• Title/Summary/Keyword: 물성측정

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Structural Analysis of Gasket and GDL for Enhanced Performance of PEMFC (고분자 전해질 연료전지 가스켓 및 GDL의 구조 해석)

  • Yoon, Jin-Young;Park, Jungsun
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.36 no.7
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    • pp.642-650
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    • 2008
  • In this paper, structural behavior of Gasket and GDL of a PEMFC stack is studied to improve the performance and to secure the safety. In the Gasket analysis Mooney-Rivlin strain energy function is used to consider hyperelasticity of load and displacement. The material properties is determined by testing specimens of the gasket at uni-axial and equi-biaxial mode and compared with finite element analysis results. By measuring a thickness change, the material property of GDL is determined. The pressure drop of a unit cell is measured along the channel for the clamping force. A cross sectional change of channel base on the experimental data is obtained experimentally and compare with FEM analysis results.

A Study on Electrode Array for Measurement of Induced Polarization of Rock Samples (암석 시료의 유도분극 측정을 위한 전극배열 비교)

  • Man-ho Han;Jung-hwan Lee;Keun-Soo Lee;Myeong-Jong Yi
    • Tunnel and Underground Space
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    • v.33 no.6
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    • pp.483-494
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    • 2023
  • Measurement of the physical properties of rocks or minerals is an important factor in determining the distribution of the underground medium as well as mineral resource investigations. Resistivity and induced polarization, which are widely used in Korea, are methods for measuring electrical properties, which are representative properties of obtaining subsurface information. In order to precisely analyze the exploration data obtained from various sites, it is important to accurately measure the material properties. Electrical properties of rock is measured using two-electrode or four-electrode method. Compared to the four-electrode method, the two-electrode method is generally used because it is very easy to contact the sample and the electrode, but there is a problem in that the impedance of the electrode and the sample is measured together. In this study, the time-domain the induced polarization effects were measured using the 2-electrode method and the 4-electrode method for artificial samples mixed with graphite and cement having induced polarization characteristics, and the results were compared. Although the 4-electrode method has difficulties in installing potential electrodes, it was confirmed that it is effective in measuring electrical properties because it can reduce the problem caused by the impedance of potential electrodes compared to the 2-electrode method.

Characterization of the Material Properties of 0.68Pb ($Mg_{1}$3/$Nb_{2}$3/)$O_3$-0.32PbT$iO_3$ Single Crystals Grown by the Solid-State-Crystal-Growth Method (고상단결정법으로 성장시킨 0.68Pb ($Mg_{1}$3/$Nb_{2}$3/)$O_3$-0.32PbT$iO_3$ 압전단결정의 물성평가)

  • 이상한;노용래
    • The Journal of the Acoustical Society of Korea
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    • v.23 no.2
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    • pp.103-108
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    • 2004
  • In this paper, all the materials constants of the PMN-32%PT single crystals grown by the solid state crystal growth method were measured by the resonance method. PMN-PT crystals of tetragonal symmetry have six elastic constants, three piezoelectric constants and two dielectric constants for their independent material constants. These materials constants were extracted from six sets of crystal samples of each different geometry to have different vibration modes respectively. Measured results showed that the crystal has larger electromechanical coupling factor k/sub 33/ (∼86%) and piezoelectric constant d/sub 33/ (∼1200pC/N) than conventional piezoceramics. Validity of the measurement was confirmed through comparison of the results with the impedance spectrum from finite element analysis of the samples and the results measured with a commercial do meter.

진공 공정장비부품의 평가 연구

  • Song, Je-Beom;Sin, Jae-Su;Gang, Sang-U;Kim, Jin-Tae;Sin, Yong-Hyeon;Yun, Ju-Yeong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.02a
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    • pp.33-33
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    • 2011
  • 반도체 산업기술이 발달함에 따라 고청정 공정 환경이 요구되고 있으며, 반도체 공정용 장비에 이용되는 부품 중 양극산화피막법(Anodizing)으로 피막을 성장시킨 anodic aluminum oxide (AAO)부품은 플라즈마에 의해 화학적, 물리적 침식이 발생하여 코팅막과 모재에 손상을 일으키며 코팅막이 깨지거나 박리되면서 다량의 Particle이 생성됨으로써 공정상의 여러 가지 문제를 야기 시킨다고 알려져 있다. 하지만 코팅막을 평가하는 방법은 거의 전무하며 기본물성 측정방법인 피막두께, 내전압, 임피던스, 내식성 측정방법을 통하여 여러 기본물성측정방법으로 부품의 평가기술을 연구하였다. 본 연구에서는 이러한 진공 부품의 하나인 anodic aluminum oxide (AAO)부품샘플을 누설전류 및 내전압 측정하여 샘플의 전기적 특성을 측정하였고, 표면 미세구조의 변화를 관찰하였다. 부식실험으로는 HCl 가스를 발생시켜 부식정도를 알아봤으며, 부식처리와 플라즈마 처리 모두 코팅 막의 손상과 전기적 특성의 감소를 보였다. 진공장비 전극 부품평가의 유익한 평가 항목으로서 플라즈마 데미지를 주는 도중에 실시간으로 부품평가에 따른 Particle을 측정함으로써 ISPM 장비를 이용하여 진공 장비용 코팅부품이 플라즈마공정에서 발생하는 오염입자를 측정할 수 있는 방법을 연구하였다. 이러한 결과를 이용하여 진공공정에서 사용되는 코팅부품이 플라즈마에 의한 손상정도를 정량화 하고 평가방법을 개발하여 진공장비용 공정 중 실시간으로 부품의 성능평가가 가능하고 코팅부품 신뢰성 향상이 가능할 것으로 본다.

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The Effect of Interfacial Properties and RTM Process of Composites with Different Cross-linking Density by Molecular Weight of Hardener (경화제의 분자량에 의한 가교밀도 차이에 따른 복합재료의 계면 물성 및 RTM 성형성에 미치는 영향)

  • Park, Ha-Seung;Shin, Pyeong-Su;Kim, Jong-Hyun;Baek, Yeong-Min;Kwon, Dong-Jun;Park, Joung-Man
    • Composites Research
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    • v.30 no.3
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    • pp.169-174
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    • 2017
  • Demand of glass fiber reinforced composites (GFRC) increased with developing aircraft and defense industries using resin transfer molding (RTM) process to produce complex product. In this research, wetting, interfacial, and mechanical properties were evaluated with different Cross-linking Density by Molecular Weight of Hardener. Epoxy resin as matrices was used bisphenol-A type and amine-type hardeners with different molecular weight. Specimens were manufactured via RTM and wetting property of resin and glass fiber (GF) mat was evaluated to viscosity of epoxy and injection time of epoxy matrix. Mechanical property of GFRC was determined via flexural strength whereas interfacial properties were determined by interlaminar shear strength (ILSS) and interfacial shear strength (IFSS). The difference in mechanical property depends upon the fiber weight fraction (wt %) of GFRC by RTM as well as the different Molecular Weight of Hardener.

Instrumented Indentation Technique: New Nondestructive Measurement Technique for Flow Stress-Strain and Residual Stress of Metallic Materials (계장화 압입시험: 금속재료의 유동 응력-변형률과 잔류응력 평가를 위한 신 비파괴 측정 기술)

  • Lee, Kyung-Woo;Choi, Min-Jae;Kim, Ju-Young;Kim, Kwang-Ho;Kwon, Dong-Il
    • Journal of the Korean Society for Nondestructive Testing
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    • v.26 no.5
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    • pp.306-314
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    • 2006
  • Instrumented indentation technique is a new way to evaluate nondestructive such mechanical properties as flow properties, residual stress and fracture toughness by analyzing indentation load-depth curves. This study evaluated quantitatively the flow properties of steels and residual stress of weldments. First, flow properties can be evaluated by defining a representative stress and strain from analysis of deformation behavior beneath the rigid spherical indenter and the parameters obtained from instrumented indentation tests. For estimating residual stress, the deviatoric-stress part of the residual stress affects the indentation load-depth curve, so that by analyzing the difference between the residual-stress-induced indentation curve and residual-stress-free curve, the quantitative residual stress of the target region can be evaluated. The algorithm for flow property evaluation was verified by comparison with uniaxial tensile test and the residual stress evaluation model was compared to mechanical cutting and ED-XRD results.

Effect of Growth Methods of InAs Quntum Dots on Infrared Photodetector Properties (InAs 양자점 형성 방법이 양자점 적외선 소자 특성에 미치는 효과)

  • Seo, Dong-Bum;Hwang, Je-hwan;Oh, Boram;Noh, Sam Kyu;Kim, Jun Oh;Lee, Sang Jun;Kim, Eui-Tae
    • Korean Journal of Materials Research
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    • v.28 no.11
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    • pp.659-662
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    • 2018
  • We report the properties of infrared photodetectors based on two kinds of quantum dots(QDs): i) 2.0 ML InAs QDs by the Stranski-Krastanov growth mode(SK QDs) and ii) sub-monolayer QDs by $4{\times}[0.3ML/1nm\;In_{0.15}Ga_{0.85}As]$ deposition(SML QDs). The QD infrared photodetector(QDIP) structure of $n^+-n^-(QDs)-n^+$ is epitaxially grown on GaAs (100) wafers using molecular-beam epitaxy. Both the bottom and top contact GaAs layers are Si doped at $2{\times}10^{18}/cm^3$. The QD layers are grown with Si doping of $2{\times}10^{17}/cm^3$ and capped by an $In_{0.15}Ga_{0.85}As$ layer at $495^{\circ}C$. The photoluminescence peak(1.24 eV) of the SML QDIP is blue-shifted with respect to that (1.04 eV) of SK QDIPs, suggesting that the electron ground state of SML QDIP is higher than that of the SK QDIP. As a result, the photoresponse regime(${\sim}9-14{\mu}m$) of the SML QDIP is longer than that (${\sim}6-12{\mu}m$) of the SK QDIP. The dark current of the SML QDIP is two orders of magnitude smaller value than that of the SK QDIP because of the inserted $Al_{0.08}Ga_{0.92}As$ layer.

Properties of Eco-friendly Acrylic Resin/Clay Nanocomposites Prepared by Non-aqueous Dispersion (NAD) Polymerization (비수계 분산중합으로 제조된 환경친화성 아크릴수지/나노클레이 복합재료의 특성 연구)

  • Kim, Yeongho;Lee, Minho;Jeon, Hyeonyeol;Lee, Young Chul;Min, Byong Hun;Kim, Jeong Ho
    • Korean Chemical Engineering Research
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    • v.54 no.1
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    • pp.120-126
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    • 2016
  • Eco-friendly acrylic resin/clay nanocomposites containing pristine montmorillonite (PM) or modified clays (30B and 25A) were prepared from acrylic and styrenic monomers using non-aqueous dispersion (NAD) polymerization. Effect of nanoclays on physical properties of polymerization product and resulting nanocomposites was investigated. In view of NAD particle stability, addition of nanoclay at the beginning of polymerization is proved to be good. Results of gel fraction, acid value and viscosity of the NAD product showed that nanocomposites containing clay 25A showed better physical properties than the ones with other clays. GPC results exhibit the increase in molecular weight and decrease in polydispersity index for the 25A nanocomposite. Increase in layer distance confirmed from XRD analysis showed good dispersion of 25A in the nanocomposite. Thermal and dynamic mechanical analysis showed that highest glass transition temperature and storage modulus for 25A nanocomposites. These results indicate that 25A nanoclay gives the best properties in the process of non-aqueous dispersion polymerization of acrylic resin/nanoclay nanocomposites.

Economic Impact Analysis of the Ready-Operational Physical Properties Laboratory on Geoscience and Mineral Resources (지질자원 연구개발을 위한 상시가동 물성실험실 구축의 경제적 파급효과 분석)

  • Ahn, Eun-Young;Lee, Sang-Kyu
    • Economic and Environmental Geology
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    • v.40 no.6
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    • pp.805-814
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    • 2007
  • To offer R&D infrastructure on geoscience and mineral resources area, a new project was launched in KIGAM to build-up of a 'Ready-Operational Physical Properties Laboratory'. In this study, we evaluate the economic impact of the concentration of physical properties measurements equipment and facilities in KIGAM. As centralization of physical properties measurements of earth samples, the direct effects, annual measurement cost reduction and equipment opportunity cost are expected 1,095 million Won (US$1.095 million) and 1,440 million Won (US$1.440 million) in present aspects, and 1,110 million Won (US$1.110 million) and 1,527 million Won (US$1.527 million) in future aspects. The indirect economic effect by increasing of the relative papers is estimated 7,524 million Won (US$7.524 million) by the input cost approach, and the contributions of gross domestic product are 8,010 billion Won (US$8.010 billion) in the heavy construction industry and 260 billion Won (US$0.260 billion) in the mining and quarrying industry.

Relaxation and Freezing in Pb-based Relaxer Ferroelectrics (Pb계 완화형 강유전체에서의 relaxation 및 freezing거동)

  • 박재환;김윤호;박재관
    • Korean Journal of Crystallography
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    • v.12 no.3
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    • pp.157-161
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    • 2001
  • The observe relaxation phenomena and freezing behavior in Pb(Mg/sub ⅓/Nb/sub ⅔/O₃, relaxor ferroelectrics, weak electric-field properties as well as strong electric-field properties were investigated. The temperature dependence of the dielectric properties obtained using the low electric-field of 1 V/w was investigated. The dielectric properties obtained from the slope of the dielectric hysteresis loop and the temperature dependence of the pyroelectric properties were also investigated. When fitting all the experimental data with the Vogel-Filcher relation, a close agreement between the experimental data and equation was observed. The freezing temperature could be consistently calculated by the various methods.

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