• 제목/요약/키워드: $SiO_2$ coating

검색결과 647건 처리시간 0.026초

Metal-Organic Decomposition법에 의한 강유전성 $YMnO_3$ 박막의 제조 및 특성 (Preparation of Ferroelectric $YMnO_3$ Thin Films by Metal-Organic Decomposition Process and their Characterization)

  • 김제헌;강승구;김응수;김유택;심광보
    • 한국세라믹학회지
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    • 제37권7호
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    • pp.665-672
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    • 2000
  • The ferroelectric YMnO3 thin films were prepared by MOD(metal-organic decomposition) method with Y- and Mn-acetylacetonate as starting materials. Thin films were grown on various substrates by spin-coating technique. The crystalline phases of the thin films were identified by X-ray diffractometer as a function of heat-treatment temperature, pH of coating solution and substrate. In addition, the effect of Mn/Y molar ratio(0.8~1.2) on the formation of hexagonal-YMnO3 phase was investigated. In forming highly c-axisoriented hexagonal-YMnO3 single phase, the Pt coated Si substrate was more effective than the bare Si substrate, and the optimum heat-treatment condition was at 82$0^{\circ}C$ for 30 min. Higher Mn/Y molar ratio within 0.8~1.2 and pH of YMnO3 precursor solution within 0.5~2.5 favored formation of ferroelectric hexagonal phase rather than orthorhombic phase. Leakage current density of the hexagonal-YMnO3 thin film formed on Pt(111)/TiO2/SiO2/Si substrate was low enough as 0.4~4.0$\times$10-8(A/$\textrm{cm}^2$) at 5 V and its remanent polarization(Pr), calculated from the P-E hysteresis loop, was 3 nC/$\textrm{cm}^2$.

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무전해 니켈도금과 무전해복합도금(Ni-P-X, X: SiC, $Al_2$O$_3$, Diamond)의 내마모성 비교 (The Wear Resistance of Electroless Nickel and Electroless Composite(Ni-P-X, X: SiC, $Al_2$O$_3$, Diamond) Coating Layers)

  • 김만;장도연;정용수;노병호;이규환
    • 한국표면공학회지
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    • 제27권4호
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    • pp.193-206
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    • 1994
  • A wear behavior of electroless (Ni-P-X, X: SiC, $Al_2O_3$, Diamond) composite coating layers, formed under various conditions on commerical grade low carbon steel, has been investigated using Taber abrasion tester and scanning electron microscope. Several factors, which are type of particles, co-deposited content, particle size, distribution of particles and heat-treatment, influenced the wear resistance. The wear resistance of the composited coating layers after heat-treatment at $400^{\circ}C$ for 1 hr was increased 70 times with diamond, 15 times with SiC and 8 times with $Al_2O_3$, compared with the electroless nickel plating layer without heat-treatment.

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다층 박막을 이용한 패럴 단면의 무반사 코팅 설계 및 특성 (Design and Characteristics of Anti-reflection Coating using Multi-layer Thin Film on the Ferrule Facet)

  • 기현철;양명학;김선훈;김태언;김회종;구할본
    • 한국전기전자재료학회논문지
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    • 제20권11호
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    • pp.991-994
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    • 2007
  • In this paper, we have designed the anti-reflection(AR) coating for $1400{\sim}1600$ nm wavelength range on the ferrule facet of optical connector. The low-temperature ion-assisted deposition was applied to AR coating on the ferrule facet in order to avoid damage of optical connector. We have measured the refractive index of coating film($Ta_2O_5\;and\;SiO_2$) using the ellipsometer and optimized the film thickness using the SEM and thickness measurement equipment. UV-VIS-NIR spectrophotometer is used to measure transmissivity of the AR coated ferrule facet. The refractive index of $Ta_2O_5\;and\;SiO_2$ is $2.123{\sim}2.125$ and $1.44{\sim}1.442$, respectively, for $1400{\sim}1600$ nm wavelength range. The transmissivity of the AR coated ferule facet is more than 99.8 % for $1425{\sim}1575$ nm wavelength range and more than 99.5 % for $1400{\sim}1600$ nm wavelength range. The return loss of the AR coated ferrule facet is 30.1 dB.

졸-겔법에 의한 $SrTiO_3:Pr^{3+}$ 형광체의 $SiO_2$$Al_2O_3$ 코팅에 따른 발광특성 (Luminescent Properties of $SrTiO_3:Pr^{3+}$ Phosphor Coated with $SiO_2$ and $Al_2O_3$ by Sol-Gel Method)

  • 이동규;임문혁;이진화;김태영
    • 한국응용과학기술학회지
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    • 제23권3호
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    • pp.243-251
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    • 2006
  • Field emission display(FED) is actively investigated in view of the development of full color flat-panel display, which can replace some cathode-ray tube(CRT). Thus, the development of new phosphors appropriate for FED is urgently needed and has been actively investigated. In this work, $SrTiO_3:Pr^{3+}$ phosphor was prepared by sol-gel method and the coating was applied by sol-gel method combined with sonication on these phosphor's surface into diluted precursor solution. It was found that very fine particles of coating material were formed on phosphor's surface. The luminescent intensity of $SrTiO_3:Pr^{3+}$ phosphor coated with $SiO_2$ and $Al_2O_3$ was considerably increased without any noticeable change in color chromaticity. The optimum concentration of coating material was found to be 1wt% and the optimum pH value of the solution was 10.

실리카 코팅된 TiO2-천연 제올라이트 복합입자 제조와 특성평가 (Surface Coating of SiO2 on TiO2-natural Zeolite Composite Particles and Its Characterization)

  • 임형미;정지숙;이동진;이승호
    • 한국재료학회지
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    • 제16권11호
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    • pp.692-697
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    • 2006
  • Deodorization of natural zeolites have been improved not only for polar but also for non-polar pollutants by sucessive ion exchanges of H and Ag ions starting from Korean natural zeolite with high adsorption capacity. The modified zeolites with $TiO_2$ coating on the surface revealed high deodorization and photocatalytic decomposition effects. Further modification was made with $10{\sim}20nm$ silica nano particles coating on the surface, the resulting composite particles of $SiO_2/TiO_2/modified$ natural zeolite revealed not only comparable deodorization but also better durability and resisatnce to color change compared to the $TiO_2$/modified natural zeolite without much compensation of photocatalytic decomposition effect, when the composite particles were exposed to the polypropylene non-woven fiber coated with organic binder. It is expected for the composite particle prepared here to be used as indoor building materials for indoor air quality control.

LiFePO4/C의 carbon coating 방법 및 다공성 구조 형성에 의한 전기화학적 특성 개선 (Improvement of Electrochemical Performance of LiFePO4 by Carbon Coating and Morphology Control into Porous Structure)

  • 공기천;주재백
    • 전기화학회지
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    • 제17권4호
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    • pp.229-236
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    • 2014
  • 본 연구에서는 리튬이온 이차전지 양극 활물질로 사용되는 $LiFePO_4$ 활물질을 이용하여 전지를 제조한 후 그 특성들을 평가하였다. 공침법을 이용하여 $FePO_4$ 전구체를 합성한 후 생성된 전구체에 리튬을 합성시키며, 열처리를 통하여 활물질을 생성시킨다. 열처리 온도에 의한 결과 중 $750^{\circ}C$에서의 결과가 가장 우수함을 확인하였으며 전도성을 확보하기 위하여 카본을 코팅하는 방법을 물리적 코팅 방식과 화학적 코팅방법으로 나누어 실험하였으며 물리적 카본 코팅의 결과 6wt%를 코팅했을 때 125 mAh/g의 용량을 보였으며 화학적 코팅에서는 코팅하지 않은 기본 활물질 보다 약 40%의 성능향상을 보여 130~140 mAh/g 대의 활물질 용량을 보였다. 다공성 구조체를 형성하기 위하여 nanocomposite을 투입한 실험에서는 $Al_2O_3$를 첨가한 활물질이 porous 형태의 구조체를 형성하고 $SiO_2$을 첨가한 활물질 보다 132 mAh/g의 용량으로 우수함을 알 수 있었다.

솔젤법에 의한 다이옵사이드 생체 세라믹의 표면코팅 및 지르코니아 기판의 생체활성 증진 (Bioactivity enhancement of zirconia substrate by surface coating of diopside bioceramics using sol-gel method)

  • 박현정;이종국
    • 한국결정성장학회지
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    • 제32권5호
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    • pp.183-190
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    • 2022
  • 다이옵사이드(CaMgSi2O6)는 생체활성이 높을 뿐만 아니라 우수한 기계적 성질도 보유한 물질로 알려져 있다. 본 연구에서는 지르코니아 세라믹스의 생체활성을 향상시키기 위하여 지르코니아 기판 표면에 다이옵사이드를 솔젤법으로 코팅하고 in vitro 시험을 통해 지르코니아 기판의 생체활성 증진을 고찰하였다. 코팅용 다이옵사이드 솔은 Ca(NO3)2·H2O, MgCl2·H2O 및 Si(OC2H5)4를 각각의 몰비로 에탄올에 용해한 후 가수분해시켜 제조하였다. 다이옵사이드 코팅에 의한 생체활성 증진을 고찰하기 위하여 SBF 용액 내에서 in vitro 시험을 진행하였는데, 침적초기에는 주로 코팅층 다이옵사이드 입자들의 표면용해가 관찰되었고, 새로운 하이드록시아파타이트 입자의 석출은 14일 침적시편에서 주로 관찰되었다. In vitro 시험 시 SBF(Simulated Body Fluid) 용액에 대한 다이옵사이드 코팅층의 용해와 기판 표면에 석출되는 하이드록시아파타이트 층의 양과 형태는 코팅횟수와 코팅층 두께에 의존하였다.