• Title/Summary/Keyword: 레이저 형광법

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Comparison of Enhancing Fingerprints Treated with Two Fluorescence Amino Acid Reactive Reagents in Accordance with Laser and LED Light Sources (광원에 따른 아미노산 반응 형광시약 처리지문의 증강 효과성 비교)

  • Kim, Chae-Won;Ki, Jin-Young;Kim, Kyu-Yeon;Kim, Ji-Yeon;Jeon, So-Young;Yu, Je-Seol
    • The Journal of the Korea Contents Association
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    • v.17 no.4
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    • pp.569-575
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    • 2017
  • Forensic light source is commonly used for enhancing evidence in a nondestructive way. Latent fingerprints play an important role in an aspect of crime scene investigation. In this study, researchers compared enhancement of standard fingerprints treated with DFO and 1,2-IND in accordance with laser and LED light sources. As a result, laser light source has a better effect rather than LED light sources. However, each light source has strengths and weaknesses in terms of performance and portability. Therefore, researchers recommend that crime scene investigators need to use laser and LED light sources depending on the situation.

레이저 유기 형광법을 이용한 자기장이 인가된 유도결합플라즈마의 전기장 특성 연구

  • Song, Jae-Hyeon;Kim, Hyeok;Jeong, Jae-Cheol;Hwang, Gi-Ung
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.474-474
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    • 2010
  • 현재 반도체시장의 확장으로 인해서 기존의 300mm 웨이퍼에서 450mm의 웨이퍼를 사용하는 공정으로 변화하는 추세이다. 450mm 웨이퍼로 대면적 화되면서 기존 300mm 공정 때보다 훨씬 효율적인 플라즈마 소스 즉, 고밀도이고, 고균등화(high uniformity) 플라즈마 소스를 필요로 한다. 본 논문에서는 고밀도 플라즈마 소스인 유도 결합형 플라즈마(Inductively Coupled Plasma ; ICP)에 축 방향의 약한 자기장을 인가시킨 자화된 유도결합형 플라즈마(Magnetized Inductively Coupled Plasma : MICP)[1]를 제안하여 기존 ICP와의 차이점을 살펴보았다. 실험 방법으로 레이저 유기 형광법(Laser Induced Fluorescence : LIF)[2]을 이용하여 플라즈마 쉬스(Sheath) 내의 전기장을 외부 자기장의 변화에 따라 높이별로 측정하고 그 결과로부터 쉬스의 전기적 특성을 살펴보았다. 플라즈마의 특성상 탐침이나 전극에 전압을 인가하면 그 주위로 디바이 차폐(Debye Shielding)현상이 일어나서 플라즈마 왜곡이 일어난다. 그렇기에 플라즈마, 특히 플라즈마 쉬스의 특성을 파악하기 위해서 레이저라는 기술을 사용하였다. 레이저는 고가의 장비이고 그 사용에 많은 경험지식(know-how)를 필요로 하지만 플라즈마를 왜곡시키지 않고, 플라즈마의 밀도, 온도, 전기장 등 많은 상수(parameter)들을 얻어 낼 수 있다. 또한 3차원적으로 높은 분해능을 가지고 있는 장점이 있다. 강한 전기장이 있는 곳에서 입자들의 고에너지 준위가 전기장의 세기에 비례하여 분리되는 Stark effect[3] 이론을 이용하여 플라즈마 쉬스내의 전기장을 측정하였다. 실험은 헬륨가스 700mTorr 압력에서 이루어졌다. 기판의 파워를 50W에서 300W까지 변화시키면서 기판에 생기는 쉬스의 전기장의 변화를 살펴보았고, 자기장을 인가한 후 동일한 실험을 하여 자기장의 유무에 따른 플라즈마 쉬스의 전기장 변화를 살펴보았다. 실험결과 플라즈마 쉬스의 전기장의 변화는 기판의 파워와 플라즈마 밀도에 크게 의존함을 알았다. 기판의 파워가 커질수록 쉬스의 전기장은 커지고, 기판에 생기는 Self Bias Voltage역시 음의 방향으로 커짐을 확인 하였다. 또한 자기장을 걸어주었을 경우 쉬스의 두께가 얇아짐으로써 플라즈마의 밀도가 증가했음을 확인 할 수 있었다.

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Study on the characteristics of laminar lifted flames using planar laser induced fluorescence technique (평면 레이저유도 형광법을 이용한 부상화염의 특성 연구)

  • Lee, Byeong-Jun;Jeong, Seok-Ho;Han, Jae-Won
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.21 no.11
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    • pp.1393-1402
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    • 1997
  • Characteristics of the lifted flame which is generated by issuing of the fuel through the miniature nozzle, d = 0.164 mm, are studied using the planar laser induced fluorescence technique. OH radical is excited on the $Q_{1}$(8) line of the $A^{2}$.SIGMA.$^{+.leq.X2}$ .PI.(1, 0) band transition (283.55 nm) and LIF signals are captured at the bands of (0, 0) and (1, 1) transition (306 ~ 326 nm) using the filters and ICCD camera. Hydroxyl radical (OH) profile for nozzle attached flame shows that OH radical populations at the flame sides and flame tip are larger than those at the base. But for the lifted flame (tribrachial flame) case, those are larger at the flame base than at the flame tip and flame sides. The OH radical is more dense near the center line of flame base at the blowing out. This fact proves the Chung and Lee's blowout theory-blowout occurs when the flame is anchored at the flame axis. axis.

An Improved Laser-Induced Fluorimetry for Assay of Uranium in Urine (레이저 유발형광법을 이용한 우라늄 작업자의 뇨 형광 분석)

  • Lee, Sang-Mok;Shin, Jang-Soo;Kim, Cheol-Jung
    • Nuclear Engineering and Technology
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    • v.25 no.2
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    • pp.255-258
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    • 1993
  • A method for analysis of trace uranium in urine sample was studied using a time-resolved $N_2$-laser-induced fluorimetry. The Fluran solution was found to be efficient to mask the chloride ions which are known to quench uranium fluorescence in the fluorimetric assay of uranium in urine. This improved method made the sample preparation much simpler than other conventional ones. The fluorescence intensities at 1% urine mixture with 10% Fluran aqueous solution showed good linearities in the concentration range of 10-500 ppb(before dilution).

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Diagnostic Utilization of Laser Fluorescence for Resin Infiltration in Primary Teeth (유치의 레진침투법을 위한 레이저 형광법의 진단적 활용)

  • Park, Soyoung;Jeong, Taesung;Kim, Jiyeon;Kim, Shin
    • Journal of the korean academy of Pediatric Dentistry
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    • v.46 no.3
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    • pp.265-273
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    • 2019
  • This study was performed to evaluate clinical use of laser fluorescence (LF) to identify early childhood caries lesions suitable for applying resin infiltration. 20 exfoliated primary molars with proximal caries were selected and cut buccolingually cross the central pit for regarding the mesial and distal surfaces respectively. 27 specimens corresponding to ICDAS code 1 and 2 were selected and the LF values were measured. When infiltrant resin was applied, double staining for microscopy detection has done simultaneously. Tooth samples were sliced with 0.7 mm thick. The maximum lesion depth, maximum penetration depth, and average penetration rate were measured from the confocal scanning laser microscope image. Pearson correlation analysis was performed. The intraclass correlation coefficient of LF values shows excellent agreement. LF values had positive correlation with penetration rate, but not lesion depth and penetration depth. Significant correlation between LF readings and penetration rate was verified in deep enamel caries and dentin caries except shallow enamel caries. Infiltrant resin could penetrate with a higher rate and LF values could be increased in more active caries lesions. In assessing radiologically similar caries lesion, laser fluorescence might be useful for identifying caries activity.

A Study on Measurement of NO Concentrations in Laminar Nonpremixed $H_2/N_2$ Flame by LIF (레이저 유도 형광법(LIF)을 이용한 층류 비예혼합 $H_2/N_2$화염에서의 NO 농도측정에 관한 연구)

  • Kim, Sun-Wook;Jin, Seong-Ho;Kim, Gyung-Soo;Park, Kyoung-Suk
    • 한국연소학회:학술대회논문집
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    • 2001.06a
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    • pp.133-138
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    • 2001
  • In this study, quantitative nitric oxide concentration distributions are investigated in the laminar nonpremixed $H_2/N_2$ flames by laser-induced fluorescence (LIF). The measurements are taken in flames for different $N_2$ dilution ratios varying from 20${\sim}$80%, and fuel now rate is fixed as lslpm. The NO A-X (0,0) vibrational band around 226 nm is excited using a XeCl excimer-pumped dye laser. We applied same excitation line used in $CH_4$ premixed flame. Overall, NO concentration was rapidly decreased with $N_2$ addition and we could not measure the concentration any longer for $N_2$ dilution above 80%.

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A Study on Measurement of NO Concentrations in Burner Flames by LIF (레이저 유도 형광법(LIF)을 이용한 버너 화염의 NO 농도측정에 관한 연구)

  • Park, K.S.;Kim, S.W.
    • Journal of ILASS-Korea
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    • v.7 no.4
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    • pp.42-49
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    • 2002
  • In this study, quantitative measurement of nitric oxide concentration distributions were investigated in the laminar CH4/O2/N2 premixed flame by laser-induced fluorescence (LIF). The NO A-X (0,0) vibrational band around 226nm was excited using a XeCl excimer-pumped dye laser. Selecting an appropriate NO transition minimizes interference from Rayleigh scattering and O2 fluorescence. The measurements were taken in CH4/O2/N2 premixed flame with equivalence ratios varying from $1.0{\sim}1.6$, and a fixed flowrate of 5slpm. NO was found to produce primarily between an inner premixed and an outer nonpremixed flame front, and total NO concentration is raised when equivalence ratios increase. These results suggest that prompt NO is likely to contribute to NO formation in CH4/O2/N2 premixed flame. Furthermore, this trend was well matched with previous works.

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A Study on Measurement of NO Concentrations in Laminar Premxied $CH_4/O_2/N_2$ Flames by LIF (레이저 유도 형광법(LIF)을 이용한 층류 메탄 예혼합 화염내 NO 농도측정에 관한 연구)

  • Kim, Sun-Wook;Jin, Seong-Ho;Kim, Gyung-Soo;Park, Kyoung-Suk
    • Proceedings of the KSME Conference
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    • 2000.11b
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    • pp.156-161
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    • 2000
  • In this study, quantitative nitric oxide concentration distributions are investigated in the post-flame zone of laminar premixed $CH_4/O_2/N_2$, flames by laser-induced fluorescence (LIF). The measurements are taken in flames for different equivalence ratios varying from $0.8{\sim}1.4$, and flow rate is fixed as 5slpm. The NO A-X (0,0) vibrational band around 226 nm is excited using a XeCl excimer-pumped dye laser. Selecting an appropriate NO transition minimizes interferences from Rayleigh scattering and $O_2$ fluorescence. NO concentration is rised when equivalence ratios increase at different vertical distances form nozzle tip. In any case, the maximum NO concentration reaches the maximum in reaction zone.

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A Study on Characteristics of Temperature and Radicals in Laminar Non-premixed H2/N2 Flame Using LIPF and LRS (레이저 유도 선해리 형광법과 래일레이 산란법에 의한 층류 비예혼합 수소/질소 화염의 온도 및 라디칼 특성에 관한 연구)

  • Jin, Seong Ho;Park, Kyoung Suk;Kim, Gun Hong;Kim, Gyung Soo
    • Transactions of the Korean hydrogen and new energy society
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    • v.13 no.3
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    • pp.169-180
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    • 2002
  • Rayleigh scattering and laser induced predissociative fluorescence are used to obtain two-dimensional images of temperature and species concentration in a laminar non-premixed flame of a diluted hydrogen jet. Rayleigh scattering cross-sections are experimentally obtained at 248nm. Planar images of OH and $O_2$ with tunable KrF excimer laser which has a) $0.5cm^{-1}$ linewidth, b) 0.5nm tuning range, c) 150mJ pulse energy, and d) 20ns pulse width are obtained to determine spatial distributions of OH and $O_2$. The technique is based on planar laser induced predissociative fluorescence (PLIPF) in which collisional quenching is almost avoided because of the fast predissociation. Dispersed LIPF spectra of OH and $O_2$ are also measured in a flame in order to confirm the excitation of single vibronic state of OH and $O_2$. OH and $O_2$ are excited on the $P_2$(8) and $Q_1$(11) line of the $A^2{\Sigma}^{+}({\nu}^{'}=3)-X^{2}{\Pi}({\nu}^{''}=o)$ band and R(17) line of the Schumann-Runge band $B^{3}{\Sigma}_{u}{^-}(\nu^{'}=0)-X^{3}{\Sigma}_{g}{^-}({\nu}^{''}=6)$, respectively. Fluorescence spectra of OH and Hot $O_2$ are captured and two-dimensional images of the hydrogen flame field are successfully visualized.

레이저 기반 플라즈마 진단

  • Seo, Byeong-Hun;Kim, Jeong-Hyeong;Seong, Dae-Jin;Yu, Sin-Jae
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.94.1-94.1
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    • 2016
  • 레이저 진단은 플라즈마 진단법 중 가정 정확한 진단법으로 알려져 있다. 특히 진단이 까다로운 고밀도, 자기장, 고압 환경에서도 그 측정 결과가 신뢰성 있다고 잘 알려져 있다. 본 특별 심포지엄에서는 중 성종을 측정 할 수 있는 레일레이 산란과 자유 전자를 측정 할 수 있는 톰슨 산란, 그리고 분자를 측정할 수 있는 라만 산란을 중심으로 발표 할 것이다. 또한 특정 준위를 갖는 원자 및 분자의 거동을 측정할 수 있는 레이저 유도 형광에 대해서도 간단히 발표 할 것이다. 그밖에 레이저 진단의 종류, 원리 등을 설명 하고 한국표준과학연구원에서 이루어 진고 있는 연구 결과에 대해 발표 할 것이다.

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