• Title/Summary/Keyword: 비파괴평가 신뢰도

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Quality Control on Neutron Activation Analysis for Urban Dust by the Proficiency Test (비교숙련도 시험을 통한 도시대기분진에 대한 중성자방사화분석법의 품질관리)

  • Moon, Jong-Hwa;Kim, Sun-Ha;Chung, Yong-Sam
    • Analytical Science and Technology
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    • v.15 no.5
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    • pp.433-438
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    • 2002
  • Trace elements in two air filters (V-50, P-50) artificially loaded with urban dust provided from IAEA were determined non-destructively using instrumental neutron activation analysis. Standard reference material (Urban Particulate Matter, SRM 1648) of National Institute of Standard and Technology was used for analytical quality control. About 20 elements in both of loaded filter samples were determined. To evaluate inter-laboratory comparison and proficiency test, analytical data were statistically treated with the results which collected from 49 laboratories, 40 countries participated in this study using neutron activation analysis, particle induced X-ray emission, inductively coupled plasma mass spectroscopy, etc,. From the results of statistical treatment, Z-scores are within ${\pm}2$. Furthermore, accuracy and precision of obtained analytical values are passed according to the criteria of the proficiency test. Consequently, it was proved that analytical quality for air dust samples being performed has been controlled properly.

Comparative Study of NIR-based Prediction Methods for Biomass Weight Loss Profiles

  • Cho, Hyun-Woo;Liu, J. Jay
    • Clean Technology
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    • v.18 no.1
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    • pp.31-37
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    • 2012
  • Biomass has become a major feedstock for bioenergy and other bio-based products because of its renewability and environmental benefits. Various researches have been done in the prediction of crucial characteristics of biomass, including the active utilization of spectroscopy data. Near infrared (NIR) spectroscopy has been widely used because of its attractive features: it's non-destructive and cost-effective producing fast and reliable analysis results. This work developed the multivariate statistical scheme for predicting weight loss profiles based on the utilization of NIR spectra data measured for six lignocellulosic biomass types. Wavelet analysis was used as a compression tool to suppress irrelevant noise and to select features or wavelengths that better explain NIR data. The developed scheme was demonstrated using real NIR data sets, in which different prediction models were evaluated in terms of prediction performance. In addition, the benefits of using right pretreatment of NIR spectra were also given. In our case, it turned out that compression of high-dimensional NIR spectra by wavelet and then PLS modeling yielded more reliable prediction results without handling full set of noisy data. This work showed that the developed scheme can be easily applied for rapid analysis of biomass.

Evaluation of Beef Freshness Using Visible-near Infrared Reflectance Spectra (가시광선-근적외선 반사스펙트럼을 이용한 쇠고기의 신선도 평가)

  • Choi, Chang-Hyun;Kim, Jong-Hun;Kim, Yong-Joo
    • Food Science of Animal Resources
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    • v.31 no.1
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    • pp.115-121
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    • 2011
  • The objective of this study was to develop models to predict freshness factors (total viable counts (TVC), pH, volatile basic nitrogen (VBN), trimethylamine (TMA), and thiobarbituric acid (TBA) values) and the storage period in beef using a visible and near-infrared (NIR) spectroscopic technique. A total of 216 beef spectra were collected during the storage period from 0 to 14 d at a $10^{\circ}C$ storage. A spectrophotometer was used to measure reflectance spectra from beef samples, and beef freshness spectra were divided into a calibration set and a validation set. Multi-linear regression (MLR) models using the stepwise method were developed to predict the factors. The MLR results showed that beef freshness had a good correlation between the predicted and measured factors using the selected wavelength. The correlation of determination ($r^2$), standard error of prediction (SEP), and ratio of standard deviation to SEP (RPD) of the prediction set for TVC was 0.74, 0.64, and 2.75 Log CFU/$cm^2$, respectively. The $r^2$, SEP, and RPD values for pH were 0.43, 0.10, and 1.10; those for VBN were 0.73, 1.45, and 2.00 mg%; those for TMA were 0.70, 0.19, and 2.58 mg%; those for TBA values were 0.73, 0.13, and 2.77 mg MA/kg; and those for storage period were 0.77, 1.94, and 2.53 d, respectively. The results indicate that visible and NIR spectroscopy can predict beef freshness during storage.

Development of Post-installable Pullout Bolts and a Loading Device for Evaluating Concrete Strength (콘크리트 강도평가를 위한 인발장치와 후매입 인발볼트의 개발)

  • Ko, Hune-Bum;Lee, Ghang;Won, Jong-Sung
    • Journal of the Korea Institute of Building Construction
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    • v.11 no.3
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    • pp.229-237
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    • 2011
  • The pullout test is a nondestructive testing method certified by the American Society for Testing and Materials (ASTM) and British Standards (BS). Research has shown that it is very reliable in terms of evaluating the concrete strength of reinforced concrete members. However, the pullout test is rarely performed on domestic construction sites due to the complex procedures and high costs involved. This study proposes a new pullout test composed of a post installable break-off bolt, an insert nut, and a pullout tester, which satisfy both economical and practical purposes on a construction site. Three different types of special fastening methods, a temporary fixed bolt, a plastic fixed panel, and a fixed bar, have been developed. A pullout tester is proposed that is driven by the circle force introduced into a handle composed of eight gears without a load cell and a hydraulic cylinder. The serviceability and reliability of these instruments were investigated through experiments at construction sites. Furthermore, the sample pullout test with a wall specimen was conducted to estimate the usefulness of the temporary fixed bolt type of fastening methods and pullout devices. Eventually, the developed instruments will be useful on construction sites if minor requirements are met.

Assessment of Impact-echo Method for Cavity Detection in Dorsal Side of Sewer Pipe (하수관거 배면 공동 탐지를 위한 충격반향법의 적용성 평가)

  • Song, Seokmin;Kim, Hansup;Park, Duhee;Kang, Jaemo;Choi, Changho
    • Journal of the Korean Geotechnical Society
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    • v.32 no.8
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    • pp.5-14
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    • 2016
  • The leakage of water under sewer pipelines is one of main sources of sinkholes in urban areas. We performed laboratory model tests to investigate the presence of cavities using impact-echo method, which is a nondestructive test method. To simulate a concrete sewer pipe, a thin concrete plate was built and placed over container filled with sand. The cavity was modeled as an extruded polystyrene foam box. Two sets of tests were performed, one over sand and the other on cavity. A new impact device was developed to apply a consistent high frequency impact load on the concrete plate, thereby increasing the reliability of the test procedure. The frequency and transient characteristics of the measured reflected waveforms were analyzed via fast Fourier transform and short time Fourier spectrum. It was shown that the shapes of Fourier spectra are very similar to one another, and therefore cannot be used to predict the presence of cavity. A new index, termed resonance duration, is defined to record the time of vibration exceeding a prescribed intensity. The results showed that the resonance duration is a more effective parameter for predicting the presence of a cavity. A value of the resonance period was proposed to estimate the presence of cavity. Further studies using various soil types and field tests are warranted to validate the proposed approach.

Strength Prediction Equations for High Strength Concrete by Schmidt Hammer Test (슈미트 해머 시험에 의한 고강도 콘크리트의 강도 추정식)

  • Kwon, Young-Wung;Park, Song-Chul;Kim, Min-Su
    • Journal of the Korea Concrete Institute
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    • v.18 no.3 s.93
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    • pp.389-395
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    • 2006
  • For the assessment of exsiting concrete structures, it is important to get the real strength of concrete. The load test or core test has many problems due to cost time, easiness, structural damage, and reliability and so on. Thus, various non-destructive test and statistical analysis techniques for strength assessment have been developed. As a result the real strength of concrete can be obtained by both direct and indirect test. In this study, a series of experimental tests of core strength and Schmidt hammer tests on 3, 7, 14, 28, 90, 180, 365, and 730 days' were done for predicting the compressive strength of high strength concrete with 65.0MPa of 28-days' strength. Each experimental results was analyzed by simple regression analysis. Then, reliability level and error rate between the proposed equations and the existing ones was examined. However, the application of the exsisting equations was inadequate to high strength concrete, because they were conducted under normal strength concrete. Therefore, the following compressive strength equations were proposed for predicting the compressive strength of high strength concrete by Schmidt hammer test. The proposed equations by Schmidt hammer test are as follows.

Evaluation of Flexible Pavement Layer Moduli Using the Depth Deflectometer and Flexible Pavement Behavior under Various Vehicle Speeds (아스팔트 콘크리트 포장구조체의 내부처짐에 의한 물성추정과 주행속도에 따른 거동분석)

  • Choi, Jun-Seong;Kin, Soo-Il;Yoo, Ji-hyung
    • International Journal of Highway Engineering
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    • v.2 no.1
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    • pp.135-145
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    • 2000
  • A new procedure needs to be developed to predict the dynamic layer properties under moving truck loads. In this study, a computer code to evaluate layer moduli of asphalt concrete pavement from measured interior deflections at various depths were developed and verified from numerical model tests. Interior deflections of the pavement are measured from Multi-Depth Deflectometer(MDD). It was found that errors between the given and backcalculated moduli in numerical analysis were less than 0.32% for several numerical models tested. When impact loads were used, a technique to determine the depth to virtual rigid base was proposed through the analysis of compressive wave velocity and impulse loading durations. It was found that errors between the given and backcalculated moduli in numerical analysis were less than 0.114% when virtual rigid base was considered in numerical analysis. The pavement behavior must be evaluated under various vehicle speeds when determining the dynamic interaction between the loading vehicle and pavement system. To evaluate the dynamic behavior on asphalt concrete pavement under various vehicle speeds, truck moving tests were carried out. From the test results with respect to vehicle speed, it was found that the vehicle speed had significant effect on actual response of the pavement system. The lower vehicle speed generates the higher interior deflections, and the lower dynamic modulus.

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Reliability Assessment and Prediction of Solder Joints in High Temperature Heaters (고온히터 솔더접합부의 신뢰성 평가 및 예측)

  • Park, Eunju;Kwon, Daeil;Sa, Yoonki
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.2
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    • pp.23-27
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    • 2017
  • This paper proposes an approach to predict the reliability of high temperature heaters by identifying their primary failure modes and mechanisms in the field. Test specimens were designed to have the equivalent stress conditions with the high temperature heaters in the field in order to examine the effect of stress conditions on the solder joint failures. There failures often result from cracking due to intermetallic compound (IMC) or void formation within a solder joint. Aging tests have been performed by exposing the test specimens to a temperature of $170^{\circ}C$ in order to reproduce solder joint failures in the field. During the test, changes in IMC formation were investigated by scanning electron microscopy (SEM) on the cross-sections of the test specimens, while changes in void formation were monitored both by resistance spectroscopy and by micro-computed tomography (microCT), alternately. The test results demonstrated the void volume within the solder increased as the time at the high temperature increased. Also, the phase shift of high frequency resistance was found to have high correlation with the void volume. These results implied the failure of high temperature heaters can be non-destructively predicted based on the correlation.

Evaluation of the Nonlinearity Parameter in Unbound Material for Asphalt Concrete Pavement using Field-NDT Equipment (현장 도로평가장비를 이용한 입상재료층의 비선형 재료상수 추정에 관한 연구)

  • Seo, Joo Won;Choi, Jun Seong;Kim, Soo Il
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.2D
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    • pp.227-234
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    • 2008
  • This study examines which models are more suitable for representing mechanical property of unbound materials to analyze behavior of asphalt pavement structure. Results from FWD (Falling Weight Deflectometer) test were used to apply to nonlinear elastic model. The new method which can deduct material constants of nonlinear elastic model is suggested from FWD test data rather than laboratory resilient modulus ($M_R$) test. It is confirmed that the material constants are within the common range in subbase. Test output from FWD and MDD (Multi-Depth Deflectometer) was used to verify reliability of the model. From the results of verification, this study shows that a non-linear elastic model agrees to MDD test data more than a linear elastic model does.

Analysis of the Manufacturing Techniques for the KwangDahoe Tying on the Sword in Joseon Dynasty (조선시대 도검 패용 광다회의 제작기법 분석)

  • Baek, Je-Sun;Chung, Kwang-Young
    • Korean Journal of Heritage: History & Science
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    • v.50 no.3
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    • pp.64-87
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    • 2017
  • Dahoe is a traditional braid in Joseon Dynasty. There are many Dahoe artifacts, which can give us a glimpse of the costume, culture, and life of that era. The study of Dahoe is necessary in various fields, but it is difficult because this manufacturing technique has been passed down from hand to hand. Few studies have been done so far. This research examines the manufacturing technique of KwangDahoe which is passed down by Maedeupjang (Decorative Knotting) and is generally used for knotting and/or tying objects. The main characteristic of TieKwangDahoe, made through the same method as WonDahoe, is the square hole in the middle. It was impossibile to remake the original braid because there is no confirmed number of the strand. Especially it is very difficult to do conservation and restoration on serious degradation state of the fiber. Therefore, it is necessary to analyze the non-destructive manufacturing techniques method for Dahoe and assess their applicability. First, we analyzed the artifacts' manufacturing technique based on the database of the Dahoe's manufacturing technique. In order to do that, we undertook schematization, restoration, morphological analyzation of the Dahoe. And then, X-ray CT scans were performed to improve the reliability of the DB. These results of scanning were interpreted based on the manufacturing technique. The selected Tie-KwangDahoe on the sword for the study are artifacts including artistic value and symbolism in Joseon Dynasty. Based on the analysis of the manufacturing technique, we found that both artifacts were made of 20-strand braid of single cross according to the length-scale measure. It was manufactured using 8-strand on left-right side, 12-strand on front-back side by the braiding manufacturing technique method Finally, this research suggests non-destructive analysis method of Dahoe's manufacturing technique is based on the database and the analysis results. I hope this research can be useful in various professional fields of Dahoe in the future. Moreover, I hope this can be of any help in preserving Korean cultural heritage.