• Title/Summary/Keyword: 내부표준법

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Quantifying Uncertainty of Vitamin C Determination in Infant Formula by Indophenol Titration Method (인도페놀 적정법에 의한 성장기용조제식 중 비타민 C 함량분석의 측정불확도 산정)

  • Jun, Jang-Young;Kwak, Byung-Man;Ahn, Jang-Hyuk;Kong, Un-Young
    • Korean Journal of Food Science and Technology
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    • v.37 no.3
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    • pp.352-359
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    • 2005
  • Uncertainty involved during determination of vitamin C content in infant formula was quantified by indophenol titration method. Uncertainty sources in measurand, such as purity, weight, final volume of standard, volume of standard solution used for titration, sample weight, final volume of sample, extraction solution used for titration, titration of extraction solution and standard solution by indophenol solution were identified and used as parameters for combined standard uncertainty based on Guide to the expression of uncertainty in measurement (GUM) and Draft EURACHEM/CITAC Guide. Uncertainty parameters of each source in measurand were identified as resolution, reproducibility and stability of chemical balance, standard material purity, repeatability, reproducibility, end point of titration, 1 mL pipet, 5 mL autopipet, and 100 mL mass flask. Each uncertainty component was evaluated by types A and B and included to calculate combined uncertainty. Analytical test result for traceability under laboratorial conditions using Certified Reference Material (CRM) test was certified as $108.4{\pm}1.7mg/100g$, which was within CRM certification range of $114.6{\pm}6.6mg/100g$. Uncertainty test result of vitamin C content of 5 g sampling was $56.7{\pm}2.44mg/100g$. Uncertainty could be reduced by identification of uncertainty sources and components related with vitamin C determination by indophenol titration method and by decreasing uncertainty sources and components.

A Study on Filter Performance of Materials in Embankment Slope during Heavy Rain (강우시 성토사면 재료의 필터조건검토에 대한 연구)

  • Kim, Sang-Hwan;Mha, Ho-Seong
    • Journal of Korean Society of societal Security
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    • v.1 no.4
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    • pp.65-71
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    • 2008
  • This paper presents the characteristics of internal erosion of embankment slopes due to the localized heavy rain. In this study, the existing analysis methods of filter performance in embankment materials were reviewed. Based on the theoretical concept of filter conditions to prevent particles from being carried in from the adjacent embankment materials, new analysis method was suggested. According to the new analysis method for filter performance, experimental programs were carried out to investigate the filter performance for controlling and sealing any leak which develops through the embankment materials as a result of internal erosion. Three sets of small scale laboratory tests were carried out with changing the main influence factors such as rainfall intensity, gradient of slope, embankment material condition. It was found that the new analysis method for filter performance to prevent particles from being carried in from the adjacent embankment materials was more capable approach to design the filter materials in embankment slopes. The new criterion or method for satisfactory filter performance, therefore, was recommended.

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Analysis of Faceted Schemes of Korean Decimal Classification (KDC의 조합식 분류체계 분석)

  • Jung Hae-Sung
    • Journal of Korean Library and Information Science Society
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    • v.36 no.4
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    • pp.133-153
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    • 2005
  • This study is to analyze and suggest the KDC's facet structure. KDC is using the Decimal Classification's facet structure. New suggestions are : Clearly use standard subdivisions and add instruction like 'Add to base number $\~$ notation $\~$ from table $\~$' : auxiliary tables contents are need to revise and expand to make a add table found in schedules and provide numbers to be added to designated schedules numbers are necessary.

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5m급 알루미늄 선체의 ISO기반 낙하시험법 적용에 관한 연구

  • Gang, Nam-Seon;Gwon, Yong-Won;Jang, Ho-Yun
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • 2012.06a
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    • pp.282-283
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    • 2012
  • 국제표준규격(ISO 12215-5) 및 국내 플레저보트 검사지침의 개정에 따라 길이 6미터 미만의 플레저보트의 낙하시험에 의한 강도시험기준을 적용 가능하게 되었다. 하지만 현재 낙하시험은 자유낙하 시 내력 및 외력에 의한 선체 내부의 찌그러짐, 크랙, 박리, 파손 등을 육안으로 검사하는 방법으로 시험결과의 정량적인 판단이 이루어지지 않고 있다. 따라서 본 연구에서는 레저선박의 낙하시험을 위한 시스템 및 운용프로그램을 개발하여 플레저보트의 구조안전성의 정량적 평가가 가능한 시스템을 개발하고 다단 롤포밍 기법을 적용한 5m급 알루미늄레저보트에 적용하여 시스템의 성능을 검증하였다.

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Quantitative Determination of ABS from Mixture of Anionic and Nonionic Detergents by NMR (NMR을 이용한 음이온 및 비이온세제의 혼합물로부터 ABS의 정량)

  • Koang-Hoon Choe;Sun-Ja Kwon
    • Journal of the Korean Chemical Society
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    • v.27 no.6
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    • pp.419-423
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    • 1983
  • Amounts of alkylbenzene sulfonate (ABS) in the mixtures of anionic and nonionic detergents were determined by nuclear magnetic resonance (NMR) method. In the NMR spectrum of anionic and nonionic detergents, benzene group showed peaks overlapping at 6.5∼8ppm, but after sampling, benzene group showed two doublet at 7∼8ppm. Calibration curve was obtained by relative ratio of area for benzene group in anionic detergent to that for methyl group in acetic acid(acetic acid was used as the internal standard).

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An Analytical Method of Thromboxane $B_2$ by Fast Atom Bombardment Mass Spectrometry (고속원자충격질량분석법을 이용한 Thromboxane $B_2$ 분석)

  • Jang, Suk-Yoon;Kim, Jung-Hoon;Lee, Yong-Moon;Jang, Seung-Ki;Moon, Dong-Cheul
    • Analytical Science and Technology
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    • v.6 no.4
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    • pp.349-357
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    • 1993
  • Analytical methods of thromboxane $B_2(TXB_2)$ using various techniques of Fast Atom Bombardment mass spectrometry (FAB MS) were studied, static FAB condition was investigated to obtain linear response curve using docosanoic acid as a internal standard. For maximum sensitivity, a continuos-flow(CF-) FAB MS by selected-ion monitoring(SIM) with devised sample introduction system, has been developed to quantiate thromboxane $B_2$ in biological sample. Instrumental parameters affecting sensitivity, reproducibility has been studied. The method has been optimized with respect to the eluent, 0.75% glycerol(in EtOH v/v) and flow rate of $3.7{\mu}l/min.$ Under the condition, detection limits were below 10pg in SIM mode and a good linear relationship between dose and response was achieved.

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The chemical speciation and analysis of trace elements in sediment with neutron activation analytical method(NAA) and atomic mass spectrometry (중성자 방사화분석법과 원자질량분석법을 이용한 침전물 시료속에 존재하는 미량원소들의 화학종 분류 및 분석)

  • Nam, Sang-Ho;Kim, Jae-Jin;Chung, Yong-Sam;Kim, Sun-Ha
    • Analytical Science and Technology
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    • v.16 no.5
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    • pp.358-367
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    • 2003
  • In this research, first of all, the analytical methods for the determination of major elements in sediment have been developed with ICP-MS (Inductively Coupled Plasma Mass Spectrometry). The analytical results of major elements (Al, Ca, K, Fe, Mg) with Cool ICP-MS were much better than those with normal ICP-MS. The analytical results were compared with those of NAA (Neutron Activation Analysis). NAA were a little superior to ICP-MS for the determination of major elements in sediment as a non-destructive trace analytical method. The analytical methods for the determination of minor elements (Cr, Ce, U, Co, Pb, As, Se) have been also developed with ICP-MS. The analytical results by standard calibration curve with ICP-MS were not accurate due to the matrix interferences. Thus, the internal standard method was applied, then the analytical results for minor elements with ICP-MS were greatly improved. The analytical results obtained by ICP-MS were compared with those obtained by NAA. It showed that the two analytical methods have great capabilities for the determination of minor elements in sediments. Accordingly, the NAA will play an important role in analysis of environment sample with complex matrix. ICP-MS also will play an important role because it has a great capability for the determination of Pb that could not be determined by NAA.

A Study on Fire Performance of HPC Column with Fiber Cocktail in KS Fire Curve under Loading Condition (표준화재 재하조건에서 Fiber Cocktail을 혼입한 고강도 콘크리트 기둥의 강도별 화재거동에 관한 연구)

  • Kim, Heung-Youl;Chae, Han-Sik;Kim, Hyung-Jun;Jeon, Hyun-Kyu;Youm, Kwang-Soo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.377-380
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    • 2008
  • The material and mechanical properties in the high temperature area of 40 to 100 MPa high strength concrete structural member was identified based on mixing of fiber cocktail and the structural element fire behavior simulation through the finite element analysis method (ABAQUS) was interpreted. The results are as follows. First, it was interpreted that the test specimen with concrete fiber cocktail mixed was more controllable in the maximum shrinkage than the one with concrete fiber cocktail not mixed the controllable range was about 25% to 55%. This means that shrinkage is controllable through mixing of fiber cocktail for the high strength concrete columns. Second, this study didn't consider the explosive spalling by the pore pressure within high strength concrete. If the properties for the pore pressure within high strength concrete is considered and database by strength and by inner temperature of various high strength concrete and steel materials are established in the future, it is interpreted that the technical foundation will be laid for performance based design of fire resistant construction.

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A Study on B2B Workflow Integration Technology (기업간 워크플로우 통합 기술에 대한 연구)

  • 정재윤;김훈태;김동수;강석호
    • The Journal of Society for e-Business Studies
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    • v.9 no.1
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    • pp.39-59
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    • 2004
  • E-business automates overall activities in a company and allows distributed systems to communicate their information. The automation and information sharing improves its productivity and responsiveness. B2B workflow systems progress their business processes electronically and help the companies to monitor their execution and administrate the processes. This research analyzes the technologies and standards for B2B workflow integration, and proposes three approaches to implement effectively workflow integration. We analyze several existing workflow standards and business process definition languages, and compare their structures and features. And we examine the messaging technologies and architectures to implement business integration. Finally we extract a reference model for B2B workflow integration, and propose three types of workflow integration and implementation designs. This research helps companies to understand the workflow standards and the messaging technologies for B2B workflow integration, and to implement workflow integration systems that are suitable for their e-business environments.

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Improvement Direction of the Public Records Management System for the Application of MSR (Management System for Records) (기록경영시스템(MSR) 적용에 대비한 공공기관 기록관리 제도의 개선 방향)

  • Kang, Dongkyun;Rieh, Hae-Young
    • Journal of Korean Society of Archives and Records Management
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    • v.16 no.4
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    • pp.121-148
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    • 2016
  • MSR identifies that records are key factors in achieving the goals of an organization and that records management is part of the business administration. Therefore, organizations could secure accountability and continuity of works through the activities of production and management records. This study explored what should be prepared to adopt MSR in public institutions based on the analysis of the requirements of the ISO 30301. which is prepared to be utilized as a certificate system. It focuses on 1) how laws could be supplemented to adopt MSR by comparing the requirements of MSR and the Public Records Management Act; 2) what should be prepared by organizations in terms of their rules and procedures; and 3) how the evaluation system of public institutions and the records management evaluation system could be revised to ensure that MSR will be sufficiently implemented in the organizations. In conclusion, the part to be supplemented by the law, the area to be operated as the internal rules of the organizations, and the way to be reflected in the evaluation of the public institutions were suggested.