• Title/Summary/Keyword: 나노정밀도

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Application of Quartz Crystal Microbalance to Understanding the Transport of Microplastics in Soil and Groundwater (토양-지하수내 미세플라스틱 거동 연구를 위한 수정진동자미세저울 기술 소개)

  • Kim, Juhyeok;Myeong, Hyeonah;Son, Sangbo;Kwon, Kideok D.
    • Korean Journal of Mineralogy and Petrology
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    • v.33 no.4
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    • pp.463-475
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    • 2020
  • Presence of microplastics in soil and groundwater has recently been reported and environmental concerns are raised as to the plastic pollution. In the subsurface environment, clay minerals and metal oxide minerals are commonly found as finely dispersed states. Because the minerals have high sorption capacities for diverse pollutants, interactions with mineral surface play an important role in the transport of microplastics in groundwater. Accordingly, environmental mineralogy investigating the interactions between microplastics and mineral surfaces is the essential research area to understand the fate and transport of microplastics in the subsurface environment. The microplastic-mineral surface research requires molecular- to nano-scale analyses to be able to probe the relatively weak interactions between them. The current report introduces a nano-scale analysis tool called quartz crystal microbalance (QCM) that can measure the sorbed/desorbed mass of nanoplastics on mineral surfaces at the level of a few nanograms (~10-9 g). This report briefly reviews the main principles in the QCM measurement and discusses applications of QCM to the environmental mineralogy research.

Preparation of Porous Polyacrylonitrile Nanofibers Membrane for the MF Application (MF 적용을 위한 다공성 PAN 나노섬유막의 제조)

  • Ahn, Hyeonryun;Jang, Wongi;Tak, Taemoon;Byun, Hongsik
    • Membrane Journal
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    • v.23 no.2
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    • pp.112-118
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    • 2013
  • Polyancrylonitrile nanofiber membrane (PAM) was prepared by using the electrospinning method with a solution of polyacrylonitrile (PAN) in DMF. The pore-diameter of PAMs and the number of PAM's layer were controlled for the microfiltration (MF) application. In addition, in order to improve the water-flux, AN-PEGMA copolymers have been synthesized via free radical polymerization with poly (ethylene glycol) methyl ether methacrylate and azobisisobutylronitrile (AIBN), and then PAN/AN-PEGMA nanofiber membranes (PAM/APM) were prepared by electrospinning with a mixture of PAN (9 wt%) and AN-PEGMA (3 wt%) in DMF (88 wt%). The prepared membranes were investigated with FT-IR and E.D.S. It was confirmed through scanning electron microscope (SEM), porometer, and porosity analysis that the porous membrane with a uniform diameter (400~600 nm) and a uniform pore characteristics (0.5~0.4 ${\mu}m$) was prepared. For the MF application, water-flux measurements were investigated and then the result was shown that the water permeability value of PAM/APMs introduced AN-PEGMA copolymers was relatively higher than that of the PVdF commercial membrane. From these results, PAN nanofiber membranes prepared by electrospinning could be utilized as a MF membrane.

Comparison on Accuracy of Static and Dynamic Contact Angle Methods for Evaluating Interfacial Properties of Composites (복합재료의 계면특성 평가를 위한 접촉각 방법의 정확도 비교)

  • Kwon, Dong-Jun;Kim, Jong-Hyun;Park, Joung-Man
    • Journal of Adhesion and Interface
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    • v.23 no.3
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    • pp.87-93
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    • 2022
  • To analyze the interfacial property between the fiber and the matrix, work of adhesion was used generally that was calculated by surface energies. In this paper, it was determined what types of contact angle measurement methods were more accurate between static and dynamic contact angle measurements. 4 types of glass fiber and epoxy resin were used each other to measure the contact angle. The contact angle was measured using two types, static and dynamic contact angle methods, and work of adhesion, Wa was calculated to compare interfacial properties. The interfacial property was evaluated using microdroplet pull-out test. Generally, the interfacial property was proportional to work of adhesion. In the case of static contact angle, however, work of adhesion was not consistent with interfacial property. It is because that dynamic contact angle measurement comparing to static contact angle could delete the error due to microdroplet size to minimize the surface area as well as the meniscus measuring error.

Microproperties and Fracture Behavior of Galvannealed Coating Layer of Automobiles (자동차용 합금화 용융아연도금강판의 도금층 미소물성 및 파괴 거동)

  • Park, Chun-Dal;Ko, Dae-Cheol;Kim, Byung-Min
    • Journal of the Korean Society for Precision Engineering
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    • v.24 no.3 s.192
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    • pp.91-99
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    • 2007
  • Fractures of galvannealed coating layer during actual press forming in automotive applications were observed by scanning electron microscopy in order to understand fracture mechanism. Fracture behaviors of galvannealed coating layer in extra deep drawing quality steels and high strength steels have been studied by performing the tests describing the representative plastic deformation in sheet metal forming such as uni-axial tensile test, compression test, bi-axial test and plane strain test. Growth and direction of cracks were deeply related to the plastic deformation modes and history. The material properties of galvannealed coating layer were investigated by nano-indentation test equipped with Berkovich diamond indentor for the specimens. Hardness and elastic modulus of the coating layer were higher than bared steels and that was the reason for crack of coating layer. Flat friction test and drawbead friction test were performed to observe the effect of the surface morphology on the frictional characteristics. The micro-plasto hydrodynamic lubrication were appeared and played an important role in reducing the coefficient of friction.

A Study on Processing of Auxiliary Electrodes for OLED Lighting Devices Using a Reverse Gravure-Offset or Gravure-Offset Printing (리버스 그라비아 옵셋 또는 그라비아 옵셋 프린팅을 이용한 조명용 OLED 소자 보조전극 형성 공정 연구)

  • Bae, Sung Woo;Kwak, Sun Woo;Kim, In Young;Noh, Yong-Young
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.6
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    • pp.578-583
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    • 2013
  • The lighting devices using organic light emitting diodes (OLEDs) are actively researched because of the various advantages such as high power efficiency and 2-dimensitonal lighting emitting. To commercialize those OLED lighting devices, the manufacturing cost must be downed to comparable price with conventional light sources. Here, we demonstrate a reverse gravure-offset or gravure off-set printed metal electrode for the auxiliary electrode for OLED lighting devices. For the fabricated OLED's auxiliary electrode, we used Ag nano-paste and printed metal grid structure with a line width and spacing of several ten and hundred micrometer by using gravure-offset printing. In the end the printing metal grid pattern are successfully achieved by optimization of various experimental conditions such as printing pressure, printing speed and printing delay time.

A Study on the Design of Flexible Display Considering the Failure Characteristics of ITO Layer (플렉시블 디스플레이에서 ITO층의 파괴 특성을 고려한 설계연구)

  • Kim, Min Gyu;Park, Sang Baek;Chae, Soo-Won
    • Journal of the Korean Society for Precision Engineering
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    • v.30 no.5
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    • pp.552-558
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    • 2013
  • In recent years the interest on flexible display has been increasing as a future display due to its bendable characteristics. An ITO(indium tin oxide) layer, which is part of a flexible display, can be broken easily while bending because it is made of brittle materials. This brittle property can cause the malfunction of flexible display. To analyze fracture characteristics of ITO layer, bending test was conducted commonly. However, it is not possible to know specific phenomena on bended ITO layer by simple bending test only. Accordingly, in this study, the FE(finite element) model is developed similarly to a real flexible display to analyze stress distribution of flexible display under bending condition, especially on ITO layer. To validate FE model, actual bending test was conducted and the test results were compared with the simulation results by measuring reaction forces during bending. By using the developed model, FE analysis about the effect of design parameter (Thickness & Young's Modulus of BL) on ITO Layer was performed. By explained FE analysis above, this research draws a conclusion of reliable design guide of flexible display, especially on ITO layer.

Fabrication of triboelectric nanogenerator for self-sufficient power source application (자가발전활용을 위한 마찰전기 나노발전소자의 제작)

  • Shin, S.Y.;Kim, S.J.;Saravanakumar, Balasubramaniam
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2013.05a
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    • pp.589-590
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    • 2013
  • The fast development of electronic devices towards wireless, portable and multi-functionality desperately needs the self-powered and low maintenance power sources. The possibility to coupling the nanogenerator to wearable and portable electronic device facilitates the self powered device with independent and self sustained power source. Nanogenerator has ability to convert the low frequency mechanical vibration to electrical energy which is utilized to drive the electronic device [1]. The self powered power source has the ability to generate the power from environment and human activity has attracted much interest because of place and time independent. The human body motion based energy harvesting has created huge impact for future self powered electronics device applications. The power generated from the human body motion is enough to operate the future electronic devices. The energy harvesting from human body motion based on triboelectric effect has simple, cost-effective method [2, 3] and meet the required power density of devices. However, its output is still insufficient to driving electronic devices in continues manner so new technology and new device architecture required to meet required power. In the present work, we have fabricated the triboelectric nanogenerator using PDMS polymer. We have studied detail about the power output of the device with respect to different polymer thickness and varied separation distance.

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Optimal Design and Performance Evaluation of PZT-driven Stage Using Min-Max Algorithm (Min-Max 알고리즘을 이용한 피에조 구동형 스테이지의 최적설계 및 성능평가)

  • Choi Kee-Bong;Han Chang Soo
    • Journal of the Korean Society for Precision Engineering
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    • v.22 no.9 s.174
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    • pp.130-136
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    • 2005
  • This paper presents an optimal design and the performance evaluation of two-axis nano positioning stage with round notched flexure hinges. A flexure hinge mechanism with round notched flexure hinges is to guide the linear motions of a moving plate in the nano positioning stage. A Min-Max algorithm is applied to the design of the flexure hinge mechanism for nano positioning stage. In the design process, the structure of the flexure hinge mechanism is fixed, then the radius of a round hole and the width of two round holes are chosen as design variables, and finally the do sign variables are calculated by the Min-Max algorithm. The machined flexure hinge mechanism, stack type PZTs for actuation and capacitance type displacement sensors for position measurement are assembled into the nano positioning stage. The experimental results of the manufactured nano positioning stage show the first modal resonance frequency of 197 Hz, the operating range of 40 um, and the resolution of 3 nm.

An investigation of tribology properties carbon nanotubes reinforced epoxy composites (표면 개질된 탄소나노튜브를 사용한 에폭시 복합재료의 마모특성에 관한 연구)

  • Sulong A.B.;Goak J.C.;Park Joo-Hyuk
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.663-667
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    • 2005
  • Surface modified carbon nanotubes were applied into the epoxy composites to investigate its tribological property. Carbon nanotubes reinforced epoxy composites were fabricated by casting. Effects to the tribological property of loading concentrations and types of surface modification of carbon nanotubes were investigated under sliding condition using linear reciprocal sliding wear tester. The results show that the small amount of carbon nanotubes into the epoxy exhibited lower weight loss than the pure epoxy. It is concluded that the effect of an enormous aspect ratio of carbon nanotubes surface area which wider than conventional fillers that react as interface for stress transfer. As increased the contents of carbon nanotubes, the weight loss from the wear test was reduced. And the surface modified carbon nanotubes show better tribological property than as produced carbon nanotubes. It is due that a surface modification of carbon nanotubes increases the interfacial bonding between carbon nanotubes and epoxy matrix through chemical bonding. Changes in worn surface morphology are also observed by optical microscope and SEM for investigating wear behaviors. Carbon nanotubes in the epoxy matrix near the surface are exposed, because it becomes the lubricating working film on the worn surface. It reduces the friction and results in the lower surface roughness morphology in the epoxy matrix as increasing the contents of the carbon nanotubes.

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A Study on a Foxtail Electrostatic Microactuator with a High Resolution (고해상도의 Foxtail형 정전력 마이크로구동기에 대한 연구)

  • Kim Man-Geun;Kim Young-Yun;Jo Kyoung-Woo;Lee Jong-Hyun
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2005.06a
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    • pp.1198-1201
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    • 2005
  • A new foxtail actuator driven by V-shape beam deflection using electrostatic force has been designed, fabricated and characterized for nano-resolution manipulators. The proposed foxtail mechanism was implemented using a pair of electrostatic actuators and a pair of holding actuators, which was analyzed based on the electromechanically coupled motion of voltage - displacement relation. The proposed actuator was fabricated onto Silicon-on-Insulator (SOI) wafer and its stepping characteristics were measured by micro optical interferometer consisting of integrated micromirror and optical fiber. The fabricated foxtail microactuator was successfully operated from 1nm to 76nm, and the magnitude of step displacement was controllable up from 26nm/cycles to 53nm/cycle by changing the voltage.

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