• Title/Summary/Keyword: 상온혼합

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The Effect of Native Oxide on the $TiSi_{2}$ Transformation after HF Cleaning (HF 세정후 자연 산화막의 존재가 티타늄 실리사이드 형성에 미치는 영향)

  • Bae, Jong-Uk;Hyeon, Yeong-Cheol;Yu, Hyun-Kyu;Lee, Jeong-Yong;Nam, Kee-Soo
    • Korean Journal of Materials Research
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    • v.8 no.5
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    • pp.464-469
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    • 1998
  • HF 세정후 자연 산화막의 존재가 급속 열처리 장비를 이용, 아르곤 분위기에서 열처리할 때 티타늄 실리사이드 형성을 관찰하였다. 고분해능 단면 투과 전자 현미경 관찰 결과 기판 온도가 상온일 때 자연산화막(native oxide)이 존재함을 확인하였으며 기판 온도가 40$0^{\circ}C$일 때는 실리콘 기판과 티타늄 박막의 계면 부위에서 자연산화막, 티타늄 및 실리콘이 혼합된 비정질층이 존재함을 확인하였다. 티타늄을 증착하는 동안 기판 온도를 40$0^{\circ}C$로 유지했을 때는 C54~$TiSi_2$상이 형성되는데 요구되는 급속 열처리(Rapid Thermal Annealing : RTA)온도가 기판 온도를 상오느로 유지 했을 때보다 $100^{\circ}C$정도 감소함을 확인하였다. 이 같은 결과는 산소불순물을 함유한 비정질 층이 핵생성 자리를 제공하여 이 상의 형성이 촉진된다는 사실을 말한다. 기판온도 $400^{\circ}C$에서 형성된 티타늄 실리사이드막의 경우 비저항 $\mu$$\Omega$cm임을 확인하였다.

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AN EXPERIMENTAL STUDY ON PULPAL RESPONSE TO THE SELP-CURING RESIN FOR THE DIFFERENCE OF MIXING TIMES IN CAT (상온중합(常溫重合) 레진의 혼합시간(混合時間) 차이(差異)에 따른 성묘(成描)의 치수(齒髓反應)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Lee, Hyun-Shick;Woo, Y.H.;Park, Nam-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.27 no.1
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    • pp.213-222
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    • 1989
  • It is considered that self-curing resin will induce a little pulpal irritation, if mixing time is insufficient. So this study was designed to compare four different conditions between control group and three experimental groups. Canine teeth of 20 cats used, and class V cavities were prepared on maxillary canine of cats. Control group was filled with zone and other experimental groups were filled with zone after the application of the self-curing resin. Animals of the experimental and control group were sacrified at 3 days, 1, 2, 3, 4 weeks after the experiment. The finding lead to the following conclusions ; 1. Odontoblasts of first and third experimental groups were condensed irregularly and were changed at early stage, and reapir was delayed. 2. Odontoblasts of second experimental group were condensed slightly but, histologic repair was appeared at 4 weeks after the experiment 3. In all groups, the damaged odontoblastic cell layer were eventually disappeared at 4 weeks after the experiment.

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Resistivity Analysis of Model Block for Using of Structure Grounding Electrode (구조체접지극 활용을 위한 모형블록의 저항률 분석)

  • Kim, Sung-Sam;Jeong, Man-Gil;Choi, Jong-Kyu;Koh, Hee-Seog
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.21 no.2
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    • pp.40-45
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    • 2007
  • This study analyzed the resistivity characteristic of model block to make the good use of structure grounding and substitution grounding electrode base of building. After making the model block of mortar and concrete block, it measured resistivity in hydrous condition and dry condition and compared with the blocks that is mixed earth resistance lowering agent to decrease resistivity. The resistance value of block accepted much influence by block resistivity. When the block resistivity was same or similar value, the value of soil resistivity has occurred as different as the value of grounding resistance.

Improvement of Pot Life in the Epoxy Resin-based Adhesive Formulation by Size Control and Coating of Curing Accelerator Powders (경화촉매 분말의 입도조절 및 표면코팅에 의한 에폭시 레진 기반 혼합조성의 상온 보관특성 개선)

  • Lee, Jun-Sik;Hyun, Chang-Yong;Lee, Jong-Hyun
    • Journal of Powder Materials
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    • v.15 no.2
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    • pp.119-124
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    • 2008
  • To increase pot life in the formulation mixed with bisphenol F epoxy resin, anhydride-based curing agent, and imidazole-based curing accelerator powders as a paste material for high-speed RFID chip bonding, size variation of the imidazole-based powders and a coating method of the powders were adopted in this study. In experiment with regard to the size variation, the pot life was not outstandingly increased. Through the idea using the coating method, however, the pot life was increased up to 4.25 times in comparison with the addition of initial imidazole-based powders. Consequently, successive bonding of RFID chip could be performed with very short time of 5sec using the suggested formulation having improved pot life.

국제 수학 올림피아드 참가 후보자들을 위한 상황대처훈련에 관한연구

  • 김보경;조성희;이군현
    • Proceedings of the Korean Society for the Gifted Conference
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    • 1994.08a
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    • pp.1.2-37
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    • 1994
  • Currently Korea encourages gifted high schoolers and junior high schoolers to participate in international achievement contests such as International Olympiads. Participants for these contests are selected nationwide among gifted students in areas of mathematics, physics, chemistry, and others. They go through a series of screening tests and programs. One of the screening processes IS Korean Olympiad School, which provides study programs each summer for student-candidates prior to following year's International Olympiads. Approximately 40 students of high schools and junior high schools, in each subject of study, gather at Korean Olympiad Summer School, and they go through intensive study programs during a short period of time. Out of 40 candidates,' less than 10 students are finally selected to participate in International Olympiads. In this study, a psycho-educational program called "Situation Coping Training Program" was developed to enhance ahievement motivation for these student-candidates. This study was to see if this training program actually improved their cognitive, emotive motivation factors, and to see how this training program affected their achievement level. Training was administered for five days. This training program was found effective for participants to increase self-efficacy, internal locus of control, and anxiety copmg. These cognitive and emotive motivation factors, other than intelligence, were found to have positive relationship with achievement level, of which self-efficacy and attribution style of students were found as two best predictors of achievement. This training program was perceived as necessary. by participants, and helpful for recovering self-confidence and self-control as well as coping pressure. Suggestions were made that this kind of training program be administered as a regular curriculum in preparative study programs such as Korean Olympiads, since cognitive, emotive motivation factors are related with achievement, and furthermore, be utilized in all gifted education programs in Korea. in Korea.

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Evaluation of Physiological Changes in Watermelon Stalk during Storage under Various Conditions of Treatments after Harvesting (수확 후 저장환경에 따른 수박줄기의 생리변화)

  • Park, Shin;Kang, Sun-Chul
    • Korean Journal of Environmental Agriculture
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    • v.24 no.1
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    • pp.56-60
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    • 2005
  • In order to increase the storage stability of watermelon stalk, storage environments such as temperature and other treatments such as vaseline, mixture of soybean oil and wheat flour, and coated paper label were tested separately after harvesting. At different storage temperatures (7, 18 and $30^{\circ}C$) shelf-life of stalk was inversely proportional to temperature. The results showed that during storage at $30^{\circ}C$ they were completely wilted in 7 days, at $18^{\circ}C$ in 15 days and at $7^{\circ}C$ in 19 days. Our data also showed that stability of watermelon stalk depending on temperature was very closely correlated with water content of watermelon stalk; during storage at $30^{\circ}C$ the water content of watermelon stalk was decreased to 21.1 % in 7 days, whereas at $7^{\circ}C$ the water content was decreased gradually to 71.2 % for 19 days of storage. In order to reduce the physiological changes in watermelon stalk at $30^{\circ}C$, following treatments such as vaseline, mixture of soybean oil and wheat flour, and coated paper label were tested. As a result, watermelon stalk without any treatment was completely wilted in 9 days, while stalks treated with vaseline and mixture of soybean oil with wheat flour were wilted in 15 and 12 days, respectively. The wilt delay was noted in the watermelon stalk for $3{\sim}6$ days during both treatments but the outward quality was found detracted, whereas when treated with coated paper label, the wilt of stalk was delayed for 3 days along with the improvement in the outward quality. Therefore this data indicate that the treatment of coated paper label during storage at $30^{\circ}C$ can be considered as a potent method for maintaining the physiology of watermelon stalk.

Strength Properties According to the Conditions of Low Carbon Inorganic Composite Using Industrial By-product (산업부산물을 사용한 저탄소 무기결합재의 조건별 강도특성)

  • Lee, Yun-Seong;Lee, Sang-Soo;Song, Ha-Young
    • Journal of the Korea Institute of Building Construction
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    • v.12 no.1
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    • pp.54-63
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    • 2012
  • The purpose of this study is to examine the potential for reducing the environmental load and $CO_2$ gas when cement is produced by using cement substitutes. These substitutes consisted of blast furnace slag, red mud and silica fume, which were industrial by-products. The most optimum mix was derived when alkali accelerator was added to low carbon inorganic composite mixed with industrial by-product at room temperature. It is determined that hardened properties and the results of compressive strength tests changed based on CaO content, Si/Al, the mixing ratio and the amount of alkali accelerator, curing conditions and W/B. The results of test analysis suggest that the optimum mix of low carbon inorganic composite is CaO content 30%, Si/Al 4, the mixed ratio of alkali accelerator $(NaOH:Na_2SiO_3)$ 50g:50g, the amount of alkali accelerator 100g and W/B 31%. In addition, if contraction is complemented, low carbon inorganic composite with superior performance could be developed.

Thermal Properties of Polyurethane Elastomers Prepared with MBCA/DMTDA Mixture as Curing Agent (MBCA/DMTDA 혼합경화제를 이용한 폴리우레탄 탄성체의 열적 성질)

  • Ahn, Won Sool
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.6
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    • pp.670-675
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    • 2016
  • Both melting temperature and enthalpy of MBCA/DMTDA mixtures were measured as a function of DMTDA compositions using DSC. The thermal properties of polyurethane elastomer samples prepared with MBCA, DMTDA, and 40/60 MBCA/DMTDA mixture as curing agents were also observed using TGA. MBCA and DMTDA showed good miscibility over the entire composition range, exhibiting individual DSC melting peaks. Peak temperatures were non-linearly reduced as DMTDA concentrations increased, being approximately $60^{\circ}C$ in the case of the 40/60 MBCA/DMTDA mixture. Furthermore, melting enthalpy of the mixture was calculated as 3.8 J/g, which was only 4.3% compared to 87.3 J/g of MBCA. Based on these results, crystallization of the mixture was considered to occur very slowly, and the fluidic gel-state of the mixture was visually confirmed to be maintained over 5 days at room temperature. Thermal decomposition of polyurethane elastomer prepared with 40/60 MBCA/DMTDA curative started at about $190^{\circ}C$, which is similar to that observed for DMTDA, only except decomposition behavior over higher temperature of $400^{\circ}C$.

Dried Noodle Making of Composite Flours Utilizing Buckwheat and Wheat Flour (메밀가루와 밀가루 복합분의 건면 제조시험)

  • Kim, Yong-Soon;Kim, Hyong-Soo
    • Journal of Nutrition and Health
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    • v.16 no.3
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    • pp.146-153
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    • 1983
  • In this study, buckwheat four was classified by the order of extraction from the inmost layer to the outmost layer, and was designated as $B_1,\;B_2,\;B_3,$ and the mixed flour of $B_1,\;B_2,\;B_3$ (1:1:1) was named $B_0$. To improve the dried noodle-making properties, various levels of strong wheat flour and additives such as sodium alginate (SA) and xanthan gum(XG) were added to buckwheat. 1) The buckwheat $B_2$ and $B_3$ flours contained much higher amounts of crude ash, protein and fat than the $B_1$ flour. 2) Buckwheat $B_3$ flour demonstrated lower maxium viscosity value by amylograph than the $B_1$ flour, but it demonstrated 2 times higher maximum viscosity value than wheat flour. Buckwheat $B_1$ flour demonstrated 4-5 times higher maximum viscosity value than wheat flour. Addition of SA and XG increased the viscosity of the flour mixtures. 3) It was possible to make dried noodles from the composite flour of (buckwheat 40 %+wheat 60 %). The lesser the quantity of buckwheat flour was, the better the kneading property of mixed flour was. 4) SA and XG, which were added at the level of 1.0-1.5%, significantly improved dough making properties and the cooking quality of the noodles.

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Effect of Hydrogen(H2) Addition on Flame Shape and Combustion Products in Mixed Coflow Diffusion Flames of Methane(CH4), Ethane(C2H6) and Propane(C3H8) (동축류 메탄(CH4), 에탄(C2H6), 프로판(C3H8) 혼합 확산화염내의 수소(H2) 첨가가 화염 형상 및 연소 생성물에 미치는 영향)

  • Park, Ho-Yong;Yoon, Sung-Hwan;Rho, Beom-Seok;Lee, Won-Ju;Choi, Jae-Hyuk
    • Journal of the Korean Society of Marine Environment & Safety
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    • v.25 no.6
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    • pp.780-787
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    • 2019
  • As a carbon-free, green growth alternative, internal and external interest in hydrogen energy and technology is growing. Hydrogen was added to co-axial methane, methane-propane, and methane-propane-ethane diffusion flames, which are the main ingredients of LNG, to evaluate its effect on flame formation and combustion products. The variation in combustion products produced by adding hydrogen gradually to diffusion pyrolysis at room temperature and normal pressure conditions was observed experimentally by using a gas analyzer, and the shape of diffusion pyrolysis was observed step by step using a digital camera. The experimental results showed that the production volume of nitrogen oxides tended to increase and became close to linear as hydrogen was added to the diffusion pyrotechnic. This is because the relatively high temperature of heat insulation and fast combustion speed of hydrogen facilitated the production of thermal NOx. On the other hand, CO2 production tended to decrease as hydrogen was added to reduce the overall carbon ratio contained in the mixed diffusion flame of methane, methane-propane, and methane-ethane-propane. This means that the mixed fuel use of LNG-hydrogen in ships may potentially reduce emissions of CO2, a greenhouse gas.