• Korean Journal of Dental Materials
• /
• v.44 no.3
• /
• pp.207-216
• /
• 2017

The effect of cooling rate on precipitation hardening of a Pd-Cu-Ga-Zn metal-ceramic alloy during porcelain firing simulation was investigated and the following results were obtained. When the cooling rate was fast (Stage 0), the hardness of the alloy increased at each firing step and the high hardness value was maintained. When the cooling rate was slow (Stage 3), the hardness was the highest at the first stage of the firing, but the final hardness of the alloy after complete firing was lower. The increase in hardness of the specimens cooled at the cooling rate of Stage 0 after each firing step was caused by precipitation hardening. The decrease in hardness of the specimens cooled at the cooling rate of Stage 3 after each firing step was attributed to the coarsening of the spot-like precipitates formed in the matrix and plate-like precipitates. The matrix and the plate-like precipitates were composed of the $Pd_2(Cu,Ga,Zn)$ phase of CsCl-type, and the particle-like structure was composed of the Pd-rich ${\alpha}$-phase of face-centered cubic structure. Through the porcelain firing process, Cu, Ga, and Zn, which were dissolved in Pd-rich ${\alpha}$ particles, precipitated with Pd, resulting in the phase separation of the Pd-rich ${\alpha}$ particles into the Pd-rich ${\alpha}^{\prime}$ particles and ${\beta}^{\prime}$ precipitates composed of $Pd_2(Cu,Ga,Zn)$. These results suggested that the durability of the final prosthesis made of the Pd-Cu-Ga-Zn alloy can be improved when the cooling rate is fast during porcelain firing simulation.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.18 no.6
• /
• pp.1455-1464
• /
• 1994

A new and efficient algorithm for the integration of the thermal-elasto-plastic constitutive equation is proposed. While it falls into the category of the return mapping method, the algorithm adopts the three point approximation of plastic corrector within one time increment step. The results of its application to a von Mises-type thermal-elasto-plastic model with combined hardening and temperature-dependent material properties show that the accurate iso-error maps are obtained for both angular and radial errors. The accuracy achieved is because the predicted stress increment in a single step calculation follows the exact value closely not only at the end of the step but also through the whole path. Also, the comparison of the computational time for the new and other algorithms shows that the new one is very efficient.

• Proceedings of the Optical Society of Korea Conference
• /
• 2009.10a
• /
• pp.255-267
• /
• 2009

PDP용 형광체는 소성 후 입자간 결합부족으로 인한 탈락현상 및 셀 결함 불량과 Red, Green, Blue 간 유전율 불일치로 인한 방전불량 현상 등의 문제점을 안고 있다. PDP용 형광체의 소성 후 입자간의 결합력을 증진시키기 위하여 frit을 조제로 첨가하였고, 이에 따른 기계적, 전기적, 광학적 특성의 변화를 조사하였다. 사용된 frit은 자체 소결시 무색의 투명하고 ZnO-$B_2O_3-SiO_2-Al_2O_3$계 비정질 세라믹 재료이며, 연화점은 $499.78^{\circ}C$이다. 형광체 중량의 3${\sim}$20wt% 범위에서 frit의 첨가량 변화에 따른 영향을 조사하였다. Frit의 첨가량이 증가할수록 경도가 증진 되었고, 5wt% 미만 함유될 경우 Red, Green, Blue 형광체 모두 유전율 조절 효과가 미약하였다. Red 형광체는 frit함량이 3wt% 이상 함유되면 휘도가 90% 미만으로 감소하였고, Green과 Blue는 frit 함량이 10wt%이상 함유되면 확연하게 휘도가 감소 하였다.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2002.05a
• /
• pp.70-73
• /
• 2002

Using a simple compression test, the viscosity measurement experiment is carried out with the grain-refined Al-Si alloy(A356). The measured rheological data are expressed with power-law(Ostwald-de Waele) model and using commercial package, MAGMAsoft, coefficients of Ostwald-de Waele model and Carreau-Yasuda model are calculated. To verify the viscosity data, the die is designed to be applicable to the semi-solid die casting of automotive component and filling test is carried out. The filling test and the simulation result are compared and in good agreement. Hereafter, these data are considered to be usefully allied other product in the semi-solid die casting.

• Transactions of Materials Processing
• /
• v.8 no.2
• /
• pp.188-199
• /
• 1999

Semi-Solid Forming Process(Thixoforming, Rheocasting) is a novel forming process which has some advantages compared with conventional die casting, squeeze casting and hot/cold forging. In this study. Thixoforming process was selected as analysis processing in terms of billet handling and easiness of automation process. The Thixoforming process consists of reheating process of billet, billet handling, filling inot the die cavity and solidification of SSM part. In filling process, two rheology models which were Newtonian and Non-Nettonian model (Ostwald-deWaele)were verified with experimental results. The Ostwald-deWaele model shows the good agreement to the real flow and filling phenomena in die cavity. To give a boost the economical efficiency of Thixoforming process and to ensure the good forming result, reheating device coupled die set was proposed and the initial billet temperature for system that was found from experimental resluts. This study presents an overview of application of numerical analysis for simulation of semi-solid metal forming process to reduce the lead time for development of manufacturing part in industrial field.

• Transactions of Materials Processing
• /
• v.24 no.2
• /
• pp.83-88
• /
• 2015

For chromaticity correction, it is necessary to dispense high viscosity phosphor slurry since it greatly affects the performance of white LEDs. However, it is quite difficult to dispense high viscosity fluorescent materials. In the current study, micro-discharge electrostatic printing has been used for dispensing various high viscosity phosphor slurries. We have achieved dispersions of up to 50 µg using drop on demand (DOD) discharge experiments. The experiments were conducted with different combinations of process variables such as applied voltage, pneumatic pressure, and frequency.

• Proceedings of the Membrane Society of Korea Conference
• /
• 1995.10a
• /
• pp.54-55
• /
• 1995

현재 수처리용 분리막으로 널리 사용되고 있는 상업용 polyamide membrane은 주사슬을 이루고 있는 amide bond가 chlorine에 쉽게 분해됨으로써 주쇄의 절단이 일어나므로 막이 파괴되는 결과를 초래하여 역삼투 분리막의 기능이 저하되는 문제점을 갖고 있다. 또한 분리막의 성능으로써 수투과도의 향상도 기존의 분리막의 개선점으로 지적되고 있다. 본 연구에서는 재료 자체의 친수성이 강한 hydroxyl group을 가진 vinyl계 화합물을 기존의 amine계 monomer와 혼합하여 가교반응을 시킴으로써 전체적인 분리막의 수투과도 및 내염소성의 향상을 도모하였다. 기존의 polyamide 분리막의 소재인 1,3-phenylenediamine(MPDA)에 친수성기인 hydroxyethylmethacrylate(HEMA) monomer를 첨가하고 가교제인 trymesoyl chloride(TMC)로 이를 가교시켜 HEMA 및 PVA의 친수성에 의한 수투과도 및 내염소성의 향상을 유도하여 보았다.

• Transactions of Materials Processing
• /
• v.3 no.4
• /
• pp.401-414
• /
• 1994

Springback for the three point bending is anlayzed and experimented. Neutral axis is assumed to remain at the midthickness for large ratio of radius of curvature to thickness. Pure bending theory is used to be extended to the analysis of the springback for three point bending. The specimen is thought to be divided into numerous small elements. The theory for pure bending is then adopted for analysis of each element to obtain springback in terms of the relationship between initial and final deflections. the boundary conditions between neighborhood elements are the deflection and slope which should be the same. Deflection is calculated by summing up the deflections of each element. Experiments have been performed for different conditions which are punch radius, span length, and initial deflections. Comparisons between the analytical solution and experimental results show the same trends.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2009.05a
• /
• pp.458-461
• /
• 2009

Thermo-mechanical simulation of the Friction Stir Spot Welding (FSSW) processes was performed for the AA5083-H18 sheets, utilizing commercial Finite Element Method (FEM) and Finite Volume Method (FVM) which are based on Lagrangian and Eulerian formulations, respectively. The Lagrangian explicit dynamic FEM code, PAM-CRASH, and the Eulerian Computational Fluid Dynamics (CFD) FVM code, STAR-CD, were utilized to understand the effect of pin geometry on weld strength and material flow under the unsteady state condition. Using FVM code, material flow pattern near the tool boundary was analyzed to explain the weld strength difference between the weld by cylindrical pin and the weld by triangular pin, while the frictional energy concept using the FEM code had limitation to explain the weld strength difference.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2007.10a
• /
• pp.223-227
• /
• 2007

New forming technologies are being introduced to automotive manufacturing processes. Among them, a simultaneous forming is one of the innovative forming technologies to be able to reduce production time and cost. Several parts can be simultaneously manufactured by the process, while the conventional stamping demands the same number of die sets with the number of parts. In this study, the automotive rear floor side member was manufactured by the simultaneous forming. The position and the size of initial blank were determined by forming analyses and try-outs, and the blank movement during the forming was controlled by introducing the spotweld.