• Title/Summary/Keyword: 감마선 분광법

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The Defect Characterization of $Gd_2O_2S$: Tb Crystals by Positron Annihilation Spectroscopy (양전자 소멸 분광법을 이용한 $Gd_2O_2S$ : Tb 결함 특성)

  • 이종용;김창규
    • Journal of the Korean Vacuum Society
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    • v.13 no.2
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    • pp.92-98
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    • 2004
  • DBPAS has been used to characterize atomic size defect structures in materials. In this investigation the numerical analysis of the Doppler spectra was employed to the determination of the shape parameter, S, defined as the ratio between the amount of counts in a central portion of the spectrum and the total counts of whole spectrum. As the samples were exposed by X-ray increasing the exposed doses from 3, 6, and 9 Gy with 6 MV and 15 MV, respectively and also irradiated by X-ray as the medical applications used for in 0, 2, 4 and 6 years. The S-parameter values were increased as increasing the exposed time and the energies, that indicated the defects generate more. The S-parameters of the samples with medical treatment is varied from 0.4932 to 0.4956.

A Study on the Natural Uranium Contamination Measuring Technology (천연우라늄 오염에 관한 방사선/능 측정기술 연구)

  • 정운수;홍상범;서범경;박진호;조용우;조성원;이정민
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2004.06a
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    • pp.407-417
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    • 2004
  • This study is to verify radiation detection method by using $\alpha$-spectroscopy and ${\gamma}$-spectroscopy for concretes and components which will be generated during the decommissioning of the uranium conversion plant. Components and inside walls of the building were contaminated with natural uranium materials. Some parts of the stainless steel pipes and concretes of the walls were sampled and analyzed their alpha and gamma activities respectively. Alpha and gamma activities are well matched each other in the range of high activity region to 0.01 Bq/g and gamma activities are over estimated comparing alpha activities corresponded in below 0.005 Bq/g region for the natural uranium of AUC sample. The $^{238}U$ originated from natural products of conversion process could be distinguished by measuring $^{214}Pb$ or $^{214}Bi$ and $^{234}Th$ or $^{234m}Pa$. Uranium contaminations mainly are in the wall surface of the plant. Decontamination process of generating wastes which can be reached tp background level gamma activities measured by gamma spectroscopy can also be used to conservative assessment data.

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Analysis of Proton Nuclear Reaction-Generated Nuclides for Different Proton Energy (양성자 에너지 변화에 따른 핵반응 생성핵종 분석)

  • Lee, Samyol
    • Journal of the Korean Society of Radiology
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    • v.13 no.5
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    • pp.819-824
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    • 2019
  • In this study, we proposed a method for identifying isotopes generated from high-energy proton $^{nat}Pb$(p,xn) nuclear reactions through the difference of gamma rays generated through nuclear reactions using different proton energies. The experiment was performed by using a high energy proton generated from a 100 MeV proton linear accelerator of the Korea Atomic Energy Research Institute. Gamma rays generated by various nuclides generated through proton nuclear reactions were measured using a gamma-ray spectroscopy system composed of HPGe detectors. Gamma-ray standard sources were used for accurate energy calibration and efficiency measurements of HPGe gamma-ray detectors. For the proposed method, 100 and 60 MeV proton energy beams were used for the same natural lead samples. This method was found to be very effective in identifying nuclides produced by comparing gamma rays generated from the same sample with each other. The results of this study are expected to be very effective in obtaining other proton nuclear reaction results in the future.

Background Reduction for the ${\gamma}$-Ray Spectrometry of Environmental Radioactivity (환경방사능의 감마선 분광분석을 위한 백그라운드 소멸)

  • Seo, Bum Kyoung;Lee, Kil Yong;Yoon, Yoon Yeol;Lee, Dae Won
    • Analytical Science and Technology
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    • v.14 no.3
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    • pp.212-220
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    • 2001
  • This study was performed to establish the analytical method of radium and radon in various environmental samples with the ${\gamma}$-ray spectrometry. The major problem in the measurements of low level ${\gamma}$-ray, such as environmental radioactivity, is the fluctuation of ${\gamma}$-ray background spectrum. To overcome this problem, a nitrogen gas was filled up in the detector chamber to reduce the background counts due to airborne radioactivities, i.e., $^{214}Pb$ and $^{214}Bi$, the daughters of $^{222}Rn$ in air. When nitrogen gas flowed around the detector, peak counts of ${\gamma}$-rays from the daughters of $^{222}Rn$ decreased about 80% below 1 MeV and about 20~50% above 1 MeV. The use of nitrogen purging results in approximately tenfold increment of sensitivity.

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A New Aluminium Container for $\gamma$-Ray Spectrometry Analysis of Radium and Radon (라듐 및 라돈의 감마선 분광 분석을 위한 알루미늄 용기의 제작 및 특성 조사)

  • Lee, Kil Yong;Yoon, Yoon Yeol;Seo, Bum Kyoung
    • Analytical Science and Technology
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    • v.13 no.6
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    • pp.743-750
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    • 2000
  • For the ${\gamma}$-ray spectrometry analysis of radium and radon in environmental samples, plastic Marinelli beakers have been usually used. But, there are two problems; one is the increment of background by adsorption of airborne radon daughters on the plastic beaker, and other is the incompleteness of radioactive equilibrium by the loss of gaseous radon produced during the radioactive equilibrium process. In order to solve these problems, we made aluminium counting container, and investigated its characteristics. We investigated radioactive equilibrium process using the aluminium container. We found that both solid and liquid samples reached at radioactive equilibrium state in the aluminium container without loss of gaseous radon. By the use of the aluminium container, we established radon and radium analysis method of solid and liquid samples using gamma-ray spectrometry.

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Simultaneous Determination of Mercury, Bromine, Arsenic and Cadmium in Biological Materials by Neutron Activation Analysis

  • Lee, Chul;Kim, Nak-Bae;Park, Euy-Byung
    • Nuclear Engineering and Technology
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    • v.5 no.4
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    • pp.279-285
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    • 1973
  • A method for the simultaneous determination of mercury, bromine, arsenic and cadmium in biological samples is described. Following neutron activation and a simple distillation of volatile compounds, mercury and bromine were determined by gamma-ray spectrometry. Arsenic and cadmium were further separated by cation exchange separation and determined similarly. Determination limits for mercury, bromine, arsenic and cadmium were 0.001$\mu\textrm{g}$, 0.003$\mu\textrm{g}$, 0.001$\mu\textrm{g}$ and 0.02$\mu\textrm{g}$, respectively. The method has been applied to the determination of mercury, bromine, arsenic and cadmium in rice and fish samples. Analysis of a standard kale powder yielded the values of 0.046$\mu\textrm{g}$/g for mercury, 24.5$\mu\textrm{g}$/g for bromine 0.17 $\mu\textrm{g}$/g for arsenic and 0.50$\mu\textrm{g}$/g for cadmium.

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Analysis of 226Ra in the Groundwater Using the Gamma-ray Spectroscopy (감마선 분광법을 이용한 지하수 중의 226Ra 분석)

  • Seo, Bum-Kyoung;Lee, Kil-Yong;Yoon, Yoon-Yeol;Lee, Kune-Woo
    • Analytical Science and Technology
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    • v.16 no.1
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    • pp.39-47
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    • 2003
  • The measurement of radium ($^{226}Ra$) in the groundwater was established using ${\gamma}$-ray spectroscopy without sample preparation. The background interference by air borne radon daughter nuclides was reduced by $N_2$ gas flow into the counting chamber. Leakage of radon gas produced in the radioactive equilibrium with radium and its daughter nuclides was prevented by use of the air-tighted aluminium container. We investigated the effect of air layer in the counting container. Radioactivity variation due to emanation of radon into the air layer was within the counting error range 5%. When the nitrogen gas was flowed around the detector, peak counts of ${\gamma}$-rays from the daughters of airborne radon was decreased and detection limit was decreased to 0.02 Bq/L. The detection limit of detector was lower than 0.74 Bq/L, the $^{226}Ra$ Maximum Contaminant Level (MCL) in the groundwater proposed by US Environmental Protection Agency (EPA). It was confirmed that $^{226}Ra$ radioactivity in the groundwater could be determined by the ${\gamma}$-ray spectroscopy.

동시계수 양전자 소멸 측정을 이용한 Cz-Si 구조 특성

  • Lee, Seung-Jae;Lee, Gwon-Hui;Lee, Jong-Yong
    • Proceedings of the Korean Vacuum Society Conference
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    • 2011.08a
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    • pp.287-287
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    • 2011
  • 동시 계수 도플러 넓어짐 양전자 소멸 분광법으로 n, p형 Cz-Si의 시료에 양성자를 0, 4 MeV 에너지와 조사량의 변화에 의한 결함을 측정하였으며, 고체 구조 특성에 대하여 조사하였다. 양전자와 전자의 쌍소멸로 발생하는 511 keV 감마선 스펙트럼의 수리적 해석 방법인 S-변수와 W-변수를 사용하여, 구조 변화를 측정하였다. 양성자 조사에너지의 세기에 따라 결함이 증가하였으며, 양성자의 조사량의 변화에 대하여는 큰 변화가 없었다.

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Fabrication and Performance of Microcolumnar CsI:Tl onto Silicon Photomultiplier (실리콘광증배관 기반의 미세기둥 구조 CsI:Tl 제작 및 평가)

  • Park, Chan-Jong;Kim, Ki-Dam;Joo, Koan-Sik
    • Journal of IKEEE
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    • v.20 no.4
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    • pp.337-343
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    • 2016
  • This study conducted the gamma ray spectroscopic analysis of the microcolumnar CsI:Tl deposited onto the SiPMs using thermal evaporation deposition. The SEM measured thickness of microcolumnar CsI:Tl and of its individual columns. From the SEM observation, the measured thickness of CsI:Tl were $450{\mu}m$ and $600{\mu}m$. The gamma ray spectroscopic properties of microcolumnar CsI:Tl, $450{\mu}m$ and $600{\mu}m$ thick deposited onto the SiPMs were analyzed using standard gamma ray sources $^{133}Ba$ and $^{137}Cs$. The spectroscopic analysis of microcolumnar CsI:Tl deposited onto the SiPMs included the measurements of response linearity over the $^{137}Cs$ gamma ray intensity; and gamma ray energy spectrum. Furthermore from the gamma ray spectrum measurement of $^{133}Ba$ and $^{137}Cs$, $450{\mu}m$ thick CsI:Tl showed good efficiency when measured with $^{133}Ba$ and $600{\mu}m$ thick CsI:Tl was highly efficient when measured with $^{137}Cs$.