• Title/Summary/Keyword: 감마선 분광법

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Study on the Measurement of Radon concentrations in soil samples using γ-spectrometer (γ-spectrometer를 이용한 토양시료의 라돈농도 측정법에 관한 연구)

  • Kang, Sunga;Lee, Sangsoo;Choi, Guirack;Lee, Junhaeng
    • Journal of the Korean Society of Radiology
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    • v.7 no.1
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    • pp.31-36
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    • 2013
  • The radioactive gas radon ($^{222}Rn$), which is generated from the decay process of uranium ($^{238}U$) originating from the soil of more than 85 percent higher the porosity of the soil, the soil can radiate out the possibility that many isotopes. In order to protect the human body from radon, above all, the development of accurate measurement techniques to formulate appropriate measures should be followed. This study Gamma-ray spectrometry using a high purity germanium (HPGe) detector, if you want to measure radon unstable the nature radiation of the background problems can be reduced, radium and radon daughter nuclides after radioactive equilibrium leads to Radon concentration was measured, the soil samples from the Gamma-ray emitting nuclides, and the energy spectrum is analyzed.

The Characterization of MgB2 Thin Film by Slow Positron Annihilation Spectroscopy (저에너지 양전자 소멸 분광법을 이용한 MgB2 박막 구조 특성)

  • Lee, C.Y.;Kang, W.N.;Nagai, Y.;Inoue, K.;Hasegawa, M.
    • Journal of the Korean Vacuum Society
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    • v.17 no.2
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    • pp.160-164
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    • 2008
  • The Characterization of $MgB_2$ Thin Film by Slow Positron Annihilation Spectroscopy Enhance signal-to-noise ratio, slow positron coincidence Doppler Broadening method has been applied to study of characteristics of $MgB_2$ superconductor film, which were performed at 30 K and 50 K sample temperature near Tc of it. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. The S-parameter values were increased then decreased while the positron implantation energies were increasing, that indicated the diffusion into the samples. The S-parameters of the anisotropic 1 ${\mu}m$ $MgB_2$ thin film which were implanted by positrons at 10 keV are 0.567 at 30 K and 0.570 at 50 K. It is believed that the positrons annihilate with normal-electrons instead of super-electrons in the $MgB_2$ superconductor.

Comparison of Photostimulated Luminescence, Thermoluminescence, and Electron Spin Resonance Spectroscopic Analyses on Dried-spices Irradiated by Gamma Ray and Electron Beam (감마선 및 전자선 조사 처리 건조향신료에 대한 광자극발광, 열발광 및 전자스핀공명의 분광학적 분석 비교)

  • Jeong, Jin-Hwa;Ahn, Jae-Jun;Baek, Ji-Yeong;Kim, Hyo-Young;Kwon, Joong-Ho;Jin, Chang-Hyun;Jeong, Il-Yun
    • Korean Journal of Food Science and Technology
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    • v.46 no.2
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    • pp.256-261
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    • 2014
  • This study was conducted to determine the effect of gamma-ray and electron-beam irradiation on dried spices (black pepper, red pepper, parsley, and basil) using the photostimulated luminescence (PSL), thermoluminescence (TL) and electron spin resonance (ESR) methods. The spices were irradiated at 0, 1, 5, and 10 kGy. All non-irradiated spices had photon counts (PCs) less than 700 PCs. The PCs of three irradiated spices (red pepper, parsley, and basil) were clearly distinguishable from those of non-irradiated ones, exhibiting PSL signals higher than 5000 PCs. However, negative PSL counts (<700 PCs) were obtained for most irradiated black pepper, except those irradiated with 5 kGy gamma rays and 10 kGy electron-beams. TL glow curves of the irradiated spices showed a higher peak at $150-250^{\circ}C$. TL ratios were found to be less than 0.1 for non-irradiated spices and higher than 0.1 for irradiated ones. No ESR signal was observed for any irradiated spice except red pepper, which displayed cellulose-based ESR spectra. Therefore, the results suggest that the PSL, TL, and ESR methods are effective detection techniques for dried spices irradiated with electron beams as well as gamma rays.

Investigation of Proton Irradiated Effect on n, p type Silicon by Positron Annihilation Method (양전자 소멸 측정에 의한 n, p형 실리콘 구조 특성)

  • Lee, C.Y.
    • Journal of the Korean Vacuum Society
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    • v.21 no.5
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    • pp.225-232
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    • 2012
  • It is described that the proton beam induceds micro-size defects and electronic deep levels in n or p type single crystal silicon. Positron lifetime and Coincidence Doppler Broadening Positron Annihilation Spectroscopy were applied to study of characteristics of p type and n type silicon samples. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. The samples were exposed by 3.98 MeV proton beams ranging between 0 to ${\sim}10^{14}$ particles. The S-parameter values strongly depend on the irradiated proton beam, that indicated the defects generate more. Positron lifetime shows that positrons trapped in vacancies and lifetime ${\tau}_2$ increased according to proton irradiation.

The Characterization of Proton Irradiated BaSrFBr:Eu Film by the Coincidence Doppler Broadening Positron Annihilation Spectroscopy (동시계수 양전자 소멸 측정에 의한 양성자 조사된 BaSrFBr:Eu 박막 특성)

  • Kim, J.H.;Nagai, Y.;Lee, C.Y.
    • Journal of the Korean Vacuum Society
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    • v.18 no.6
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    • pp.447-452
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    • 2009
  • Enhance signal-to-noise ratio, Coincidence Doppler Broadening positron method has been applied to study of characteristics of BaSrFBr:Eu film sample. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. The films were exposed by 0, 3, 5, and 7.5 MeV proton beams ranging from 0 to $10^{13}$ ptls. The S-parameter values were increased as increasing the exposed time and the energies, that indicated the defects generate more.

Synthesis of Electroactive PAAc/PVA/PEG Hydrogel Soft Actuator by Radiation Processing and Their Dynamic Characteristics (방사선을 이용한 전기 활성 PAAc/PVA/PEG 하이드로겔 소프트 액추에이터의 제조 및 구동 특성 분석)

  • Shin, Yerin;Kim, So Yeon
    • Applied Chemistry for Engineering
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    • v.30 no.6
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    • pp.698-706
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    • 2019
  • Over the last few decades, there have been a lot of efforts to develop soft actuators, which can be external stimuli-responsive and applied to the human body. In order to fabricate medical soft actuators with a dynamic precision control, the 3D crosslinked poly(acrylic acid) (PAAc)/poly(vinyl alcohol) (PVA)/poly(ethylene glycol) (PEG) hydrogels were synthesized in this study by using a radiation technique without noxious chemical additives or initiators. After irradiation, all hydrogels showed high gel fraction over 75% and the ATR-FTIR spectra indicated that PAAc/PVA/PEG hydrogels were successfully synthesized. In addition, the gel fraction, equilibrium water content, and compressive strength were measured to determine the change in physical properties of PAAc/PVA/PEG hydrogels according to the irradiation dose and content ratio of constituents. As the irradiation dose and amount of poly(ethylene glycol) diacrylate (PEGDA) increased, the PAAc/PVA/PEG hydrogels showed a high crosslinking density and mechanical strength. It was also confirmed that PAAc/PVA/PEG hydrogels responded to electrical stimulation even at a low voltage of 3 V. The bending behavior of hydrogels under an electric field can be controlled by changing the crosslinking density, ionic group content, applied voltage, and ionic strength of swelling solution.

Simultaneous Determination of Titanium, Zirconium and Niobium by Reactor Neutron Activation (원자로 중성자에 의한 티탄, 지르코늄 및 니오브의 동시 정량)

  • Chul Lee;Yung Chang Yim;Koo Soon Chung
    • Journal of the Korean Chemical Society
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    • v.18 no.1
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    • pp.40-46
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    • 1974
  • The fission neutron reactions of $^{47}Ti(n.p)^{47}Sc$ and $^{93}Nb(n,{\alpha})^{90m}Y$, along with epicadmium neutron reaction of $^{96}Zr(n,{\gamma})^{97}Zr$ were used for the simultaneous determination of Ti, Nb and Zr in synthetic mixture. Prior to neutron irradiation, Ti, Zr and Nb in the mixture were separated together in one group through the cation exchange column of Dowex $50{\times}8$ resin using 0.5 M ${\alpha}$-hydroxy-iso-butyric acid as the eluent. After irradiation of the eluate the product nuclides, $^{97}Zr$, ^{47}Sc$ and ^{90m}Y$, were eluted sequentially through the same column with 0.5 M ${\alpha}$-HIBA, 0.5 M ${\alpha}$-HIBA-1 N HNO_3 and 0.5 M ${\alpha}$-HIBA-2 N HNO_3$ solution, respectively. The gamma-ray spectrometry was used for the measurement of the gamma-ray activities of the eluted nuclides. The detection limits of Nb, Ti and Zr were found to be 0.2 %, 0.01 % and 0.002 %, respectively.

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Proton Irradiated Cz-Si by the Coincidence Doppler Broadening Positron Annihilation Spectroscopy (동시계수 양전자 소멸 측정에 의한 양성자 조사된 Si 구조 특성)

  • Lee, K.H.;Lee, C.Y.
    • Journal of the Korean Vacuum Society
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    • v.20 no.5
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    • pp.367-373
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    • 2011
  • It is described that the proton beam induces micro defects and electronic deep levels in Cz single crystal silicon. Enhance signal-to-noise ratio, Coincidence Doppler Broadening Positron Annihilation Spectroscopy has been applied to study of characteristics of p type and n type silicon samples. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. The samples were exposed by 4.0 MeV proton beams ranging from 0 to ${\sim}10^{14}$ ptls. The S-parameter values were increased as increasing the irradiated proton beam, that indicated the defects generate more.

Natural Radioactivity of Soils by Bed Rocks Distributed in the Keum River Area (금강유역 기반암 토양의 자연방사능 특성)

  • Lee, Kil-Yong;Yoon, Yoon-Yeol;Cho, Soo-Young;Lee, Jung-Hwa;Lee, Jin-Soo;Koh, Kyung-Seok;Kim, Yong-Je
    • Journal of Soil and Groundwater Environment
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    • v.14 no.2
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    • pp.10-16
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    • 2009
  • Characteristics of natural radioactivity were investigated for soils collected from seven sites of different bed rocks distributed in the Keum River area of Korea by the use of a Gamma-ray spectrometry. Specific activity (SA) and SA ratio (SAR) of typical naturally occurring radioactive nuclide such as $^{226}$Ra, $^{228}$Ac and $^{40}$K were determined for the soil samples. The SA values of $^{226}$Ra, $^{228}$Ac and $^{40}$K in 41 soils of 7 sites are 26.7-485 (74.2 ${\pm}$ 72.2), 30.9-157 (90.7 ${\pm}$ 32.7) and 203-1558 (990 ${\pm}$ 203) Bq/kg, respectively. The SA of $^{226}$Ra has very different values by the soils and the sites. Especially the SA of $^{226}$Ra in a soil sample of Ogcheon site is 485 Bq/kg while most SA of 41 soil samples are < 100 Bq/kg. SA of $^{228}$Ac has a little different values with the soils and sites, however the SA of $^{40}$K has almost constant values in all soil samples. The SAR values of $^{26}$Ra/$^{228}$Ac, $^{226}$Ra/$^{40}$K and $^{228}$Ac/$^{40}$K in 41 soils of 7 sites are 0.343-6.11 (0.865 ${\pm}$ 0.883), 0.0258-0.759 (0.0814 ${\pm}$ 0.1l17) and 0.0373-0.178 (0.0945 ${\pm}$ 0.0373), respectively. The SARs of $^{226}$Ra/$^{228}$Ac and $^{226}$Ra/$^{40}$K have very different values by the soils and the sites, however the SAR of $^{228}$Ac/$^{40}$K has a little difference by the soil and sites.

Cesium Radioisotope Measurement Method for Environmental Soil by Ammonium Molybdophosphate (환경토양에서 몰리브도인산 암모늄을 이용한 세슘 동위원소 평가방법)

  • Choe, Yeong-hun;Seo, Yang Gon
    • Clean Technology
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    • v.22 no.2
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    • pp.122-131
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    • 2016
  • Caesium radioisotopes, 134Cs and 137Cs which come from the atmospheric nuclear tests and discharges from nuclear power plants, are very important to study artificial radioactivity. In this work, in order to lower the minimum detection activity (MDA) we investigated environmental radioactivity according to the Environment Measurement Laboratory procedure by 137Cs and 134Cs which is similar to chemical and environmental behaviors of 137Cs. The environmental soils in high mountain areas near nuclear power plant were collected, and an Ammonium Molybdophosphate (AMP) precipitation method, which showed high selectivity toward Cs+ ions, was applied to chemically extract and concentrate Caesium radioisotopes. Radioactivity was estimated by a gamma-ray spectrometry. In gamma energy spectrum, with an increasing of 40K radioactivity, it increased the MDA of 134Cs and 137Cs. Therefore, if the natural radionuclides were removed from the soil samples, the MDA of Caesium may be reduced, and the contents of 137Cs of in the environmental soils can effectively be estimated. In the standard soil sample of Korea Institute of Nuclear Safety, radioactivity of 40K was removed more than 84% on average, and the MDA of 134Cs was reduced 2 times. The content of 137Cs was recovered over 84%. On the other hand, in environmental soils, AMP precipitation method showed removal ratio of 40K up to 180 times, which reduced the MDA about 5 times smaller than those of Direct method. 137Cs recovery ratio showed from 54.54% to 70.06%. When considering the MDA and recovery ratio, AMP precipitation method is effective for detection of Caesium radioisotopes in low concentration.