• Title/Summary/Keyword: 기계적물성

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Quality Characteristics of Seolgiddok added with Aloe Powder during Storage (알로에가루 첨가 설기떡의 저장기간에 따른 품질특성)

  • Yoon, Sook-Ja;Hwang, Su-Jung
    • Korean journal of food and cookery science
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    • v.22 no.5 s.95
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    • pp.650-658
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    • 2006
  • This study investigated the effects on the quality characteristics of the korean steamed rice cake, Seolgiddok of the addition of aloe powder at 0%, 1.5%, 3.0%, 4.5% and 6.0% and 4-days storage. The moisture content of the control 0% aloe, steamed rice cake was 47.76%, and steadily decreased with increasing powder addition to the lowest of 37.38% for the cake with 6.0% added. The moisture content was decreased with extending storage time in both the control and powder-added groups. The cohesiveness, springiness, adhesiveness, gumminess and chewiness of the cake tended to decrease with increasing powder content, while the hardness increased with both increasing powder content and extending storage time. The Hunter color value L in the chromaticity of the cake was significantly decreased with increasing powder addition. The a value of the control, 0% aloe steamed cake was -0.86, but became positive with red color with increasing powder content, The b value was significantly increased with increasing powder content. The powder addition inhibited the increase in bacteria number. The sensory characteristics of the cake. such as color, aloe flavor and taste, and bitterness were increased with increasing powder content, while the moist and soft feeling of the cake were more highly evaluated at lower powder content. The overall taste was judged to be best for the sample with 3% added powder. Accordingly, it was expected that a highly functional and healthy product with improved quality might be developed by the addition of aloe powder to the Korean steamed cake, Seolgiddok.

Physicochemical and Organoleptic Properties of Starch Isolated from Gamma-Irradiated Acorn (감마선 조사 도토리로부터 분리한 전분의 이화학적 및 관능적 특성)

  • Kwon, Joong-Ho;Kim, Soo-Jin;Lee, Jung-Eun;Lee, Soo-Jeong;Kim, Sung-Kon;Kim, Jeong-Sook;Byun, Myung-Woo
    • Korean Journal of Food Science and Technology
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    • v.34 no.6
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    • pp.1007-1012
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    • 2002
  • Physicochemical and organoleptic properties were investigated in starch extracted from acorn gamma-irradiated for insect control. Hunter's color L, a, and b values were unchanged upon irradiation at 0.25 to 10 kGy. Scanning electron microscopic observation revealed no changes with gamma irradiation at 1 kGy, that is effective for disinifestation, whereas 10 kGy resulted in some clefts on the starch surface. X-ray diffraction analysis showed patterns of both amorphous and crystalline regions were not different among the treatment groups. Water-binding property, swelling power, solubility, and gelatinization patterns of starch were influenced by irradiation dose, but 1 kGy dose was not detrimental to the physicochemical properties. Textural parameters of acorn gel were relatively stable, but significant reductions were found in hardness, adhesiveness, and chewiness in samples irradiated at 3 kGy or higher. Rrsults revealed that irradiation at 1 kGy or lower could be applied for insect control without causing apparent changes in physicochemical and organoleptic properties of acorn starch.

Bulk Polymerization of L-lactide with Mixed Aluminum Organometallic Catalysts (Al계 유기금속화합물 혼합촉매 시스템을 이용한 L-lactide 벌크중합 특성 연구)

  • Noh, Yee-Hyeon;Ko, Young-Soo
    • Polymer(Korea)
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    • v.36 no.1
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    • pp.53-58
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    • 2012
  • The differences between single and mixed aluminium catalyst systems in the bulk polymerization of L-lactide were studied. $Al(O-i-Pr)_3$, TMA, TOA and TIBA were employed for the mixed-catalyst systems, and TIBA was chosen as a reference catalyst. For the $Al(O-i-Pr)_3$/TIBA catalyst system, the conversion of polymerization increased as the composition of $Al(O-i-Pr)_3$ in the mixed catalyst increased. The molecular weight of the resulting PLA reached to about 13000 g/mol, and the polydispersity index of the polymer from the $Al(O-i-Pr)_3$/TIBA catalyst was slightly increased than that of single catalyst. The higher molecular weight tail or shoulder was revealed in the GPC curve. The conversion of the TOA/TIBA catalyst system decreased as the composition of TOA in the mixed catalyst increased. The molecular weight of PLA prepared with TOA/TIBA catalysts increased up to 14000 g/mol. The Al compounds-mixed catalysts could produce a higher molecular weight tail or shoulder in the GPC curve, which may result in enhancement of mechanical properties of PLA.

Effects of Tempering Condition on the Microstructure and Mechanical Properties of 30MnB5 Hot-Stamping steel (핫스탬핑용 30MnB5강의 템퍼링 조건에 따른 미세조직 및 기계적 물성 연구)

  • Jeong, Junyeong;Park, Sang-Cheon;Shin, Ga-Young;Lee, Chang Wook;Kim, Tae-Jeong;Choi, Min-Su
    • Korean Journal of Metals and Materials
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    • v.56 no.11
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    • pp.787-795
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    • 2018
  • The effects of tempering condition on the microstructure and mechanical properties of 30MnB5 hot stamping steel were investigated in this study. Before the tempering, hot-stamped 30MnB5 steel was composed of only ${\alpha}^{\prime}$-martensite microstructure without precipitates. After the tempering at $180^{\circ}C$ for 120 min, nano-sized ${\varepsilon}$-carbides were precipitated in the ${\alpha}^{\prime}$-martensite laths. After tempering at $250^{\circ}C$ for 60 min, cementite was precipitated along the ${\alpha}^{\prime}$-martensite lath boundaries. The cementite was also observed in the specimens tempered at $350^{\circ}C$ for 30 min and $450^{\circ}C$ for 6 min, respectively. The globular ${\alpha}$-ferrite appeared at $350^{\circ}C-30min$ tempering, and the volume fraction of ${\alpha}$-ferrite increased when the tempering temperature was increased. The yield strength increased after tempering, and it reached a peak with the tempering condition of $180^{\circ}C-120min$, due to the nano-sized precipitates in the ${\alpha}^{\prime}$-martensite lath. After the tempering, the steel's ultimate tensile strength (UTS) was decreased due to the reduction in dislocation density and C segregation to lath boundaries. The highest elongation was observed at the $180^{\circ}C-120min$ tempering condition, due to the reduction of residual stress, and the lack of precipitates along the lath boundaries. The $180^{\circ}C-120min$ tempering condition was considered to have outstanding crash performance, according to toughness and anti-intrusion calculation results. In drop tower crash tests, the 30MnB5 door impact beam tempered at $180^{\circ}C$ for 120 min showed better crash performance compared to a 22MnB5 door impact beam.

Radiation Synthesis and Anti-inflammatory Evaluation of Polysaccharide Hydrogels from Ulmus Davidiana Var. Japonica (방사선을 이용한 느릅나무 추출 다당류가 함유된 하이드로젤의 제조 및 항염증성 평가)

  • Gwon, Hui-Jeong;Park, Eun Ji;Choi, Jong-Bae;Lim, Jong-Young;Jeong, Jin-Oh;Shin, Young-Min;Jeong, Sung In;Park, Jong-Seok;Lim, Youn-Mook;Choi, Young-Hun;Kim, Sang-Suk
    • Polymer(Korea)
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    • v.38 no.1
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    • pp.69-73
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    • 2014
  • In this study, polysaccharide-poly(vinyl alcohol) (PVA) hydrogels were prepared by using ${\gamma}$-ray and evaluated for potential application as an anti-inflammation patch. Ulmus davidiana var. japonica (UD), one of polysaccharides has been particularly used as an oriental remedy for the treatment of inflammation and ulcers. PVA as a biocompatible polymer and glycerin as a moisturizer were blended with the UD, and its hydrogels were prepared by radiation crosslinking. Characterizations for UD hydrogels were performed by using cytotoxicity assay, antioxidant activity test, and physicochemical test such as gel fraction ratio, and swelling behavior. The results showed that these UD hydrogels had excellent physical properties, anti-inflammation activity, and non-cytotoxicity on the cells. Therefore, these polysaccharide based-UD hydrogels can be effectively used as an inflammation patch.

Quality Characteristics of Backsulgi with Dextrinized Rice (호정화에 의한 백설기의 품질특성)

  • Doo, Hwa-Jin;Lee, Eun-Suk;Kim, Yong-Ro;Shim, Jae-Yong
    • Food Engineering Progress
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    • v.13 no.4
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    • pp.289-296
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    • 2009
  • The purpose of this study was to investigate the effect of dextrinization methods (dry oven and roaster) and the ratio of dextrinized rice on the quality of Backsulgi during storage. The moisture content significantly increased with increasing the amount of dextrinized rice regardless of dextrinization methods. As the ratio of dextrinized rice increased, the L value of the Backsulgi decreased, but the a and b values increased. The a and b values of dry oven method were higher than those of roaster method due to their thermal denaturalization. However, there were no significant pattern's change in sample's colors during storage. In the texture profiles, the hardness, cohesiveness, gumminess and chewiness significantly decreased with increasing the amount of dextrinized rice depending on the dextrinization methods and the ratios. The time constant (1/k) of the Backsulgi with dextrinized rice comparatively higher than that of control and appeared to be the highest in the Backsulgi formulated by 100% of dextrinized rice. In the sensory evaluation, Backsulgi with dextrinized rice over 30% after 1day storage showed higher value in overall quality and lower value in hardness than control. The addition of 30% dextrinized rice made by roaster showed the most effective on the quality and retrogradation of Backsulgi.

A Study on the Atmospheric Pressure Control of the VARTM Process for Increasing the Fiber Volume Fraction and Reducing Void (섬유부피분율 증가와 공극 감소를 위한 VARTM 공정의 대기압 제어에 관한 연구)

  • Kwak, Seong-Hun;Kim, Tae-Jun;Tak, Yun-Hak;Kwon, Sung-Il;Lee, Jea-Hyun;Kim, Sang-Yong;Lee, Jong-Cheon
    • Composites Research
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    • v.34 no.2
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    • pp.88-95
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    • 2021
  • VARTM (Vacuum-assisted resin transfer molding) process is a low-cost process technology and affiliated with OoA (Out of Autoclave). Besides, it has been widely used in various fields. However, because of its lower quality than the autoclave process, it isn't easy to apply the VARTM process to the aerospace industry, which requires high reliability. The main problem of the VARTM process is the loss of mechanical properties due to the low fiber volume fraction and high void content in comparison to the autoclave. Therefore, many researchers have studied to reduce void and increase fiber volume fraction. This study examines whether the method of controlling atmospheric pressure could increase the fiber volume fraction and reduce void during the resin impregnation process. Reliability evaluation was confirmed by compressive strength test, fiber volume fraction analysis, and optical microscopy. As a result, it was confirmed that increasing the atmospheric pressure step by step in the VARTM process of impregnating the preform with resin effectively increases the fiber volume fraction and reduces void.

Synthesis and Characterization of 4-Component Polyimide Films with Various Diamine and Dianhydride Compositions (다양한 조성 변화에 따른 4성분계 폴리이미드 필름 제조와 물성분석)

  • Park, Yun Jun;Yu, Duk Man;Choi, Jong Ho;Ahn, Jeong-Ho;Hong, Young Taik
    • Applied Chemistry for Engineering
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    • v.22 no.6
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    • pp.623-626
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    • 2011
  • Various poly(amic acid)s were synthesized from PMDA/BPDA/p-PDA/ODA with different mole ratios and effectively converted into 4-component polyimide films by thermal imidization. The chemical structures and thermo-mechanical properties of polyimide films were examined using Fourier transform infrared spectroscopy (FT-IR), thermo-gravimetric analyzer (TGA), thermo-mechanical analyzer (TMA), dynamic mechanical analyzer (DMA) and universal tensile machine (UTM). The tensile strength, modulus, and thermal properties of polyimides films increased with the amount of rigid PMDA and p-PDA, while the elongation and moisture absorption of polyimide films increased with the amount of flexible BPDA and ODA. One of 4-component polyimide films exhibited a similar coefficient of thermal expansion (CTE) value to that of copper when it was composed of PMDA : BPDA : p-PDA : ODA with the ratio of 5 : 5 : 4 : 6. Thus, this polyimide film could be useful for a base film for flexible copper clad laminates (FCCL) of flexible printed circuit boards.

A Review on Development of PPO-based Anion Exchange Membranes (PPO 기반 음이온 교환막 소재 개발 동향)

  • An, Seong Jin;Kim, Ki Jung;Yu, Somi;Ryu, Gun Young;Chi, Won Seok
    • Membrane Journal
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    • v.31 no.6
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    • pp.371-383
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    • 2021
  • Anion exchange membranes have been used for water electrolysis, which can produce hydrogen, and fuel cells, which can generate electrical energy using hydrogen fuel. Anion exchange membranes operate based on hydroxide ion (OH-) conduction under alkaline conditions. However, since the anion exchange membrane shows relatively low ion conductivity and alkaline stability, there is still a limit to its commercialization in water electrolysis and fuel cells. To address these issues, it is important to develop novel anion exchange membrane materials by rationally designing a polymer structure. In particular, the polymer structure and synthetic method need to be controlled. By doing so, for polymers, the physical properties, ionic conductivity, and alkaline stability can be maintained. Among many anion exchange membranes, poly(2,6-dimethyl-1,4-phenylene oxide) (PPO) is commercially available and easily accessible. In addition, the PPO has relatively high mechanical and chemical stability compared to other polymers. In this review, we introduce the recent development strategy and characteristics of PPO-based polymer materials used in anion exchange membranes.

Low-Temperature Characteristics of Type 4 Composite Pressure Vessel Liner according to Rotational Molding Temperature (타입 4 복합재 압력용기 라이너의 회전 성형 온도에 따른 저온 특성)

  • Jung, Hong-Ro;Park, Ye-Rim;Yang, Dong-Hoon;Park, Soo-Jeong;Kim, Yun-Hae
    • Composites Research
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    • v.35 no.3
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    • pp.147-152
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    • 2022
  • Low-temperature characteristics according to internal temperature conditions during rotational molding of Type 4 pressure vessel liners were studied in this paper. Since rotational molding has a sensitive effect on the formability of the liner depending on the temperature conditions, the temperature conditions for the polyamide used should be accurately set. The structural changes of polyamide as the liner material was analyzed the surface by atomic force microscope (AFM), and the crystallinity measured with a differential scanning calorimeter (DSC) is used to evaluate the change of the mechanical strength value at low temperature. In addition, the formability of the liner was confirmed by observation of the yellow index inside the liner. As a result, as the melting range of the internal temperature becomes wider, the yellow index shows a lower value, and the elongation and impact characteristics at low temperatures are improved. It was also confirmed that the structure of the polyamide was uniform and the crystallinity was high by AFM and DSC. These experimental results contribute to the improvement of characteristics at low temperatures due to changes in temperature conditions during rotational molding.