기 발광소자를 제작하고 전기적 특성과 광학적 성질을 조사하였다. 하이브리드 발광층을 사용하여 제작된 유기발광소자는 20 mA/cm2의 전류 밀도에서 6.2 cd/A의 발광 효율을 나타내었고, 최대 밝기는 약 16,200 cd/m2로 측정 되었다. 하이브리드 발광층을 사용한 청색 유기발광소자는 전류의 흐름이 단일 발광층 유기발광소자에 비교하여 상대적으로 안정적인 전류 흐름을 가지며 발광층 내부에 더 많은 정공과 전자를 포획하여 엑시톤 형성 확률이 증가하여 발광효율과 밝기가 향상되었다. 하이브리드 발광층을 적용한 유기발광소자는 469 nm파장에서 형광 발광층의 주 전계발광 피크가 나타났고 그와 함께 인광 발광층의 부 전계발광 피크가 491 nm의 파장에서 관측되었다. 또한 전계발광 스펙트럼의 반치폭이 10 nm 감소하여 청색의 색 순도 증가에도 기여하였다. 하이브리드 발광층을 가진 청색 유기발광소자의 색 좌표는 전압 변화에 관계없이 일정한 값을 나타내었다. 이러한 결과는 형광과 인광 발광층으로 구성된 하이브리드 발광층 유기발광소자가 전기적으로 안정성을 가지며 발광 특성을 개선하고 안정적인 청색 유기 발광 디스플레이 소자로 사용 가능함을 나타내고 있다.

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Food Nutritional Composition of Castor Aralia (Kalopanax pictus N) Sprouts (음나무(Kalopanax pictus N) 순의 식품학적 성분 분석)

  • Choi, Hye-Jin;Kim, Do-Hee;Chung, Hun-Sik;Moon, Kwang-Deog
    • Food Science and Preservation
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    • v.19 no.5
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    • pp.720-726
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    • 2012
  • This study was carried out to investigate the food value of K. pictus sprouts. The total ginsenoside content was 67.4 mg/kg. Including Ginsenoside Rg1, a total of five different types were detected by the experiment. The total phenol content was 33.77 mg/100 g. Including seven different type of essential amino acids, the total amino acid content of K. pictus sprouts was 33,744 mg/100 g. The results of the analysis of the free amino acid content showed that the total bitterness was much higher than the total sweetness. From the above results, the food characteristics of K. pictus sprouts could be determined. To improve their consumption, their bitterness must be reduced.

Water resource vulnerability assessment of South Korea using hydrological model (수문 모형의 활용을 통한 국내 수자원 취약성 평가)

  • Won, Kwang Jai;Chung, Eun-Sung;Kim, Soo Hyun
    • Proceedings of the Korea Water Resources Association Conference
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    • 2015.05a
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    • pp.264-264
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    • 2015
  • 최근 기후변화는 우리 삶에 다양한 영향을 미치고 있으며, 이에 따른 수문순환 변화 역시 자명하게 받아들이고 있다. 이에 따라 수자원 취약성 평가 및 대책에 관한 연구는 다양하게 진행되고 있는 실정이다. 하지만 국내의 경우 전체 유역에 대한 수자원 취약성 평가 연구는 부족한 실정이다. 따라서 본 연구에서는 국내 총 12 수계인 한강, 안성천, 금강, 삽교천, 영산강, 섬진강, 탐진강, 만경강, 동진강, 낙동강, 태화강, 형산강 유역에 대한 수자원 취약성 평가를 실시하였다. 평가 방법으로는 장기간에 걸친 다양한 토양의 특징, 토지이용, 관리상태의 변화에 따른 크고 복잡한 유역의 유출량을 추정하기 위해 개발된 SWAT(Soil and Water Assessment Tool) 모형을 이용하여 수문 모형을 구축하였고, 유출 관련 매개변수 최적화 작업은 SWAT-CUP 모형을 이용하였다. 최적화된 매개변수의 적용을 통해 각 유역별 유출량을 산정하였다. 그 결과 2009년과 2011년은 한강, 낙동강, 금강, 영산강순 이였으며, 2010년은 낙동강, 한강, 금강, 영산강순 이였다. 면적별 유출량인 비유량(specific discharge)을 산정한 결과, 2009년에는 영산강, 낙동강, 금강, 한강순 이며, 2010년에는 영산강, 금강, 낙동강, 한강순 이였으며, 2011년에는 금강, 한강, 영산강, 낙동강 순을 보였다. 또한, 인구당 유출량 산정 결과 2009년에는 영산강, 금강, 낙동강, 한강순 이며, 2010년에는 영산강, 금강, 낙동강, 한강순 이며, 2011년에는 영산강, 금강, 낙동강, 한강순 이었다. 이를 바탕으로 국내 총 12 수계에 대한 수자원 취약성을 산정해보았다. 대응변수는 이수의 수요 및 공급적인 측면에서 구분하였으며, 사회/경제, 물 이용, 환경, SWAT으로 구성하였습니다. 수자원 취약성 평가를 위해 다기준의사결정기법(MCDM, Multi-Criteria Decision Making) 중 하나인 TOPSIS(Technique for Order of Preference by Similarity to Ideal Solution)기법을 사용하였다. 산정 결과 삽교천, 동진강, 형산강, 안성천, 섬진강, 만경강, 낙동강, 영산강, 태화강, 금강, 한강, 탐진강 순 이였다. 본 연구 결과는 향후 다중 공간에 구축한 고해상도 모형을 통해 국내 수문상황 진단 및 고해상도 미래 수문 시나리오 생산을 통한 수자원 관리에도 활용될 전망이며, 기후변화 취약성 평가를 위한 지표 개발에 이용될 예정이다.

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A study on the fabrication of high purity lithium carbonate by recrystallization of low grade lithium carbonate (저급 탄산리튬의 재결정화를 통한 고순도 탄산리튬 제조에 대한 연구)

  • Kim, Boram;Kim, Dae-Weon;Hwang, Sung-Ok;Jung, Soo-Hoon;Yang, Dae-Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.31 no.1
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    • pp.16-23
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    • 2021
  • Lithium carbonate recovered from the waste solution generated during the lithium secondary battery manufacturing process contains heavy metals such as cobalt, nickel, and manganese. In this study, the recrystallization of lithium carbonate was performed to remove heavy metals contained in the powder and to increase the purity of lithium carbonate. First, the leaching efficiency of lithium carbonate according to pH in the aqueous hydrochloric acid solution was examined, and the effect on the recrystallization of lithium carbonate according to the equivalent and concentration of sodium carbonate was confirmed. As the equivalent and concentration of sodium carbonate increased, the recovery rate of lithium carbonate improved. And the SEM image showed that the crystal shape was changed depending on the reaction conditions with sodium carbonate. Finally, the high purity lithium carbonate of 99.9% or more was recovered by washing with water.

Direct MR Arthrography of the Hip: Diagnosis and Pitfalls of Acetabular Labral Lesions (고관절 직접 자기공명관절조영술: 비구순 병변의 진단 및 함정)

  • Eun Sol Lim; Yong Kyun Kim;Hye Mi Park;Seung Jin Lee
    • Journal of the Korean Society of Radiology
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    • v.82 no.5
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    • pp.1140-1162
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    • 2021
  • Tearing of the acetabular labrum is a common cause of chronic hip pain. MR arthrography (MRA) of the hip is the imaging procedure of choice for the evaluation of acetabular labrum. Familiarity with the various imaging findings of MRA of the hip allows recognition of normal variants and differentiation from true pathologic conditions. This article comprehensively reviews the technical aspects and interpretation of MRA of the hip. The appearances of normal and abnormal labra in MRA are discussed. Potential pitfalls in labral tear interpretation, such as sulci around the hip, normal variants of the labrum and plicae, and osseocartilaginous and soft tissue lesions identified on MRA of the hip are also described.

A Study on the Status of Utilization and Criteria for Selection of Medical Care Facilities of Elementary School Children (초등학생들의 의료기관 이용양상 및 선택 기준에 관한 연구)

  • Han, Seung Pyo;Kim, Eun Young;Rho, Young Il;Yang, Eun Seok;Park, Sang Kee;Park, Yeong Bong;Moon, Kyung Rye
    • Clinical and Experimental Pediatrics
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    • v.45 no.2
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    • pp.166-173
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    • 2002
  • Purpose : The aim of this study is to find out the distribution of illness, patterns of medical care utilization and factors determining medical care utilization in elementary school children. Methods : We performed the questionnaires in Gwangju city on 2,036 children of two elementary schools from June 1 to June 30, 1998. Results : The prevalence rate of illness was 32.3%. The distribution of illness was respiratory disease(64.7%), gastrointestinal disease(12.8%), injury & poisoning. The rate of persons having received medical treatment when they were sick, was 89.8%. The selection distribution among various medical facilities was pediatric hospital(46.7%), otolaryngologic hospital(19.8%), pharmacy (13.2%) and internal medicine in the decreasing frequency sequence. The major factors influencing the selection of medical facility were geographic accessibility and good results. The most common reason for the first visit to the pediatric hospital was geographic accessibility. The most common reason for a visit and to otolaryngologic hospital was a good result. The most frequently utilized medical facility for respiratory symptoms and gastrointestinal symptoms was pediatric hospital. The persons influencing the selection of medical facility in the children were mother(73.3%), father( 10.8%), doctor and others in decreasing sequence. The persons answering the questionaire thought that the optimal age of pediatric care was from 0 to 12 years(47.8%), to 10 years(22.4%) and to 15 years(18.5%) in decreasing rate. Conclusion : Other departments instead of pediatrics have treated children. Children have particular growth and development process, which is different to those of adults. So, it is necessary to choose special medical care and adequate medical facilities for children.

Studies on Inorganic Components of Korean Wild Edible Mushrooms - Trace Mineral Elements of Armillariella Mella, Hygrophorous russula, Armillariella tabescens, Lepista nuda and lepista sordida, Hygrocybe conica. - (한국산 야생(野生) 식용버섯의 무기성분에 관한 연구 - 뽕나무버섯, 뽕나무버섯부치, 벚꽃버섯, 민자주방망이버섯, 자주방망이버섯아재비, 붉은산무명버섯의 미량금속원소 -)

  • Park, Wan-Hee
    • The Korean Journal of Mycology
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    • v.21 no.4
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    • pp.273-278
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    • 1993
  • In order to determine of trace mineral elements of wild edible mushrooms in Korea, the dried carpophores of Armillariella mella(Vahl.ex Fr.) karst., Armillariella tabescens(Scop.) Sing., Lepista nuda(Bull.ex Fr.) Cooke and Lepista sordida(Schum.ex Fr.) Sing., Hygrophorus russula (Schaeff.ex Fr.) Qu'el., Hygrocybe conica(Scop.ex Fr.) Kummur were incinerated and analyzed by an atom adsorption spectrophotometry. The six mushrooms contained ubiquitously potassium, iron, zinc, sodium, manganase, copper and calsium in that order, and the content of potassium was the highest than other inorganic components and the content of zinc in Hygrocybe conica was especially the most than the other five mushrooms. Total contents of inorganic components(except Cd) were universally the highest in Hygrocybe conica than other five mushrooms, and decrease in order Hygrophorus russula, lepista nuda, lepista sordida, Aarmillariella mella and Armillariella tabescens. Calsium was not present in Amillariella mella and lepista nuda, and copper not in Hygro­cybe conica, and content of cadimium in Hygrophorus russula and Hygrocybe conica were trace.

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Gene Flow of Oriental Fruit Moth, Grapholita molesta, Populations Analyzed by RAPD Molecular Markers (RAPD 분자지표를 이용한 복숭아순나방(Grapholita molesta)의 집단 유전적 변동 분석)

  • Son, Ye-Rim;Kim, Yong-Gyun
    • Korean journal of applied entomology
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    • v.47 no.1
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    • pp.37-44
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    • 2008
  • Oriental fruit moth, Grapholita molesta, is a serious pest on apples. To control this pest in an environmentally friendly method, mating disruption strategy using sex pheromone has been developed. Area-wide application of mating disruption has been needed to be effective, with little understanding on how much size of apple cultivating area should be treated in one time application of the mating disruption technique. On this matter, we needed to determine a minimal mating active zone of G. molesta that should be applied with mating disrupters to be effective. Molecular markers to discriminate a specific population should be developed to trace population migration for reproductive behaviors. Here we developed two effective molecular markers using random amplified polymorphic DNA (RAPD) technique. Different field populations of G. molesta, based on locations and seasons, were analyzed with these markers. In a specific location, G. molesta populations varied in genetic composition with different seasons. Different local populations showed differential variation according to their relative distances among apple orchards. In overall, genetic variation among different populations became lessen with progression of seasons.