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Contents character of phthalates in school supplies (학용품 중 프탈레이트류 함유특성 연구)

  • Kim, Kyeo-Keun
    • Analytical Science and Technology
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    • v.25 no.1
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    • pp.69-75
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    • 2012
  • This study was performed to survey the school supplies such as pencil, eraser, notebook and color paper. Twenty-two kinds of samples were collected near the school zone, and eight kinds of phthalate which is one of the environmental hazard factors analyzed to estimate the contents characteristics of products. As the results of these research, three kinds of phthalates (BBP, DNOP and DIDP) were not detected in the selected samples. In the A group, DEHP and DINP were detected in the rage of 22%~28%, and DINP was selected 28%, 24% and 28% in the A-1, A-3 and A-4 samples, respectively. But the selected samples in the B group were detected less than 1,000 ppm as regulated level. Also, The DBP was detected 1% in the C-2 sample, and DEHP was detected 0.3% in the C-1 and C-6 samples. The DEHA was detected 0.3% in the D-3 sample. In this study, the DINP was mainly detected the eraser, therefore this kind of phthalate can be exposed through dermal exposure.

Analysis of Multiple Pesticide Residues in Raw Materials Used in Dietary Supplements by GC/ECD and NPD (GC/ECD와 NPD를 이용한 건강기능식품 주요 원료 중 다성분 잔류농약 분석)

  • Park, Sun-Young;Oh, Sang-Suk
    • Korean Journal of Food Science and Technology
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    • v.36 no.6
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    • pp.863-871
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    • 2004
  • Analyses of residual pesticides in raw materials used for dietary supplements were performed using multi-ingredients simultaneous analysis method. Pesticides such as BHC, chlorpyrifos, and quintozene were detected in 12 domestic and 7 imported samples, suggesting need for monitoring pesticides in domestic and imported raw materials and establishing residual limit of each pesticide.

An Improved Proton Recoil Telescope Detector for Fast Neutron Spectroscopy

  • Chung, Moon-Kyu;Kang, Hee-Dong;Park, Tong-Soo
    • Nuclear Engineering and Technology
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    • v.5 no.3
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    • pp.191-201
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    • 1973
  • For fast neutron spectroscopy in MeV region, a recoil proton telescope detector was designed and constructed so as to increase in detection efficiency without appreciable deterioration in energy resolution by adopting a special type of recoil proton radiator which is a combination of a ring-shaped vertical radiator and a cone-shaped horizontal radiator at a certain geometry. A neutron stopper was built in the detector system to minimize the background due to direct exposure of the Si(Li) detectors to primary incident neutrons. The detection efficiency and the energy resolution calculated at various neutron energies and geometries are given and these characteristics of the detector system were tested by 14.1 MeV neutrons. As the calculation predicted, the relative detection efficiency in case of the combined radiator system is almost 2.2 times of that for a single, ring-shaped vertical radiator system. The calculated energy resolution is 3.7% FWHM, whereas the measured resolution was 3.9% which means resolution broadening of approximately. 30% was resulted by introducing a combined radiator system into the telescope. Increase in background less than 40% was also observed.

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Development and International Collaborations on Quantum Noise Reduction Technology for Gravitational Wave Detectors (중력파 검출기 양자잡음 저감기술 개발 및 국제협력)

  • Lee, Sungho;Kim, Chang-Hee;Park, June Gyu;Kim, Yunjong;Seong, Hyeon Cheol;Jeong, Ueejeong;Je, Soonkyu;Ra, Young-Sik;Gwak, Geunhee;Yoon, Youngdo;Go, Byeong Yoon;Kim, Hyunjin;Roh, Chan
    • The Bulletin of The Korean Astronomical Society
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    • v.46 no.2
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    • pp.60.2-60.2
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    • 2021
  • 중력파 관측은 2015년에 사상 최초로 검출에 성공한 이래, 불과 5년 만에 주 1 회 이상 안정적으로 검출되고 있으며 검출기들의 성능이 계속 향상됨에 따라 관측 범위와 빈도가 급격히 확대되는 추세에 있다. 이제 중력파는 전자기파 외에 우주를 보는 새로운 창으로서 확고한 지위를 구축하고 있으며 향후 무궁무진한 발전의 잠재력을 보여주고 있다. 이러한 가능성을 일찌감치 내다본 미국과 유럽의 선도 국가들은 현재 운영 중인 LIGO와 Virgo 검출기의 지속적인 업그레이드는 물론 Cosmic Explorer, Einstein Telescope 등 차세대 거대 검출기 개발을 병행해서 진행하고 있으며, 일본, 인도, 중국, 호주 등 후발주자들도 제각기 다양한 중력파 검출기 계획들을 추진하고 있다. 이에 한국천문연구원에서도 2019년부터 중력파 검출기술 연구를 시작하였으며, 특히 한국과학기술원 물리학과와 협력하여 차세대 핵심기술인 양자잡음 저감기술을 중점적으로 개발하고 있다. 이 발표에서는 본 연구팀의 최근 연구 진행상황을 요약하고 국제 중력파 검출기 공동개발 참여 현황을 소개한다.

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Determination of Sulfite Contents in Medicinal Herbs (생약재에 함유된 이산화황 함유량 조사)

  • 김충모;송병준;나환식
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.29 no.3
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    • pp.375-379
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    • 2000
  • 이산화황 함유량에 대해 한약재를 대상으로 실험하였으며, 한약을 달여서 탕으로 섭취하는 점을 감안하여 한약을 달인 액을 시료로 이산화황 함량을 조사하여 소비자들이 한약을 달여서 섭취하는 과정에 안전성을 검토하고자 실험을 실시하여 다음과 같은 결과를 얻었다. 생약재 중 이산화황 함유량은 국산 14건중 맥문동(16.9 ppm), 백작약(56.0), 산약(67.7)이 검출되었으며, 수입산은 13건 중 금은화(653.4 ppm), 길경(628.9), 반하(37.1), 백부근(11.7), 부자(82.4), 상백피 (82.7), 석창포(98.0), 패모(497.0),에서 이산화황이 검출되었다. 구입 시기 및 장소를 달리하여 구입한 생약재는 시기나 장소가 달라지면서 생약재에 함유된 이산화황 함량이 서로 차이가 있음을 알 수 있었다. 국산과 수임산과의 이산화황 함량 차이를 조사한 결과 국산의 경우에는 천화분 1건(29.5 ppm)을 제외한 나머지 시료에서 불검출을 보였으나, 수입산의 경우 13건중 7건(건지황, 과루인, 지실, 구기자, 남성, 우슬, 천화분)이 검출되어, 수입산이 국산보다 이산화황을 더 많이 함유하고 있는 것으로 나타났다. 약탕기로 한약액을 달여서 검사한 결과 최초 구입한 생약재의 함유량보다 이산화황 함량이 감소하는 경향을 보였으나, 원래 생약에 다량 함유되어 있는 경우에는 최종 잔류되는 함유량도 높게 나타났다.

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A Study of the Design of NIDS System for the Effective Information Detection (효율적인 정보검출을 위한 NIDS 시스템 설계에 관한 연구)

  • 이선근
    • Journal of the Korea Society of Computer and Information
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    • v.8 no.3
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    • pp.156-162
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    • 2003
  • With the network environment and user's application service increasing information protection and private information protection fields are very important fields. But it is necessary detection methodology to unspecified unknown signal, information increasing and various information media. Therefore in this thesis, we design NIDS that classify others information for detection of the unknown signal as the unauthenticated signal or illegal outer access, etc. proposed NIDS design used Synopsys Ver. 1999 and VHDL. The proposed NIDS system is practical in the system performance and cost for the individually existed NIDS, and utilized a part of system resources.

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Heavy Metal Contents in Ginseng and Ginseng Products (인삼 및 인삼제품류의 중금속 함량)

  • Hu, Soo-Jung;Kim, Mee-Hye;Park, Sung-Kug;Lee, Jong-Ok
    • Korean Journal of Food Science and Technology
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    • v.37 no.3
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    • pp.329-333
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    • 2005
  • Contents of heavy metals, mercury (Hg), lead (Pb), cadmium (Cd), arsenic (As), manganese (Mn), zinc (Zn), and copper (Cu), In ginsengs and ginsengs products their safety were evaluated using a mercury analyzer, atomic absorption spectrophotometer and Inductively coupled plasma spectrometer. Contents of heavy metals in ginsengs were [min-max(mean), mg/kg]; Hg 0.002-0.02(0.007), Pb 0.018-0.39(0.106), Cd 0.004-0.413(0.106), As ND-0.094(0.013), Cu 0.24-5.5(3.2), Mn 3.18-50.4(20.09), Zn 0.76-44.27(13.42). Ginseng products values were; Hg 0.0001-0.002(0.001), Pb 0.001-0.133(0.017), Cd ND-0.07(0.004) As ND-0.181(0.008), Cu ND-1.1(0.13), Mn 0.73-30.15(1.61). Zn 0.02-13.42(1.02), similar to those reported by other countries. Average weekly Intakes of Hg, Pb and Cd from ginseng and ginseng products were 0,003, 0.01 and 0,02% of provisional tolerable weekly intake established by FAO/WHO, respectively. Our result could be utilized as important references to establish the standard of lead in ginseng and ginseng products.

Trace Metal Contents in Fishes and Shellfishes and Their Safety Evaluatins (우리나라 어패류중 미량금속 함량 및 안전성 평가)

  • 소유섭;김정수;정소영;김미혜;홍무기
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.29 no.4
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    • pp.549-554
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    • 2000
  • This study was carried out to estimate the contents of trace metals in the fishes and shellfishes available on Korean markets. The maples were digested with acids, then analyzed by ICP (INductively Coupled Plasma Spectrometer) and AAS (Atomic Absorption Spectrometer) for the contents of lead (Pb), cadmium (Cd), arsenic (As), copper (Cu), manganese (Mn) and zinc (Zn). The contents of mercury (Hg) were determined using a mercury analyzer. The contents of trace metals [minimum~ maximum (mean), mg/kg] in fishes were as follows; Hg;0.004~0.500(0.082), Pb;N.D.~ 1.87 (0.29), Cd;N.D. ~0.094 (0.020), As;0.01~5045 (0.84), Cu;0.04~3.74 (0.66), Mn; N.D. ~7.56 (0.57), Zn;0.92~18.33(6.03). Those contents in shellfishes were as follows (mg/kg); Hg;N.D.~0.221 (0.029), Pb;0.01~1.51 (0.38), Cd;0.02~1.93 (0.51), As;0.18~3.07 study showed that trace metal contents in both fishes and shellfishes on our markets of lead, cadmium and mercury from fishes and shellfishes takes about 1~13% of PTWI(Provisional Tolerable Weekly Intakes) that FAO/WHO Joint Food Additive and Contaminants Committee has set to evaluate their safeties.

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A Study on Minimum Detection Limit of Environmental Radioactivity in HPGe Detector (HPGe 검출기에서 환경방사능측정의 검출하한치에 관한 연구)

  • Jang, Eun-Sung
    • Journal of the Korean Society of Radiology
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    • v.5 no.1
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    • pp.5-10
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    • 2011
  • Based on basic concept of detection limit, sample measurement time & background measurement time was considered, and MDA values according to background measurement time and sample measurement time in land samples(river soil, surface soil, drinking water, underground water, surface water, pine leaf, mugwort) analysis among environmental samples were compared. Seeing the water sample analysis result, it was shown that most of the samples were not detected, and most of the samples in land specimen analysis showed to be below the detection limit of "Ministry of Education, Science and Technology Announcement Je-2008-28-ho", but $^{137}Cs$ which is one of artificial radioactive nuclide was detected in some samples. It can be traced back to 1950s and 1960s when nuclear tests were carried out in atmosphere and catastrophic Chernobyl atomic power station accident that caused fallouts in the sky, and this is common level of detection that can be observed worldwide. Seeing the result that the $^{134}Cs$(which is a isotope of $^{137}Cs$, and it has relatively short half life) was not detected in all samples, it can be considered it doesn't affect to the operation of atomic power station.

The Formation of N-Nitrosamine in Kimchi and Salt-fermented Fish Under Simulated Gastric Digestion (김치 및 젓갈류의 인공소화시 N-Nitrosamine의 생성)

  • 김경란;신정혜;이수정;강현희;김형식;성낙주
    • Journal of Food Hygiene and Safety
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    • v.17 no.2
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    • pp.94-100
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    • 2002
  • This work was performed in order to examine the effect of nitrite, thiocyanate and ascorbic acid on formation of N-nitrosamine(NA) in kimchi, fermented anchovy and shrimp under simulated gastric digestion, in vitro. The contents of nitrate were 10.7~24.5 mg/kg in kimchi, 1.5~5.6 mg/kg in fermented anchovy, 1.0~2.0 mg/kg in fermented shrimp and those of nitrite were average 0.3 mg/kg in all analyzed samples. Dimethylamine and trirmethylarnine contents were 4.9~l5.4 mg/kg, 0.6~0.8 mg/kg in kimchi, 3.3~4.0 mg/kg, 1.9~2.8 mg/kg in fermented anchovy, 30.3~177.9 mg/kg, 4.4~21.3 mg/kg in fermented shrimp, respectively. The contents of N-nitrosodime -thylamine(NDMA) were in the range of 0.8~6.9 $\mu\textrm{g}$/kg in kimchi, 0~l.2 $\mu\textrm{g}$/kg in fermented anchovy and 0~0.9 $\mu\textrm{g}$/kg in fermented shrimp. After simulated gastric digestion, NDMA was increased about 1.5 times in all sample. In every nitrite added samples, the contents of NDMA were increased by 183.1 times in fermented shrimp and were detected 192.4 $\mu\textrm{g}$/kg and 220.9 $\mu\textrm{g}$/kg when it was treated with 4 mM and 8 mM of nitrite, respectively. NDMA, when above samples were added 8 mM nitrite and 6.4 mM thiocyanate, was increased about 1.5 times than control samples. The formation of NDMA was inhibited by 49.9~92.4% in all samples added 12.8 mM ascorbic acid compared with the control sample.