• 제목/요약/키워드: 수정진동자

검색결과 101건 처리시간 0.026초

Measurement of Water Absorption in Anticorrosive Organic Coatings Using Quartz Crystal Microbalance (QCM) (수정진동자 미세저울을 이용한 방식도막의 물 흡수 측정)

  • 이근대;도윤정;김진호;박성수;홍성수;서차수;박진환
    • Journal of Ocean Engineering and Technology
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    • 제17권6호
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    • pp.77-82
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    • 2003
  • The absorption of water into an anti-corrosive organic coating, such as alkyd and urethane resin coating, was investigated, using a quartz crystal microbalance (QCM). Anticorrosive properties of the coatings were also measured, by means of electrochemical impedance spectroscopy (EIS). The overall absorption of water in the coating is determined by the chemical nature of resin, and decreases with increasing thickness. The enhancement of anti-corrosive performance, through increase of coating thickness, was more remarkable in the case of the coating that hadlower equilibrium water absorption. The absorption kinetics curves were Fickian in nature. The EIS analysis confirmed that the resin, having lower equilibrium water absorption, shows higher anti-corrosive performan.

On-Line Measurement of Solid Particles in Air Using a Quartz Crystal Microbalance (수정진동자 미량저울을 이용한 공기 중 먼지의 온라인 측정)

  • Choi, Kwang-Jae;Kim, Young-Han;Chang, Sang-Mok
    • Journal of Sensor Science and Technology
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    • 제8권4호
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    • pp.314-319
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    • 1999
  • The measurement of solid particles suspended in air is conducted with a quartz crystal microbalance. The measurement system is connected to a personal computer and multiple sensors are utilized to make simultaneous measurement possible. In this paper, the detail of experimental setup is extensively explained for the possible future application of the system in other areas. It is found that the measurement system is suitable for an on-line continuous determination of the concentration of solid particles in air.

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Development of high-speed near-field scanning optical microscopy by using a high-frequency quartz-crystal resonator (고주파 수정진동자를 이용한 고속 근접장 광학 현미경 제작)

  • 서용호;제원호
    • Proceedings of the Optical Society of Korea Conference
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    • 한국광학회 2001년도 제12회 정기총회 및 01년도 동계학술발표회
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    • pp.120-121
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    • 2001
  • 고분해능을 장점으로 하는 근접장 광학 현미경(NSOM)은 최근 높은 관심을 모으고 있으나, 그 촬영 속도가 너무 느린 이유로 실제적인 활용이 미비한 상황이다. scanning 속도를 높이고자 하는 노력들이 많이 진행되고 있으나[1-2] 아직도 실시간 촬영과는 거리가 멀다. 기존의 근접장 광학 현미경(NSOM)은 tuning fork를 사용하여 탐침을 진동시키고 그 진동의 진폭 또는 위상의 변화를 측정함으로써 탐침과 시료의 거리를 측정하는 방식을 사용한다. (중략)

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Utilization of Domestic Natual Quartz as Elecrtic Resonators; Feasibility Study (한국산 천연수품을 이용한 수품공진자의 생산가능성에 관한 연구)

  • Choe, Se-Gon;Jeong, Gi-Ho;Lee, Mu-Yeong
    • Journal of the Korean Institute of Telematics and Electronics
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    • 제13권3호
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    • pp.11-15
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    • 1976
  • 한국산 천연수정은 보석장식용으로서는 그 품질이 이미 알려져 있으나 수정진동자로서의 특성에 관해서는 아직 보고된 바가 없다. 본 연구는 특히 경상도일대에서 채굴되고 있는 천연수정을 채집, 선별, 가공하여 그 수정진동자로서의 사용가능성을 실험을 통하여 검토한 것이다. 필자들은 채굴현장 근처에서 채집한 원석을 특별히 고안제작된 검사경을 이용하여 분석선별하였으며 X-ray를 사용하여 AT-cut로 orientation 한후 시판을 절단하였다. 다음 적용하여 전기적, 광학적 쌍수상태를 검토하고 다시 선별하였다 Dimensioning은 5MHz를 목표로 하였는데 연잠제를 사용하여 5MHz의 조도까지 연마하고 전극으로서 표준형의 은막을 부착하여 시판을 완성하였다. 시판을 대한 측정결과는 모든 등가정수가 대표적인 수입수정판의 것과 대등하였으며 특히 Q는 모두 105를 넘었다. 온도특성도 AT-cut의 이론치와 대차가 없었으며 -20℃-+100℃ 범위에서 최대 20PPM 이내의 편차를 보였다. 즉, 한국산 천연수정은 적절히 선별, 가공 한다면 부유한 수정진동자의 원재로서 사용할수 있음이 증명되었다. Samples of domestic natural quartz were collected and screened optically and chemically, and, after weeding out portions unfit for electrical resonator, were cut into AT-cut wafers, which in turn were dimensioned, trimmed and lapped into 5MHz resonator units. The results of measurements obtained from the specimens indicated excellent electrical characteristics of domestic natural quartz with the average Q quotient of 10s or higher. Temperature characteristics also showed typical AT-cut corves with the frequency deviation of 20PPM at maximum throughout the range of -20 to 100℃. The experiment on the initial batch of samples amply indicates the excellent electrical quality of domestic natural quartz as quartz resonator units.

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Direct measurement technique of the oscillation amplitude of a quartz tuning fork in atomic force microscopy (AFM용 수정진동자 진동폭의 직접 측정 기술)

  • Kim, Jeong-Hoi;Han, Hae-Wook
    • Proceedings of the IEEK Conference
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    • 대한전자공학회 2006년도 하계종합학술대회
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    • pp.645-646
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    • 2006
  • The oscillation amplitude of a probe tip is an important parameter to determine the resolution of atomic force microscopy (AFM) techniques. In this work, we introduce a new method for the measurement of the oscillation amplitude of a quartz tuning fork tip sub-nanometer resolution.

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Analysis of the Redox Reaction for Polypyrrole Thin Film by Using a Quartz Crystal Analyzer (수정진동자 분석기(QCA)를 이용한 폴리피롤 박막의 산화-환원반응 해석)

  • Chang, Sang-Mok;Kim, Jong-Min;Park, Ji-Sun;Son, Tae-Il;Hiroshi, Muramatsu
    • Applied Chemistry for Engineering
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    • 제9권1호
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    • pp.44-51
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    • 1998
  • In this work, the in-situ viscoelastic characteristics of electropolymerized polypyrrole (PPy) thin film were investigated in the electrolyte solutions of $NaClO_4$, $LiClO_4$, and $KClO_4$ by using quartz crystal analyzer (QCA). One side of quartz crystal was used as a working electrode mounted in a special fabricated QCA electrochemical ceil. The resonant frequency and resonant resistance diagram (F-R diagram) was used to interpret the viscoelastic characteristics of Pby thin film and compared with AFM photograph. The resonant frequency, resonant resistance, and current were measured to analyze the redox reaction behaviors when the cyclic voltammetry was performed using AT-cut quartz crystal electrode coated with galvanostatically polymerized Ppy film. The result suggests that the Ppy film polymerized onto the crystal behaves as a rigid elastic layer at the initial stage of electropolymerization, while the film becomes a viscoelastic layer the polymerization proceeds further. At the same time, the film thickness increases and some morphological changes take place due to the penetration of electrolyte solution into the film. These phenomena take place when cyclic voltammetry was performed using different electrolyte solution compared with polymerization process.

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Development of Red-Tide Prediction Technique Using Quartz Crystal Oscillator (수정진동자를 이용한 적조예측 방법의 개발)

  • Kim, Byoung-Chul;Kim, Young-Han;Chang, Sang-Mok
    • Journal of Navigation and Port Research
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    • 제28권6호
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    • pp.573-578
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    • 2004
  • The most important effects on algae multiplication are coming from maintaining the growth environment such as necessary nutrients and proper temperature, but it is difficult to adjust for every species individually. In this study, therefore, the environment is obtained using the local water where target organisms live, and their growth is promoted by raising the water temperature. A sensor to count the organism population is developed here. Because the early stage of a sudden increase of the algae population is detected using the sensor, it is available to predict the sudden increase of algae, a source of red tide.

Measurement of Adsorption Characteristic Using a Quartz Crystal Resonator (수정진동자를 이용한 흡착특성의 측정)

  • Kim, Byoung Chul;Sung, Ick Gi;Yamamoto, Takuji;Kim, Young Han
    • Korean Chemical Engineering Research
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    • 제47권3호
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    • pp.368-372
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    • 2009
  • A technique to measure the adsorption characteristic of surface area and pore size distribution is proposed and its performance is examined. While the existing equipment utilizes liquid nitrogen, the proposed uses carbon dioxide at the room temperature leading to the small measuring device with easy operation and short measurement time. The performance of the device has been examined with micro-particle carbon cryogel and bamboo activated carbon. The results from the proposed device compared with those of the adsorption apparatus indicate that the measurement of meso-porous material is comparable but micro-porous material gives some error.