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Dyeing Properties of Morus alba L. Fruit Powder on the Silk Fabric (오디 분말을 이용한 견직물의 염색성)

  • Bai, Sang-Kyoung
    • Fashion & Textile Research Journal
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    • v.10 no.5
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    • pp.779-783
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    • 2008
  • The main colorant of Morus alba L. fruit is anthocyanin which is a kind of flavonoid group. In this article, the dyeing properties of colorant extracted from Morus alba L. fruit were investigated on some silk fabrics. The results were as follows: The maximum absorbance of Morus alba L. fruit showed at 284 nm, and 516 nm by UV-VIS spectrophotometer. The dye adsorption increased according as dye concentration. The optimal dyeing temperature was $60^{\circ}C$ and the dye equilibrium was reached 40 minutes after dyeing. The highest K/S value of the colorant obtained at bath ratio 40:1. The effect of pH of dye solution showed higher K/S value at acidic than alkaline condition. Almost Mordants except pre-Fe and Sn did not significantly increased dye adsorption. The pre mordanted silk fabrics showed RP, P, and post mordanted ones showed PB, GY. The color fastnesses to light, washing, and perspiration were modified at pre-Sn mordanted samples.

Characteristics of the Water Soluble Browning Reaction of Korean Red Ginseng as Affected by Heating Treatment (열처리에 따른 고려홍삼의 수용성 갈변물질의 특성)

  • 이종원;이성계
    • Journal of Ginseng Research
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    • v.22 no.3
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    • pp.193-199
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    • 1998
  • The purpose of this study was to Investigate characteristics of the water soluble browning reaction products (WS-BRPs) from Korean red ginseng by heat treatment. Absorbance of WS- BRPs was increased with increases of heating temperature and time, but pH value were decreased In Muter color value L and b value were decreased, while a value was increased. and absorbance at 280 nm in spectrum of the WS-BRPs was increased according to the increase of heating temperature. When the WS-BRPs were applied on Bio-Gel P-30 column after heating and pH treatment, two majors browning products increased according to the progress on time. And pH 3.0 increased in quantity of high molecular fractions and pH 8.0 increased in quantity of low molecular fractions.

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A Study on Suggestion of Insulating Oil Ageing Degree in Pole-Transformer by Absorbance (흡광도법에 의한 주상변압기 절연유의 열화판정기준 설정에 관한 연구)

  • Lee, Dong-Zoon;Jung, Jong-Uk;Kim, Kyung-Hwa;Kwak, Hee-Ro;Yun, Yong-Ja
    • Proceedings of the KIEE Conference
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    • 1996.07c
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    • pp.1851-1853
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    • 1996
  • In this paper the criteria for insulating oil condition of pole transformer were suggested by applying the UV-Visible spectrophotometric method. Ageing of insulating oil caused the change in absorbances of oil os well os the deterioration of electrical properties of oil. By comparing the electrical properties such as $tan{\delta}$ and breakdown voltage with the UV-Visible absorbances of oil, criteria for absorbance values determining oil condition were established. This UV-Visible spectrophotometric method might be applied in ageing analysis of oil and be expected to replace the current method.

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Deposition condition and Confirmation of Organic Charge Transfer complex Langmuir-Blodgett Film (유기전하 이동착물 Langmuir-Blodgett막의 누적조건 및 누적확인에 관한 연구)

  • Jeong, Soon-Wook
    • Journal of the Korean Applied Science and Technology
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    • v.14 no.1
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    • pp.89-93
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    • 1997
  • In this research, ultra-thin films of organic charge transfer complex were deposited on to ordinary microscope slide-glass subtrates with a Langmuir-Blodgett technique. ${\pi}$-A isotherm characteristics of these complex were studied in order to find optimum conditions of deposition by varying temperature of subphase, compression speed, and spreading amount. Transfer ratio of these films were studied during the process of deposition. The UV-visible absorbance spectra of LB films were measured to find state of deposition by varing layer number. The observed optimum conditions of surface, pressure, spreading amount, and dipping speed for depositing LB films(Y-type) were 38m/Nm, $150{\mu}l$ and 5mm/min, respectively. Since the tansfer ratio is close to 100%, the monolayer on the subphase seems to be well transferred to the solid substrate. The thickness of the film was well-controlled as the UV-vis absorbance of films were changed linear according to the number of layers.

A Study of the Developement of Washable Panties for Elderly Women of Incontinence Urine (노인여성을 위한 요실금 팬티 개발에 관한 연구)

  • 조진숙;최진희;허은영
    • Journal of the Korean Society of Clothing and Textiles
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    • v.25 no.5
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    • pp.856-867
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    • 2001
  • The purpose of this study was to develop washable panties for elderly women of incontinence urine. We carried out a questionnaire survey in order to find out what are the inconvenience of incontinence. Also we analyse the properties of incontinence panties available in silver market. Then we did wearing test of the existing continence panties to 40 subjects. Having done the wearing test, it was clear that the composit and the size of the absorbing layers must be crucial points of the development of the prototype panty. The prototype was designed to improve absorbing speed as well as capability without sacrificing of wearing comfort. The developed prototype panty went through wearing test and property tests to assure the design. The results are as follows:- 1. Absorbing capability as a whole, quick absorbance at the moment of passing of urine, the touch of the cover layer after quick absorbance and deodorant property were improved than existing incontinence panties. 2. The size and the dimensions of each part, specially absorbing layers at the crotch area, were remarkably improved.

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Dyeing of Cotton fabrics by Glycyrrhizae Radix Extract (감초추출물에 의한 면직물의 염색)

  • Lee, Young-Sook;Jang, Jeong-Dae
    • Textile Coloration and Finishing
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    • v.22 no.1
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    • pp.21-27
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    • 2010
  • The purpose of this research was to investigate the color characteristic and the dyeing properties of Glycyrrhizae Radix extract on cotton fabrics. The highest absorbance of Glycyrrhizae Radix extract was obtained in 75 v/v% of ethyl alcohol in water. Pre-mordanted cotton fabrics dyed at $30^{\circ}C$ and pH 3 for 80 minutes showed the highest K/S value. According to the dyeing conditions, the colors of the fabrics varied from yellow(Y) and yellowish red(YR) to greenish yellow(GY). The color fastness of the fabrics in dry-cleaning and water was 4~5 rating. The deodorization capacity and UV-cut effect of the dyed fabrics were higher than those of undyed ones.

A Study on Spectrophotometric Determination of Oleic Acid by Basic Dye Methylen Bblue (염기성색소(鹽基性色素) Methylen Blue에 의(依)한 Oleic Acid의 흡광광도정량(吸光光度定量))

  • Lee, Sook-Yun
    • Journal of Pharmaceutical Investigation
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    • v.4 no.1_2
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    • pp.46-54
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    • 1974
  • A new spectrophotemetric method was estalished for the determination of oleic acid. This method is based on the 1,2-dichloroe-thane extraction of the ion-pair formed between methylene blue and oleic acid. But the absorbance of an ion-pair in the 1,2-dichloroe-thane layer was variable with the temperature, the ion-pair was extracted back into a diluted hydrochloric acid solution. The maximum absorbance of the acid extract observed at $660m{\mu}$ and a lineal relationship was observed from the initial amount over the range of $50-800{\gamma}/ml$ of oleic acid in the aqueous phase. The composition ratio of the ion-pair formed between methylene blue and oleic acid was determined to be 2 : 1 by both the mole ratio and continuous variation methods.

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Studies on the Natural Dyes(12) -Dyeing Properties of Amur Cork Tree Colors for Silk- (천연염료에 관한 연구(12) -황벽 색소의 견섬유에 대한 염색성-)

  • 조경래;강미정
    • Textile Coloration and Finishing
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    • v.12 no.4
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    • pp.239-247
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    • 2000
  • The coloring matter was extracted from the heartwood of Amur cork tree by distilled water. Change of UV-Visible spectra of coloring matter solution by extraction condition and stability for irradiation were determined, and the effect of repeated dyeing with condition of dyebath and mordanting method on shade depth and lightfastness were also investigated. The results are as follows : 1) Absorbance of Amur cork tree extract increased with the lapse of extraction time. λmax of color solution extracted from Amur cork tree was found at 420, 333, and 262nm. 2) Absorbance of Amur cork tree extract decreased remarkably after 2hr irradiation. 3) The K/S of silk fabrics increased with the increase of dyeing temperature, time, amounts of Amur cork tree for extraction, and pH of color solution. 4) K/S of silk fabrics dyed by repeated dyeing method was affected by pH and concentration of color solution. 5) Lightfastness of silk twice dyed with Amur cork tree extract after pre-mordanted by 8%(o.w.f) chromium acetate was moderately improved.

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Nondestructive Measurement of Sugar.Acid Contents in Fruits Using Spectral Reflectance (분광 반사 특성을 이용한 주요 과실의 비파괴 당.산도 측정)

  • 노상하;김우기;이종환
    • Journal of Biosystems Engineering
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    • v.22 no.2
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    • pp.247-255
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    • 1997
  • This study was conducted to develop regression models predicting sugar and acid contents in intact fruits nondestructively by using the second derivative of absorbance spectrum measured with a spectrophotometer wavelength range of 400nm to 2, 400nm. The correlation analysis was made in wavelength range of 600nm to 1, 100nm and 600nm to 2, 400nm respectively, in order to examine the feasibility of using a real time spectrophotometer, which covers the former range, in predicting sugar and acid contents. The second derivative data of the spectrum were obtained by varying smoothing size and derivative size of the original absorbance spectrum. SAS statistical package program was used for the regression analysis. The sugar contents of Fuji apple, Shingo pear md Yumyung peach could be predicted with SEPs of 0.40, 1.17 and 0.77 respectively, in the spectrum range of 600 to 1, 100nm. The highest correlation coefficient of the titratible acidity of apple was -0.45 at 2, 346nm and regression models indicated determination coefficient less than 0.47.

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Physicochemical Study on the Synthesis of Progesterone Immunogen (프로제스테론의 면역원 합성에 관한 물리화학적 연구)

  • Park, Jun-hong;Kwun, Jong-kuk
    • Korean Journal of Veterinary Research
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    • v.26 no.2
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    • pp.225-228
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    • 1986
  • Progesterone immunogen has been synthesized and its melting point, Rf-value, UV and IR spectrum have been measured to develope the essential step in antisera production against low molecular weight substance. Mixed anhydride reaction was used to conjugate $11{\alpha}$-hydroxy-progesterone with succinic anhydride. Melting point of one intermediate compound was $156^{\circ}C$, and Rf-value was 0.41 in benzene : acetone : methanol (5 : 5 : 2). Maximum absorbance was measured at 242nm and ${\varepsilon}$ was $1.641{\times}10^4cm^2/mole$. Loss of hydroxy group was observed at 3450nm, and carbonyl group was appeared at 1160nm, 1250nm and 2960nm. These results indicated that the intermediate compound was progesterone hemisuccinate. Maximum absorbance of progesterone bovine-serum albumin(BSA) conjugate was observed at 250nm. Molar ratio of progesterone to BSA was average 15.4 on UV spectrum.

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