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Fabrication of $YBa_{2}Cu_{3}O_{7-x}$-Ag Composite Superconductors by Pyrophoric Synthetic Method (발화합성법에 의한 $YBa_{2}Cu_{3}O_{7-x}$-Ag 복합 초전도체 제조)

  • Yang, Seok-U;Kim, Chan-Jung;Hong, Gye-Won;Sin, Hyeong-Sik
    • Korean Journal of Materials Research
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    • v.8 no.12
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    • pp.1082-1089
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    • 1998
  • To obtain fine dispersion of Ag particles in $YBa_2$$Cu_3$$O_{7-y}$ (123) superconductors, 123 samples were made by pyrophoric synthetic method using malic acid and the subsequent solid- state reaction. As the pyrophoric synthetic powder was used as a precursor material, fine 123 powder of submicron size was produced in a short reaction time. The added $Ag_2$O was converted to metallic Ag during Pyrophoric reaction and it accelerated both the formation of 123 phase and the grain growth via the enhanced mass transfer. The Ag particles of the sample sintered using the pyrephoric synthetic powder were more finely dispersed in the 123 matrix, compared to those of the sample sintered using the mechanically mixed powder, attributing to the improvement of the superconducting properties.

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반도체 및 디스플레이 세정 공정용 $CO_2$ 클러스터 장비의 클러스터 발생 특성 분석

  • Choe, Hu-Mi;Jo, Yu-Jin;Lee, Jong-U;Kim, Tae-Seong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2013.02a
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    • pp.303-303
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    • 2013
  • 표면에 부착된 나노/마이크로 입자는 다양한 분야에서 오염물질로 작용한다. 특히 형상이 미세하고 공정 단계가 복잡한 반도체 및 디스플레이 등의 전자 소자 공정에서 미치는 영향이 크다. 따라서 입자상 오염물질의 제거에 관하여 상용화된 습식 세정 방법이 다양하게 존재하지만 표면 손상, 화학 반응, 부산물, 세정 효율 등 여러 가지 문제점이 있어 새로운 세정 방법이 요구된다. 이에 건식 세정 방법, 그 중에서도 입자의 충돌을 통해 제거하는 방법인 에어로졸 세정, 필렛 세정 등이 개발되었으나 마이크로 크기로 생성되는 입자로 인하여 형상의 손상이 크다. 따라서 본 연구에서는 나노 단위로 기체/고체 혼합물만 생성하여 세정하는 가스 클러스터 세정 방법을 이용하여 이러한 문제점을 해결하고자 하였다. 클러스터 세정 장비를 이용한 표면 처리는 충돌에 의한 제거에 기반한다. 따라서 생성 및 가속되는 클러스터로부터 대상으로 전달되는 운동량의 정도가 세정 특성에 영향을 미치며 이는 생성되는 클러스터의 크기에 종속적이다. 생성 클러스터의 크기 분포는 분사 거리, 유량, 분사 각도, 노즐 냉각 온도 등의 변수에 관한 함수이다. 따라서 본 연구에서는 $CO_2$ 클러스터를 이용한 세정 특성을 정의 및 제어하기 위하여 생성되는 클러스터 특성에 관하여 이론적, 수치 해석적, 실험적 연구를 수행하였다. 먼저, $CO_2$의 물리적 특성 및 이를 이용한 특정 크기 오염 물질을 제거하는데 요구되는 임계 클러스터 크기 계산을 이론적으로 구하였다. 이는 오염물질의 부착력과 클러스터의 운동량 전달에 의한 제거력의 비교를 통해 이루어졌다. 두 번째로 클러스터 크기분포를 수치 해석적으로 예측하기 위하여 각 조건에 대하여 유동해석을 수행하고 이를 통해 구해진 노즐 내 기체의 냉각 속도를 GDE (General Dynamic Equation) 계산에 대입하여 구하였다. 마지막으로 PBMS(Particle Beam Mass Spectrometer)를 이용하여 실험적으로 클러스터 크기분포를 각 조건에 대하여 구할 수 있었다. 또한 크기 분포 경향에 대한 간접적 확인을 위하여 포토레지스트가 코팅된 웨이퍼에 클러스터의 충격으로 생성된 크레이터 크기의 경향을 분석하였다. 이와 같은 방법에 의하여 생성되는 클러스터는 노즐의 유량 증가, 온도 상승에 각각 비례하여 작아지는 것을 확인할 수 있었다.

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Region-Based Moving Object Segmentation for Video Monitoring System (비디오 감시시스템을 위한 영역 기반의 움직이는 물체 분할)

  • 이경미;김종배;이창우;김항준
    • Journal of the Institute of Electronics Engineers of Korea CI
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    • v.40 no.1
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    • pp.30-38
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    • 2003
  • This paper presents an efficient region-based motion segmentation method for segmenting of moving objects in a traffic scene with a focus on a Video Monitoring System (VMS). The presented method consists of two phases: motion detection and motion segmentation. Using the adaptive thresholding technique, the differences between two consecutive frames are analyzed to detect the movements of objects in a scene. To segment the detected regions into meaningful objects which have the similar intensity and motion information, the regions are initially segmented using a k-means clustering algorithm and then, the neighboring regions with the similar motion information are merged. Since we deal with not the whole image, but the detected regions in the segmentation phase, the computational cost is reduced dramatically. Experimental results demonstrate robustness in the occlusions among multiple moving objects and the change in environmental conditions as well.

Influence of Electroless Ni-plated MWCNTs on Thermal Conductivity and Fracture Toughness of MWCNTs/Al2O3/Epoxy Composites (무전해 니켈도금된 다중벽 탄소나노튜브의 첨가가 알루미나강화 에폭시 복합재료의 열전도도 및 파괴인성에 미치는 영향)

  • Choi, Jeong-Ran;Lee, Young-Sil;Park, Soo-Jin
    • Polymer(Korea)
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    • v.37 no.4
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    • pp.449-454
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    • 2013
  • In this work, the effect of electroless Ni-plating of multi-walled carbon nanotubes (MWCNTs) on thermal conductivity and fracture toughness properties of MWCNTs/$Al_2O_3$/epoxy composites was investigated. The surface properties of the Ni-plated MWCNTs were determined by scanning electron microscopy (SEM), X-ray photoelectron spectrometry (XPS), and X-ray diffraction (XRD) analyses. Thermal conductivity was tested using a thermal conductivity measuring system. The fracture toughness of the composites was carried out through the critical stress intensity factor ($K_{IC}$) measurement. As a result, the electroless Ni-plated MWCNTs led to a significant change of surface characteristics of the MWCNTs. Thermal conductivity and fracture toughness of the MWCNTs/$Al_2O_3$/epoxy composites were greater than those of non-treated ones. These results were probably due to the improvement of intermolecular interaction between the Ni-MWCNTs and the matrix resins.

Sensitivity Analysis on PWR Reactivity Induced Accidents (가압경수로 반응도사고에 대한 민감도 분석)

  • Myung Hyun Kim;Un Chul Lee;Ki In Han
    • Nuclear Engineering and Technology
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    • v.14 no.3
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    • pp.122-137
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    • 1982
  • Analyzed is the sensitivity of reactor transient behavior to various reactor parameters during the reactivity induced accidents (RIA) of the Kori Unit 1. Included in the analysis is a partial spectrum of RIAs with relatively fast transients such as uncontrolled rod cluster control assembly bank withdrawl from a subcritical or low power startup condition and rod ejection accidents. The analysis can be performed generally in three steps: calculation of an average core power change, hot spot heat transfer calculation and DNBR (departure from nucleate boiling ratio) calculation. The computer codes used for the analysis are either developed based on the codes relevent to it. These codes are evaluated to be highly reliable. An extensive sensitivity analysis is performed to study the effects of various reactor design and operating parameters on the reactor transient behavior during the accidents. The assumptions and initial conditions used for the RIA analysis in the Kori Unit 1 FSAR (Final Safety Analysis Report) are reexamined, and the corresponding analysis results are reassessed, based on the sensitivity analysis results, to be conservative and reliable.

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Effects of Sizing Treatment of Carbon Fibers on Mechanical Interfacial Properties of Nylon 6 Matrix Composites (탄소섬유의 사이징처리가 탄소섬유/나일론6 복합재료의 기계적 계면 특성에 미치는 영향)

  • Park, Soo-Jin;Choi, Woong-Ki;Kim, Byung-Joo;Min, Byung-Gak;Bae, Kyong-Min
    • Elastomers and Composites
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    • v.45 no.1
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    • pp.2-6
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    • 2010
  • The sizing treatments of PAN-based carbon fiber surfaces were carried out in order to improve the interfacial adhesion in the carbon fibers/nylon6 composite system. The parameter to characterize the wetting performance and surface free energy of the sized fibers were determined by a contact angle method. The mechanical interfacial properties of the composites were investigated using critical stress intensity factor ($K_{IC}$). The cross-section morphologies of sized CFs/nylon6composites were observed by SEM. As the experimental results, it was observed that silane-based sizing treated carbon fibers showed higher surface free energies than other sizing treatments. In particular, the KIC of the sizing-treated carbon fibers reinforced composites showed higher values than those of untreated carbon fibers-reinforced composites. This result indicated that the increase in the surface free energy of the fibers leads to the improvement of the mechanical interfacial properties of carbon fibers/nylon6 composites.

A Study to Develop a Practical Probabilistic Slope Stability Analysis Method (실용적인 확률론적 사면안정 해석 기법 개발)

  • 김형배;이승호
    • Journal of the Korean Geotechnical Society
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    • v.18 no.5
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    • pp.271-280
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    • 2002
  • A probabilistic approach to identify the effects of uncertainties of soil strength parameters on searching a critical slip surface with the lowest reliability is introduced. In general construction field, it is impossible for the engineer to always gather a variety of statistical information of soil strength parameters for which lots of laboratory and in-situ soil testing are required and to use it with enough statistical knowledge. Thus, in order that the engineer may easily understand the probabilistic concept for the slope stability analysis, this study proposes a combined procedure to incorporate the engineering probabilistic tools into the existing deterministic slope stability analysis methods. Using UTEXAS 3, a slope stability analysis computer program developed by U.S. Army Corps of Engineers (U.S. COE), this study provides the results of this probabilistic slope stability analysis in terms of probability of failure or reliability index. This probabilistic method f3r slope stability analysis appears to yield more comprehensive results of slope reliability than does existing deterministic methods with safety factors alone.

A Study on the Method for Releasing the Internal Pressure of the Propane Cylinder caused by Liquid Expansion (액팽창을 고려한 프로판용기의 내압 해소방안에 대한 연구)

  • Yim, Sang-Sik;Jang, Kap-Man;Lee, Jin-Han;Park, Gi-Dong;Kim, Ki-Bum
    • Journal of the Korean Institute of Gas
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    • v.19 no.5
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    • pp.98-103
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    • 2015
  • Liquefied petroleum gas can be charged up to 85% of cylinder volume by enforcement regulations of safety control and business of liquefied petroleum gas act. The charged mass by enforcement regulations is considered by liquid expansion of internal liquefied petroleum gas at $65^{\circ}C$. But the temperature of liquid would not be suspended under $65^{\circ}C$ in a cylinder or portable vessel at certain situation. In the thermodynamics view point, the cylinder can be exposed to high pressure by liquid expansion. Consequently, it can be possible to potential risk such as physical explosion. Hence, this paper will offer a method of estimated internal pressure by liquid expansion at critical state in the closed system. Also, the structural factor which is given rise to volume increasement of cylinder is offered by experiment. This paper is expected as crucial reference for a cylinder design of liquefied petroleum gas.

3-D Slope Stability Analysis on Influence of Groundwater Level Changes in Oksan Landslide Area (지하수위 변화에 따른 옥산 산사태 지역의 3차원 사면안정성 해석)

  • Seo, Yong-Seok;Kim, Sung-Kwon;Lee, Kyoung-Mi
    • The Journal of Engineering Geology
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    • v.18 no.2
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    • pp.177-183
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    • 2008
  • In the study, we carried out a 3-D analysis to assess the influence of groundwater level changes on the slope stability, conducting a series of back-numerical analysis to delineate the critical line of the shear strength of the failure surface of a landslide, and a laboratory test to determine the geo-mechanical properties of soil samples. The analysis result shows that the shear strength determined by the laboratory test was distributed below the critical line of shear strength estimated by back-analysis. Differences between driving and resisting force were also analyzed in groundwater conditions of dry and saturation. It appeared that the stress gets greater towards the slope center of the landslide, and the debris mass moves downwards. According to the analysis, the factor of safety becomes 1 with the rise of foundwater level up to -0.85 m from the slope surface, while the slope tends to stay stable during dry seasons.

A Development of Dam Risk Analysis Model Using Bayesian Network Model in Hydrologic (Bayesian Network(BN) 모형을 활용한 수문학적 댐 위험도 해석 기법 개발)

  • Kim, Jin Young;Kim, Jin-Guk;Kwon, Hyun-Han
    • Proceedings of the Korea Water Resources Association Conference
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    • 2015.05a
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    • pp.501-501
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    • 2015
  • 댐과 같은 수공구조물의 치수능력부족은 구조물의 파손이나 붕괴로 직결되며, 대규모 재산피해와 인명피해가 불가피하다. 또한 최근 기후변화 현상에 의해 발생되고 있는 예상치 못한 큰 강우와 홍수는 댐 안전을 저하하는 요소로 간주되며, 복합적으로 발생시 댐의 치수능력이 크게 저하되어 댐 파괴에 영향을 미칠 가능성이 크다. 또한 ICOLD, 세계대댐회 등의 조사 결과 댐 파괴에 큰 영향을 미치고 있는 수문학적 요소로서 예상치 못한 강우, 홍수 및 월류로 조사되었다. 이러한 이유로 수문학적 위험인자를 효과적으로 고려하기 위해 2000년도 이후 선진국에서는 위험도 해석 기법을 기반으로 파괴모드, 다양한 하중조건 등을 조합하여 위험도 해석을 통해 댐의 안전도 검토를 실시하고 있다. 따라서 최근 증가하는 기상변동성을 능동적으로 고려하기 위해서는 위험도 해석기반의 수공구조물 안정성 평가기법을 기반으로 하는 종합적인 위험도 해석 방안수립이 요구된다. 이러한 이유로 본 연구에서는 BN 모형 기반의 댐 위험도 적용에 앞서 실증댐을 대상으로 분석을 수행하였으며, 분석 절차는 다음과 같다. 첫째, ICOLD 및 세계대댐회 등 다양한 논문, 보고서 등을 조사하여 댐 붕괴에 가장 큰 영향을 미치는 수문학적 파괴인자를 도출하였다. 둘째, BN 모형 구축시 각 노드는 앞서 도출된 수문학적 파괴인자를 이용하였으며, 각 파괴인자에 적합한 확률분포형을 부여하였다. 마지막으로, 노드별 임계값을 부여하여 상황별 파괴인자의 변화 양상을 도출하였다. 본 연구의 결과로 인해 연구대상댐의 가장 취약한 수문학적 파괴인자 도출이 가능하며, 댐의 보수 보강시 우선순위 의사결정의 지원이 가능 할 것으로 판단된다.

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