• Proceedings of the Korea Crystallographic Association Conference
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• 2002.11a
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• pp.22-23
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• 2002

Titanium은 높은 강도, 낮은 밀도, 부식에 대한 저항 등, 타 금속에 비해 월등히 뛰어난 성질을 가지고 있기 때문에 산업 전반에 거쳐 그 응용이 크게 증가하고 있으며, 특히 고온에서의 응용이 중요성을 띠게 됨에 따라 고온으로의 상전이 관계에 따른 구조적 규명이 필요하다. 순수한 titanium은 상온에서 조밀충진 육방정계의 α-상구조(a=2.953Å, c=4.683 Å, P6₃/mmc)를 이루고 있으나, 대략 880℃ 이상에서는 β-상의 체심입방정계 (a=3.320Å, Im3m)로 상전이가 되는 것으로 알려져 있다. 이에 대한 대부분의 연구가 kinetics와 thermodynamics에 관련되어 있으며, TEM을 이용한 직접가열실험은 거의 전무한 상태이다. 본 실험에서는 TEM 직접가열을 통하여 titanium의 고온에서의 상전이와 가열시 발생할 수 있는 산화층 형성을 연구하였다. TEM 시편은 순도 99.94％의 titanium foil(Alfa Aesar, ＃00360, 0.025mm thick)를 이용하였고, 분석 장비로는 에너지여과 기능이 있는 TEM(EM912 Omega, Carl Zeiss)과 Gatan사의 double-tilt heating holder를 사용하였다. Titanium의 상전이를 관찰하기 위해 900℃ 까지 분당 10℃ 의 속도로 가열을 하였다. 통계적 분석 오차를 줄이기 위해 서로 다른 4군데의 관찰영역을 선택하여, 상온 - 600℃ - 900℃ - 상온의 단계별로 회절패턴을 관찰 및 기록하였고, 발생 가능한 산화에 대해서는 동일한 장비를 사용하여 EDS 분석을 하였다. 상온에서의 서로 다른 영역의 회절패턴들은 결함의 존재에 상관없이, 온도가 증가함에 따라 그 결함수가 증가하게 된다. 특히 600℃ 에서는 쌍정과 관련된 회절점들이 본래의 회절점 주위에 형성되어있지만, 각 면들의 격자상수의 변화는 나타나지 않았다. 그러나 900℃ 에서는 쌍정에 의한 회절점의 수가 증가하며, 회절점 사이에 발달한 뚜렷한 막대모양의 강도분포와 격자상수의 변화를 관찰할 수 있었다. 다시 상온으로 냉각시킨 후 관찰한 각각의 회절패턴에서는 격자 상수의 감소와 함께 900℃에 보여진 막대 모양의 강도분포와 쌍정에 의한 회절점들이 여전히 남아있었다. EDS분석 결과 가열 실험을 통해 시편이 열적 산화가 되어 있음을 확인 할 수 있었다. 순수한 titanium의 α-상에서 β-상으로의 상전이를 파악할 수 있는 격자상수의 변화자체는 매우 작은 값이기 때문에 상온과 900℃ 에서 기록된 전자회절패턴 상에서의 면간거리와 면간각도의 측정만으로는 상전이 여부를 명확히 구별할 수 없었다. 그러나, 결함에 의한 상변화가 900℃ 에서 심하게 관찰되어지는 것은 상전이와 관계가 있는 것으로 볼 수 있다. 고온에서 상온으로의 가역적 반응을 관찰할 수 없었던 이유는 열적산화로 생긴 산화층의 산소원자들이 고온의 상전이 과정 중에 Ti 원자와 반응이 일어나 TiO/sub X/ 구조로 전이되었기 때문으로 추정하고 있다.

• Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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• 2001.10a
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• pp.363-366
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• 2001

The present process of grading leather quality by the rare eyes is not reliable. Because inconsistency of grading due to eyes strain for long time can cause incorrect result of grading. Therefore it is necessary to automate the process of grading quality of leather based on objective standard for it. In this paper, leather automatic classification system consists of the process obtaining the information of leather and the process grading the quality of leather from the information. Leather is graded by its information such as texture density, types and distribution of defects. This paper proposes the algorithm which sorts out leather information like texture density and defects from the gray-level images obtained by digital camera. The density information is sorted out by the distribution value of Fourier spectrum which comes out after original image is converted to the image in frequency domain. And the defect information is obtained by the statistics of pixels which is relevant to Window using searching Window after sort out boundary lines from preprocessed images. The information for entire leather is used as standard of grading leather quality, and the proposed algorithm is practically applied to machine vision system.

• Journal of the Korean Society for Nondestructive Testing
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• v.15 no.2
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• pp.378-385
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• 1995

The ultrasonic non-destructive testing uses the directivity of the ultrasonic pulse wave which propagates in one direction. The directivity is expressed as the relationship between the propagate direction and its sound pressure. The directivity of ultrasonic wave is closely related to determination of probe arrangement, testing sensitivity, scanning pitch and defect location and characterization. The paper measured the directivity of shear wave, which reflected from artificial defect located in weld metal zone in butt welded joint similar model made of pyrex glass by using visualization method. 2 MHz and 4 MHz angle probes were used to measure the directivity of reflection wave at the artificial defect. The directivity of shear waves reflected from the defect was different according to the probe position and the shape of butt welded joint. The difference of directivity of reflection wave was existed between 2 MHz and 4 MHz angle probes. The angle of reflection wave became equal to angle of incidence as increase of the height of excess metal.

• Korean Journal of Crystallography
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• v.5 no.2
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• pp.67-77
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• 1994

From the Y3-3xNd3xAl5O12single crystals grown by the Czochralski technique, various types of defects were detected and 1) the reason of opical in homogeneous phases, 2) the mechanism of formation of the iridum metal inclusions accompanying bubbles, and 3) the mechanism of formation of the core and facet were analysed After preparing the wafers of the <111> growth parallel, defscts were observed by the polarising microscope using a photoelasic effect and then some images of stress-birefringence were compared to their etch Pits patterns.

• Journal of the Korean Vacuum Society
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• v.18 no.6
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• pp.447-452
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• 2009

Enhance signal-to-noise ratio, Coincidence Doppler Broadening positron method has been applied to study of characteristics of BaSrFBr:Eu film sample. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. The films were exposed by 0, 3, 5, and 7.5 MeV proton beams ranging from 0 to $10^{13}$ ptls. The S-parameter values were increased as increasing the exposed time and the energies, that indicated the defects generate more.

• Korean Journal of Optics and Photonics
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• v.28 no.1
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• pp.1-8
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• 2017

A method for inspecting defects in display substrates utilizing Fourier optics is proposed in this paper. A cost-effective inspection system can be realized with the proposed method, because it does not require a high-magnification microscope. Also, the proposed method can avoid tight tolerance for variations in displacement between substrate and camera, which is stems from shallow depth of field of the high-magnification microscope. In addition, possible damage caused by collisions between substrate and the inspection equipment can be avoided. The decision algorithm can be simpler than for a conventional inspection system, because spatial shift of periodic substrate patterns does not affect the intensity distribution of the diffracted light, by the Fourier transform property. The proposed method is explained with numerical studies, and experiments are carried out to check its feasibility for color-filter substrates of a liquid-crystal display.

• Journal of Digital Convergence
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• v.11 no.11
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• pp.335-342
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• 2013

In this study, reliability software cost model considering logarithmic fault detection rate based on observations from the process of software product testing was studied. Adding new fault probability using the Goel-Okumoto model that is widely used in the field of reliability problems presented. When correcting or modifying the software, finite failure non-homogeneous Poisson process model. For analysis of software cost model considering the time-dependent fault detection rate, the parameters estimation using maximum likelihood estimation of inter-failure time data was made. In this research, Software developers to identify the best time to release some extent be able to help is considered.

• Journal of Advanced Marine Engineering and Technology
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• v.37 no.2
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• pp.135-143
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• 2013

Friction Stir Welding (FSW) was developed, it is successfully commercialized in the field of transportation vehicles. In this study, we analyzed the defects of A2024-T4 alloy using non-destructive test of radiograph, ultrasonic, electrical conductivity and destructive test of microstructure observation, tensile strength. As the results of experiment, mapping of defects was obtained. Fine defects which were not detected in radiograph test were detected in ultrasonic test, and it enabled efficient detection of defects by difference of sound pressure and color. The values of electrical conductivity was decreased as amount of defects was increasing. Joint efficient of defect-free weldment that found by non-destructive and destructive test was 91%. Therefore it was considered that non-destructive test of friction stir welded A2024-T4 Alloy was an efficient method.

• Proceedings of the Korean Vacuum Society Conference
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• 2010.02a
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• pp.260-260
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• 2010

OTFT소자는 각 박막계면간의 접촉성에 따라 그 성능이 좌우 된다는 것은 널리 알려진 사실이다. 즉 박막계면간의 접촉성 저하는 계면간의 결함을 형성하여 OTFT소자 성능을 저하시킨다. 이러한 결함을 고품질의 자기조립단분자막을 제작함으로써 박막계면간 결함을 최소화 할 수 있다. 이러한 고품질의 자기조립단분자막 형성은 박막계면간의 결함을 최소화 하기때문에 고성능OTFT소자 제작시 박막계면간 접촉성 향상에 효율적으로 적용할 수 있을것이다. 이 논문에서는 계면간의 접촉성 향상을 위해 실리콘 웨이퍼 위에 3-Aminoproplytriethoxtsilane과 용매인 무수톨루엔을 이용하여 고품질의 자기조립단분자막을 제작 하였으며 고품질을 자기조립단분자막 성장 조건을 찾기 위해 엄격한 수분조절 및 APS농도, 담근시간, 온도를 조절하여 각기 다른 조건의 샘플을 제작하였다. 또한 APS성장 분포를 알기위하여 접촉각 측정기를 이용하여 접촉각을 측정 하였고 AFM 이용하여 실리콘 웨이퍼에 생성된 박막의 균질도를 측정하였다. 그 결과 APS농도(33%) 24시간 $25^{\circ}C$, APS농도(33%) 24시간 $70^{\circ}C$, APS농도(33%) 72시간 $25^{\circ}C$, APS농도 (33%) 72시간 $70^{\circ}C$ 샘플이 기존에 알려진 APS 접촉각인 $19^{\circ}C{\sim}21^{\circ}C$ 접촉각이 나왔으며 AFM 이미지 또한 높은 균질도를 보였다. 이 결과 고품질의 APS단분자막은 농도와 시간 그리고 온도에 영향은 받으며 이렇게 완성된 단분자막은 높은 균질도를 가지게 된다. 현재 실험을 통해 얻어진 고품질의 자기조립단분자막 성장 조건을 이용하여 OTFT소자 제작하고 있으며 고품질의 자기조립단분자막 형성에 의해 결함을 최소화 하므로써 박막계면간 옴성결합을 형성하여 OTFT소자의 성능 향상이 기대되어 진다.

• Proceedings of the Korean Institute of Information and Commucation Sciences Conference
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• 2022.10a
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• pp.570-573
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• 2022

This paper presents the identification of void diameters for a cast-resin transformer using an artificial neural network (ANN) model. A PD signal was measured by the Rogowski coil sensor which has the planar and thin structures fabricated on a printed circuit board (PCB), and the PD electrode system was fabricated to simulate a PD defect by a void. In addition, void samples with different diameters were fabricated by injecting air in a cylindrical aluminum frame using a syringe during the epoxy curing process. To identify the diameter of void defects, PD characteristics such as the discharge magnitude, pulse count, and phase angle were extracted and back propagation algorithm (BPA) was designed using virtual instrument (VI) based on the Labview program. From the experimental results, the BPA algorithm proposed in this paper has over 90% accurate rate to identify the diameter of void defects and is expected to use reference data of maintenance and replacement of insulation for cast-resin transformers in the on-site PD measurement.