• Title/Summary/Keyword: 마이크로반응기

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마그네트론 스퍼터링법을 이용한 Al-Ni Nano-foils의 형성 기구 및 미세구조 특성

  • Yu, Gwang-Chun;Lee, Won-Beom;Jo, Yong-Gi;Yu, Se-Hun;Kim, Hyeong-Sun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2013.05a
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    • pp.175-175
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    • 2013
  • Al-Ni nano-foil은 상온에서 외부 방전 및 촉발에 따라 급속한 자기 발열 반응이 일어나는 특성을 보이며, 외부 촉발을 통해 상온에서 온도를 높일 수 없는 접합이나 마이크로 수준의 미세 접합이 가능한 접합재료로서 현재 상당한 기대가치를 갖고 있는 재료이다. 코팅기술로서 sputtering법을 이용하여 Al-Ni 다층막의 nano-foil를 제조하여 Al-Ni 혼합 비율 및 Bi-layer 수에 따른 self-propagating reaction에 대해 조사하였다.

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Output Characteristics of Compact Far Infrared Free Electron Laser driven by a Conventional Microtron (마이크로트론을 이용한 소형 원적외선 자유전자레이저에서의 발진 특성)

  • ;;;;;;Gregory Kazakevich
    • Proceedings of the Optical Society of Korea Conference
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    • 2000.02a
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    • pp.48-49
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    • 2000
  • 한국원자력연구소에서는 가속기의 직경이 70 cm이고, 마그네트론 고주파 발생장치를 사용하는 소형 마이크로트론을 이용한 원적외선 자유전자레이저를 개발하였다$^{(1)}$ . 발진 파장은 100 - 200 $mu extrm{m}$ 영역이며, 첨두 출력은 약 1 - 10 kW이다. 본 연구에서는 개발된 원적외선 자유전자레이저의 시스템 개요와 출력 특성에 관하여 살펴보았다. 최근, 반도체와 물성의 분광학연구, 생명공학연구, 광화학 반응연구, 환경감시 기술개발, 인체영상, 군사용 감시기술 개발 등의 분야에서 새로운 연구와 첨단기술개발에 필요한 원적외선 광원의 요구가 점차 높아지고 있다. 이러한 요구에 부응하기 위하여 원적외선 영역의 다양한 광원 개발이 이루어지고 있으며, 특히, 테라헤르쯔 반도체 소자를 개발하기 위한 노력이 국내외에서 활발히 이루어지고 있다. 그러나, 아직까지는 이러한 광원의 출력이 mW 이하이고, 분광특성이 나빠서 실제응용에 많은 제한이 있다. (중략)

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An Investigation on the Surface Reactions after the Etching of $CeO_2$ Thin Films using High Denstity Inductively Coupled $C1_2CF_4Ar$Ar Plasmas (고밀도 유도결합 $C1_2CF_4Ar$ 플라즈마를 이용한 $CeO_2$ 박막 식각후 표면반응에 관한 연구)

  • 장윤성;김남훈;김경섭;이병기;엄준철;김태형;장의구
    • Proceedings of the International Microelectronics And Packaging Society Conference
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    • 2002.05a
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    • pp.255-258
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    • 2002
  • In this study, $CeO_2$thin films were etched with an addition of $Cl_2$gas to $Ar/CF_4$gas mixing in an inductively coupled plasma(ICP) etcher. The surface reactions of the etched $_CeO2$thin films were investigated by X-ray photoelectron spectroscopy(XPS). It was analyzed that Ce peaks were mainly observed in Ce-O bonds formed $CeO_2$or $CeO_3$compounds. Cl peaks were detected by the peaks of Cl $2p_{3/2}$ and Cl $2p_{1/2}$. Almost all of Cl atoms were combined with Ce atoms like $CeCl_{x}$ compounds.

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Study of On-chip Liquid Cooling in Relation to Micro-channel Design (마이크로 채널 디자인에 따른 온 칩 액체 냉각 연구)

  • Won, Yonghyun;Kim, Sungdong;Kim, Sarah Eunkyung
    • Journal of the Microelectronics and Packaging Society
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    • v.22 no.4
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    • pp.31-36
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    • 2015
  • The demand for multi-functionality, high density, high performance, and miniaturization of IC devices has caused the technology paradigm shift for electronic packaging. So, thermal management of new packaged chips becomes a bottleneck for the performance of next generation devices. Among various thermal solutions such as heat sink, heat spreader, TIM, thermoelectric cooler, etc. on-chip liquid cooling module was investigated in this study. Micro-channel was fabricated on Si wafer using a deep reactive ion etching, and 3 different micro-channel designs (straight MC, serpentine MC, zigzag MC) were formed to evalute the effectiveness of liquid cooling. At the heating temperature of $200^{\circ}C$ and coolant flow rate of 150ml/min, straight MC showed the high temperature differential of ${\sim}44^{\circ}C$ after liquid cooling. The shape of liquid flowing through micro-channel was observed by fluorescence microscope, and the temperarue differential of liquid cooling module was measuremd by IR microscope.

Charge Storage Behavior of the Carbons Derived from Polyvinylidene Chloride-resin and Polyvinylidene Fluoride in Different pH Electrolytes (다른 pH의 전해질에서 polyvinylidene chloride-resin와 polyvinylidene fluoride로부터 합성된 다공성 탄소의 전하 저장 거동)

  • Sang-Eun, Chun
    • Composites Research
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    • v.35 no.6
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    • pp.394-401
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    • 2022
  • Two polymer precursors, polyvinylidene chloride-resin (PVDC-resin) and polyvinylidene fluoride (PVDF), are assembled into the microporous carbon by pyrolysis. Microporous carbon is advantageous as an electrode for supercapacitors that store electric charges through ion adsorption/desorption. The pyrolysis also turns the various heteroatoms of two precursors into functional groups, contributing to the additional charge storage. The analysis of the porous structure and function group during carbonization are important to develop the carbon for energy storage. Here, we analyzed the functional groups of two polymer-derived carbons through X-ray photoelectron spectroscopy. The electrochemical properties of the functional groups were explored in various pH electrolytes. The specific capacitance of two carbons in the acidic electrolyte (1 M H2SO4) was improved compared to that in the neutral electrolyte (0.5 M Na2SO4) due to the faradaic charge/discharge reaction of the quinone functional group. In particular, the carbon electrode derived from PVDC-resin exhibits a lower capacity than the carbon from PVDF due to the small micropores. In the alkaline electrolyte (6 M KOH), the highest specific capacitance and rate capability were obtained among the three electrolytes for both electrodes based on the facile adsorption of the constituent electrolyte ions (K+, OH-).

Catalytic Reactor of Hydrogen Peroxide for a Micro Thruster (마이크로 추력장치용 과산화수소 촉매 반응기)

  • Lee, Dae-Hun;Cho, Jeong-Hun;Kwon, Se-Jin
    • 한국연소학회:학술대회논문집
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    • 2002.11a
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    • pp.237-240
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    • 2002
  • Micro catalytic reactors are alternative propulsion device that can be used on a nano satellite. When used with a monopropellant, $H_2O_2$, a micro catalytic reactor needs only one supply system as the monopropellant reacts spontaneously on contact with catalyst and releases heat without external ignition, while separate supply lines for fuel and oxidizer are needed for a bipropellant rocket engine. Additionally, $H_2O_2$ is in liquid phase at room temperature, eliminating the burden of storage for gaseous fuel and carburetion of liquid fuel. In order to design a micro catalytic reactor, an appropriate catalyst material must be selected. Considering the safety concern in handling the monopropellants and reaction performance of catalyst, we selected hydrogen peroxide at volume concentration of 70% and perovskite redox catalyst of lantanium cobaltate doped with strondium. Perovskite catalysts are known to have superior reactivity in reduction-oxidation chemical processes. In particular, lantanium cobaltate has better performance in chemical reactions involving oxygen atom exchange than other perovskite materials. In the present study, a process to prepare perovskite type catalyst, $La_{0.8}Sr_{0.2}CoO_3$, and measurement of its propellant decomposition performance in a test reactor are described.

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Development of Land Fill Gas(LFG)-MGT Power Generation and Green House Design Technology (쓰레기 매립지 MGT 발전 및 유리온실 설계기술개발)

  • Hur, Kwang-Beom;Park, Jung-Keuk;Lee, Jung-Bin
    • Journal of Energy Engineering
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    • v.20 no.1
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    • pp.13-20
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    • 2011
  • The high fuel flexibility of Micro Gas Turbine(MGT) has boosted their use in a wide variety of applications. Recently, the demand for biogas generated from the digestion of organic wastes and landfill as a fuel for gas turbines has increased. We researched the influence of firing landfill gas(LFG) on the performance and operating characteristics of a micro gas turbine combined heat and power system. $CH_4$ and $CO_2$ simultaneous recovery process has been developed for field plant scale to provide an isothermal, low operating cost method for carrying out the contaminants removal in Land Fill Gas(LFG) by liquid phase catalyst for introduce into the green house for the purpose of $CO_2$ rich cultivation of the plants. Methane purification and carbon dioxide stripping by muti panel autocirculation bubble lift column reactor utilizing Fe-EDTA was conducted for evaluate optimum conditions for land fill gas. Based on inflow rate of LFG as 0.207 $m^3$/min, 5.5 kg/$cm^2$, we designed reactor system for 70% $CH_4$ and 27% $CO_2$ gas introduce into MGT system with $H_2S$ 99% removal efficiency. A green house designed for four different carbon dioxide concentration from ambient air to 1500 ppm by utilizing the exhaust gas and hot water from MGT system.

A study of aldol condensation reaction product using a microreactor (마이크로 반응기를 적용한 알돌 축합반응 생성물 제조연구)

  • Kim Young-Jun;Lee Sang-Seo;Son Sung-Kwang;Song Kwang-Ho;Choe Jae-Hoon
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2006.05a
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    • pp.543-544
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    • 2006
  • 3-methyl-2-cyclopentenone is a valuable reaction intermediate for various high value added products. 3-methyl-2-cyclopentenone is not only expensive but also difficult to produce. 3-methyl-2-cyclopentenone can be synthesized by base catalyzed intermolecular aldol condensation. In this work, we studied a simple and practical method for synthesizing 3-methyl-2-cyclopentenone. Experimental results showed the advantages of the continuous flow process using a microreactor with kenic mixers for the synthesis of 3-methyl-2-cyclopentenone.

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Surface Reactions after the Etching of CeO$_2$ Thin films using Inductively Coupled C1$_2$/CF$_4$/Ar Plasmas (유도결합 C1$_2$/CF$_4$/Ar 플라즈마를 이용한 CeO$_2$ 박막 식각후 표면반응)

  • 이병기;김남훈;장윤성;김경섭;김창일;장의구
    • Journal of the Microelectronics and Packaging Society
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    • v.9 no.2
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    • pp.27-31
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    • 2002
  • In this study, $CeO_2$ thin films were etched with an addition of $Cl_2$ gas to $Ar/CF_4$ gas mixing in an inductively coupled plasma (ICP) etcher by the etching parameter such as RF power of 700 W, chamber pressure of 15 mTorr and dc bias voltage of -200 volts. The etch rate of $CeO_2$ films was 250 $\AA$/min with an addition of 10% $Cl_2$ gas to $Ar/CF_4$ gas mixture and the selectivity to SBT film was 0.4 at that condition. The surface reactions of the etched $CeO_2$ thin films were investigated by X-ray photoelectron spectroscopy (XPS). It was analyzed that Ce peaks were mainly observed in Ce-O bonds formed $CeO_2$ or $Ce_2O_3$ compounds. Cl peaks were detected by the peaks of Cl $2p_{3/2}$ and Cl $2p_{1/2}$. Almost all of Cl atoms were combined with Ce atoms like $CeCl_x$ or $Ce_x/O_yCl_z$ compounds.

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Separation Between Soil Particles and Magnetic Beads by Magnetic Force (자력을 이용한 토양입자와 마이크로자성체의 분리 연구)

  • So, Hyung-Suk;Shin, Hyun-Chul;Yoo, Yeong-Seok
    • Journal of the Korean Magnetics Society
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    • v.15 no.2
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    • pp.76-80
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    • 2005
  • It was evaluated whether magnetic beads able to add the functionality of environment purification can be employed in processing soil pollutants. In this study, the micro scale magnetic beads containing carboxyl groups were mixed with water and the soil $(<0.025{\cal}mm) filtered through a sieve, and then it was agitated before isolating the magnetic substances by the use of outer magnetic force. The factors considered at this step were the ratio of soil to magnetic beads, ratio of soil to water, size of the tube where the reaction occur, and intensity of the magnetic force. From the separation experiment between soil and magnetic beads, it was concluded that the magnetic beads and water quantity have an impact on the degree of separation, yet the size of the tube and magnetic force does not have a considerable effect upon that in this small-scaled experiment. Through this experiment, the reaction conditions were optimized to achieve $90\~100\%$ of separation. Therefore, it was concluded that when the functionalized magnetic beads is introduced to environmental processing, it is able to be adopted to the soil processing as well as the water processing.