• 제목/요약/키워드: 나노 재료

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$Al_2O_3$/5vo1%Cu 나노복합재료의 제조 및 기계적특성 (Preparation and Mechanical Properties of $Al_2O_3$/5vo1%Cu Nanocomposites)

  • 오승탁;이재성
    • 한국분말재료학회지
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    • 제7권4호
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    • pp.212-217
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    • 2000
  • An optimum route to fabricate the $Al_2O_3/Cu$ nanocomposites with sound microstructure and improved mechanical properties was investigated. Microstructural investigations for the composites prepared using $Al_2O_3/Cu$-nitrate showed that fine Cu particles with average size of 150 nm were homogeneously distributed within the $Al_2O_3$ matrix grains and at the grain boundaries. Fracture strength of 953 MPa and toughness of 4.8 Mpa(equation omitted)m were measured for the composite. The strengthening and toughening of the composites are explained by the refinement of the microstructure and the crack bridging/deflection, respectively.

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입자 함유율의 변화에 따른 나노 실리카 복합재료의 마모 특성 (Wear characteristics on particle volume fraction of nano silica composite materials)

  • 이정규;고성위
    • 수산해양기술연구
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    • 제49권4호
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    • pp.492-499
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    • 2013
  • The characteristics of abrasive wear of the rubber matrix composites filled with nano sized silica particles were investigated at ambient temperature by pin-on-disc friction test. The range of volume fraction of silica particles tested are between 11% to 25%. The cumulative wear volume and friction coefficient of these materials on particle volume fraction were determined experimentally. The major failure mechanisms were lapping layers, deformation of matrix, ploughing, deboding of particles and microcracking by scanning electric microscopy photograph of the tested surface. The cumulative wear volume showed a tendency to increase nonlinear with increase of sliding distance. As increasing the silica particles of these composites indicated higher friction coefficient.

Ni-Fe 합금입자 분산 Al2O3 나노복합재료의 미세조직 및 특성 (Microstructure and Properties of Nano-Sized Ni-Fe Alloy Dispersed Al2O3 Composites)

  • 남궁석;정재영;오승탁;이재성;이홍재;정영근
    • 한국분말재료학회지
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    • 제9권3호
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    • pp.161-166
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    • 2002
  • Processing and properties of $Al_2O_3$ composites with Ni-Fe content of 10 and 15 wt% were investigated. Homogeneous powder mixtures of $Al_2O_3$/Ni-Fe alloy were prepared by the solution-chemistry route using $Al_2O_3$, $Ni(NO_3)_2{\cdot}6H_2O$ and $Fe(NO_3)_3{\cdot}9H_2O$ powders. Microstructural observation of composite powder revealed that Ni-Fe alloy particles with a size of 20nm were homogeneously dispersed on $Al_2O_3$ powder surfaces. Hot-pressed composites showed enhanced fracture toughness and magnetic response. The properties are discussed based on the observed microstructural characteristics.

핫엠보싱 공정에서 PMMA의 마이크로/나노 레올로지 특성 (Micro/Nano Rheological Characteristics of PMMA in Hot Embossing Process)

  • 김병희;김광순;반준호;신재구;김헌영
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2004년도 춘계학술대회 논문집
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    • pp.259-264
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    • 2004
  • The hot embossing process as a method for the fabrication of polymer is becoming increasingly important because of its simple process, low cost, high replication fidelity and relatively high throughput. In this paper, we carried out experimental studies and numerical simulations in order to understand the viscous flow of polymer film during hot embossing process. As the initial step of quantitating the hot embossing process, simple parametric studies for the embossing conditions have been carried out using high resolution masters which patterned by DRIE process. Under different embossing times and pressures, the viscous flow of PMMA films into micro/nano cavities has been investigated. Also, the viscous flow during the hot embossing process has been simulated by the continuum based FDM analysis considering micro/nano effect, such as surface tension and contact angle.

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나노결정립 금속재료의 변형기구지도 (Deformation Mechanism Map of Nanocrystalline Metallic Materials)

  • 윤승채;복천회;곽은정;김형섭
    • 소성∙가공
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    • 제16권6호
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    • pp.473-478
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    • 2007
  • In this study, a deformation mechanism map of metallic nanocrystalline materials(NCMs) using the phase mixture model is proposed. It is based on recent modeling that appears to provide a conclusive description of the phenomenology and the mechanisms underlying the mechanical properties of NCMs. The proposed models adopted the concept of a 'phase mixture' in which the grain interior and the grain boundaries are treated as separate phases. The volume fraction of this grain boundary 'phase' may be quite appreciable in a NCM. Based on the theoretical model that provides an adequate description of the grain size dependence of plasticity covering all grain size range from coarse down to the nanoscale, the tensile deformation response of NCMs, especially focusing on the deformation mechanisms was investigated. The deformation mechanism map is newly proposed with axes of strain rate, grain size and temperature.

접촉 역학적 접근에 의한 점탄성/탄성, 점탄성/점탄성 재료간의 접합 에너지 측정 (A Measurement of Adhesion Energy between Viscoelastic/Elastic, Viscoelastic/Viscoelastic Materials Using Contact Mechanics Approach)

  • 이찬;엄윤용
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 춘계학술대회
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    • pp.1030-1035
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    • 2003
  • The nanoimprint lithography technology makes higher density of semiconductor device and larger capacity of storage media. In this technology the induced damage while detaching polymer pattern from mold should be minimized. In order to analyze the problem, the basic knowledge of adhesion between the polymer and the mold is required. In this study a contact experiment of polyisobutylene specimen with spherical steel tip and polyisobutylene bead tip was conducted using nano indenter. During the contact experiment with various loading rate under load control the contact behavior of viscoelastic material was measured, i.e., the load and displacement between the tip and the specimen were measured. The data was analyzed by HBK model to obtain the stress intensity factor of contact edge and the contact radius as a function of time. Also the adhesion energies between steel/polyisobutylene and polyisobutylene/polyisobutylene were obtained employing the analysis of the crack of viscoelastic material by Schapery.

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미세성형공정에서의 폴리머 레올로지의 정량화 (Quantitative rheology of polymers in high resolution structuring)

  • 김병희;김헌영;김호;김광순;강신일
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2003년도 춘계학술대회
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    • pp.1036-1042
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    • 2003
  • The hot embossing process has been mentioned as one of major nanoreplication techniques. This is due to its simple process, low cost, high replication fidelity and relatively high throughput. As the initial step of quantitating the embossing process , simple parametric study about embossing time have been carried out using high-resolution masters which patterned by the DRIE process and laser machining. Under the various embossing time, the viscous flow of thin PMMA films into microcavities during compression force has been investigated. Also, a study about simulating the viscous flow during embossing process has planned and continuum scale FDM analysis was applied on this simulation. With currently available test data and condition, simple FDM analysis using FLOW3D was made attempt to match simulation and experiment.

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나노스케일 재료 변형 거동을 위한 새로운 멀티스케일 접근법 (A New Approach of Multi-Scale Simulation for Investigating Nano-Scale Material Deformation Behavior)

  • 박준영
    • 한국기계가공학회지
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    • 제8권1호
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    • pp.43-47
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    • 2009
  • Recently, an approach for nano-scale material deformation has been developed that couples the atomistic and continuum approaches using Finite Element Method (FEM) and Molecular Dynamics (MD). However, this approach still has problems to connect two approaches because of the difference of basic assumptions, continuum and atomistic modeling. To solve this problem, an alternative way is developed that connects the QuasiMolecular Dynamics (QMD) and molecular dynamics. In this paper, we suggest the way to make and validate the MD-QMD coupled model.

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재료의 기계적 물성측정 시험장치를 위한 이중서보 시스템에 관한 연구 (Study of Dual Servo System for Measurement System of Mechanical Property)

  • 최현석;송치우;한창수;이형욱;최태훈;이낙규;나경환
    • 반도체디스플레이기술학회지
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    • 제2권2호
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    • pp.31-37
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    • 2003
  • This paper presents a measurement system of mechanical property using dual servo system. There are many kinds of method to measure material properties such as tensile test, indention and bending test. It is highly required to measure the properties of nano-sized material and structure. However, It is need more accurate measurement system, more stable and frequency response than conventional test. In this paper, we designed the dual servo system for a measuring instrument The dual servo system consisting of a coarse stage and a fine motion stage with VCM and PZT is proposed. Mechanical mechanism is designed with the leaf spring type of flexure hinge joint. Lead compensator is applied to this control system, and is designed by PQ method.

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고온수전해 수소극용 Cu/YSZ의 제조 및 특성 (Synthesis and Characteristic of Cu/YSZ Composite for High Temperature Electrolysis Cathode)

  • 홍현선;김종민;신석재
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2007년도 추계학술대회 논문집
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    • pp.101-104
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    • 2007
  • 700 $^{\circ}C$이상의 온도에서 실시되는 고온수전해는 다가오는 수소경제시대의 주요한 수소제조기 술로 주목되고 있다. 이 연구에서는 Ni보다 전기전도도가 우수하고 가격이 저렴한 Cu를 사용하여 고온수 전해 수소극용 Cu/YSZ 복합체를 기계적합금법에 의해 제조하여 미세구조를 관찰하였고 Cu/YSZ를 수소전극으로 한 반전지를 제조하여 수조제조 실험을 실시하였다. Cu/YSZ 복합체는 Cu와 YSZ를 6:4(vol%)의 조성비로 유성밀을 사용하여 400 rpm으로 24시간 동안 실시하여 제조하였다. 고에너지 볼밀 후 500 nm이하의 나노크기의 복합체가 제조되었으며 Cu입자에 YSZ가 고르게 분포되어 있었다. 수은압입법으로 측정한 기공률은 70%이고 기공크기는 평균 0.5 ${\mu}m$으로 미세한 기공으로 이루어져 있었다. 제조된 Cu/YSZ 복합체를 수소전극으로 한 반전지를 제조하여 수소제조 실험을 실시한 결과 Ni/YSZ 전극보다 수소제조 성능이 우수한 것으로 나타났다. Cu의 높은 열팽창계수와 낮은 녹는점을 보완하면 우수한 고온수전해용 전극재료로 사용될 것으로 판단된다.

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