• Title/Summary/Keyword: $In_2Se_3$상

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Quantification of seleno proteins in Korean blood serum using solid phase extraction and affinity chromatography-inductively coupled plasma/mass spectrometry (고체상 추출과 친화 크로마토 그라피-유도결합 플라즈마 질량분석법을 이용한 한국인 혈청에서의 셀레노 단백질 정량)

  • Ahn, Ji-Yun;Kwon, Hyo-Sik;Pak, Yong-Nam
    • Analytical Science and Technology
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    • v.27 no.2
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    • pp.92-99
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    • 2014
  • Interferences were removed using anion exchange solid phase extraction (AE SPE) in quantification of selenoproteins in Korean human blood serum with affinity high performance liquid chromatography (AF HPLC)-inductively coupled plasma/mass spectrometry (ICP/MS). The average selenium level obtained for healthy Koreans was $94.3{\pm}2.3ngg^{-1}$ using isotope dilution method. AE SPE was coupled to AF column to separate 3 selenoproteins, glutathione peroxidase GPx, selenoprotein SelP, and selenoalbumin SeAlb. Post column isotope dilution was employed to quantify the proteins. The certified reference material of human blood serum BCR-637 was analyzed to give total selenoprotein concentration of $85.4{\pm}3.4ngg^{-1}$, which agreed well with the reference value of $81{\pm}7ngg^{-1}$. The pooled concentration of GPx, SelP, and SeAlb from healthy Koreans (n=20) was $12.1{\pm}1.4ngg^{-1}$, $57.2{\pm}2.0ngg^{-1}$, and $20.0{\pm}1.9ngg^{-1}$, respectively. The sum of selenoproteins is $89.3ngg^{-1}$, which is about the same as the total selenium concentration of $94.3ngg^{-1}$. The fact suggests that selenium in blood serum is mostly consisted of selenoproteins. After the removal of interference, GPx showed a significant decrease (more than 50%) from $25.0ngg^{-1}$ to $12.1ngg^{-1}$. It was identified that the interference in blood serum was mostly from GPx and the use of AE SPE was proven to be efficient in eliminating Cl and Br that cause interference to GPx.

Effects of In concentration and substrate temperature on properties of ZIO films deposited by RF magnetron sputtering (RF 스퍼터링법에 의해 증착한 ZIO 박막의 물성에 미치는 In 함량과 기판온도의 영향)

  • Park, Se-Hun;Park, Ji-Bong;Song, Pung-Geun
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2009.05a
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    • pp.135-135
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    • 2009
  • ZIO 박막은 RF 마그네트론법으로 다양한 $In_{2}O_{3}$ 함량을 소결체 ZIO 타겟을 사용하여 유리 기판위에 증착되었다. $In_{2}O_{3}$ 9.54 wt%를 함유한 ZIO 타겟을 이용하여 PT에서 증착한 박막이 가장 낮은 비저항 $9.13{\times}10^{-4}{\Omega}cm$를 나타내었다. 전기적 특성을 향상시키기 위하여 기판온도를 상승하였으나 오히려 전기적 특성이 저하되는 결과를 나타났다. 게다가 기계적 특성 역시 기판온도 상승에 따라 저하되었다. 한편 XRD 측정을 통하여 기판온도 200과 $300^{\circ}C$에서 ZnO (002) 면과 $In_{2}O_{3}$ (400) 면이 동시에 관찰되었다. 그러므로 전기적, 기계적 특성의 저하는 상분리, 결정립크기의 감소와 같은 결정성 저하에 기인한다고 생각된다.

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Determination of Protein Amino Acids as the N-TFA N-Butyl Esters by Gas Liquid Chromatography (Gas Liquid Chromatography에 의한 단백질 아미노산의 분석)

  • Woo, Kang-Lyung
    • Korean Journal of Food Science and Technology
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    • v.22 no.1
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    • pp.88-93
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    • 1990
  • For effective separation of the N-TFA n-butyl ester amino acids on the stainless steel column by GLC, dual column of the mixed stationary phases, 3.36% OV-17+3.0% SE-30(column 1) and 1% NPGS +0.5% OV-17+0.5% SE-30(column 2) on chromosorb W HP 100-120 mesh, were used. On the column 1. the nineteen amino acids except histidine were obtained. However, alanine and valine peaks were not separated by this column. On the column 2, the sixteen amino acid peaks showed good separation, but tryptophan. arginine, histidine, and tyrosine peaks were not obtained. Calibration graphs for all amino acids obtained by the plotting the ratios of their peaks hights to that of internal standard versus the micro mole of the amino acids in the range $1.25{\times}10^{-3}{\mu}mol-1.0{\times}10^{-2}{\mu}mole$ showed linearity and passed through the origin.

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Occurence of Bakanae Disease (Gibberella fujikuroi) Growth Characteristics of Rice by Different Disinfection Methods (소독 방법에 따른 벼 키다리병 발생 및 생육 특성)

  • Kim, Se-Jong;Won, Jong-Gun;Ahn, Duok-Jong;Park, So-Deuk;Choi, Chung-Don
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.53 no.4
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    • pp.417-420
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    • 2008
  • This study was carried out to compare the growth and yield characteristics between bakanae diseases (Gibberella fujikuroi) infected and uninfected rice plants with different disinfection mothods. The infected rice seeds, harvested previous year, were disinfected either with prochloraz for 48 hours at $33^{\circ}C$ in germinator or 24 hours at room temperature and not disinfected. In the methods of disinfection, it is more effective in disinfected by prochloraz for 48 hours at $33^{\circ}C$ using germinator near to 0% of infection rate, followed by conventional method as 5.0% and 76% in not disinfected rice seeds. In the rice yield components among the disinfection methods, panicles were increased about 11% in the disinfected seeds using germinator for 48 hours compared to conventional method. Ripening grain rate also increased at the disinfected using germinator as $80.3{\sim}80.3%$, improved more than $4.9{\sim}5.9%$ compared to the conventional disinfection. From these results, the rice yield was $512{\sim}517\;kg/1,000\;m^2$ at the disinfected using germinator which increased more than $6{\sim}7%$ compared to the conventional disinfection.

A Study on Tensile Restraint Crack Critical Stress Characteristcs of Gravity-Wet-Type Underwater Welded Joints (중력식 습식 수중용접부의 인강구속균열 임계응력 특성에 관한 연구)

  • O, Se-Gyu;Gang, Mun-Ho;Han, Sang-Deok
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.23 no.2
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    • pp.61-65
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    • 1987
  • In this study, the characteristics of TRC (tensile restraint crack) critical stress in the gravity type underwater wet welding process and in the in-air welding have been investigated for Y, y and 45$^{\circ}$r grooves using the KR Grade A-3 steel plates and the E4303 covered electrodes. The following results were obtained: (1) In the TRC tests, the initial critical stress of Y groove is higher than those of the 45$^{\circ}$r single bebel grooves in both in-air and underwater weldings, and the cold fracture sensitivity is higher in the underwater welding than in the in-air welding. (2) The hardness of underwater weld metal is the highest in heat affected zone is about Hk 365 in the in-air weld but Hk 670 in the underwater weld which is higher for cooling speed is more rapid, resulting in the lower critical stress by increase of fracture sensitivity. (3) The diffusible hydrogen quantity for 48 hours is about 18cc/100g-weld-metal in the in-air welding but 48cc/100g-weld-metal in the underwater welding. So that, in the case of underwater welding the diffusible hydrogen penetrates about 3 times more than that in the in-air welding.

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Statistical Study of Failure-Modes around the Pibanryeong Region, Boeun-Gun, Chungbuk (충북 보은군 피반령 부근 절취사면의 파괴양상에 대한 통계학적 연구)

  • Cheong, Sang-Won;Choi, Byoung-Ryol
    • The Journal of Engineering Geology
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    • v.19 no.4
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    • pp.517-528
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    • 2009
  • Statistical analyses of cut-slope stability were performed over approximately 5.7 km section along the National road No. 25, which cross-cuts in NW-SE direction the Cheongwon and Boeun-Gun area, Chungbuk. A measure of slope-stability was established by using direct reinforcement and indirect protection methods in whole section. Orientations(dip/dip direction) of the slopes, foliations(bedding), cleavages and joints were measured in total of 30 slope sites. The results analyzed using stereographic projection indicate that major directions of the slopes come out predominantly in three directions: 1) $58^{\circ}/095^{\circ}$, 2) $60^{\circ}/296^{\circ}$ and 3) $59^{\circ}/212^{\circ}$. In analyses of dip direction and frequency of cut-slopes established by reinforcement and protection methods, slopes with dip direction of $80-120^{\circ}$ and $280-320^{\circ}$ mostly occur. However, slopes with dip direction of $0-80^{\circ}$(N and NW) and $120-160^{\circ}$(SE) are not distributed in the study area. Failure aspects were analyzed for three major directions of the slopes, respectively. The results of failure aspects analyzed indicate that slopes in the study area could generate various failures as the results of intersection and/or intersection combination among joints, foliations(bedding) and cleavages. However, possibility of failure in a slope of major direction No. 3 is statistically very low because of low frequency in total number of slopes with the direction and of formation of small scale-slopes geographically, although the slope might generate all aspects of failure-modes.

3DTV System Adaptive to User's Environment (사용자 환경에 적응적인 3DTV 시스템)

  • Baek, Yun-Ki;Choi, Mi-Nam;Park, Se-Whan;Yoo, Ji-Sang
    • The Journal of Korean Institute of Communications and Information Sciences
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    • v.32 no.10C
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    • pp.982-989
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    • 2007
  • In this paper, we propose a 3DTV system that considers user's view point and display environment. The proposed system consists of 3 parts - multi-view encoder/decoder, face-tracker, and 2D/3D converter. The proposed system try to encode multi-view sequence and decode it in accordance with the user's view point and it also gives a stereopsis to the multi-view image by using of 2D/3D conversion which converts decoded two-dimensional(2D) image to three-dimensional(3D) image. Experimental results shows that we are able to correctly reconstruct a stereoscopic view that is exactly corresponding to user's view point.

Effect of Methionine Levels on Brain Lipid Peroxidation in Ethanol-treated Rats of Selenium Deficiency (메티오닌과 셀렌이 에탄올 중독된 흰쥐의 뇌지질과산화에 미치는 영향)

  • 조수열;이미경;박은미;장주연;김명주
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.26 no.1
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    • pp.109-115
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    • 1997
  • This study was designed to investigate the effects of methionine(Met) on the activities of brain lipid peroxidation related enzymes in ethanol administrated rats of selenium(Se) deficiency. Male Sprague-Dawley rats were fed Se deficiency diets containing one of the three levels of Met (0, 3, 9g/kg diet) and ethanol(2.5g/kg of body weight) was administrated as 25v/v% ethanol treated groups orally. The rats sacrificed after 5 and 10 weeks of feeding periods. Alcohol dehydrogenase activity was increased in ethanol treated groups and was higher Met normal group than Met deficiency and excessive groups at 5 and 10 weeks dieting. Aldehyde dehydrogenase activity was decreased in ethanol treated groups and significantly decreased in Met deficiency group. Monoamine oxidase activity in brain was increased in ethanol treated groups and was predominently increased in Met deficiency groups. Superoxide dismutase and glutathione peroxidase activities were decreased in ethanol treated groups and tended to increase in proportion to level of dietary methionine. Glutathione S-transferase and catalase activities and lipid peroxide content were increased by ethanol administration and were higher Met deficiency group than normal and excessive groups.

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A Technique for Building Occupancy Maps Using Stereo Depth Information and Its Application (스테레오 깊이 정보를 이용한 점유맵 구축 기법과 응용)

  • Kim, Nak-Hyun;Oh, Se-Jun
    • Journal of the Institute of Electronics Engineers of Korea SP
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    • v.45 no.3
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    • pp.1-10
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    • 2008
  • An occupancy map is a representation methodology describing the region occupied by objects in 3D space, which can be utilized for autonomous navigation and object recognition. In this paper, we describe a technique for building an occupancy map using depth data extracted from stereo images. In addition, some techniques are proposed for utilizing the occupancy map for the segmentation of object regions. After the geometric information on the ground plane is extracted from a disparity image, the occupancy map is constructed by projecting each matched point to the ground plane-based 3D space. We explain techniques for extracting moving object regions using the occupancy map and present experimental results using real stereo images.

Behavior of Microdomains in Block Copolymer/Nanoparticle Nanocomposite Thin Films under Electric Field (공중합체/나노입자 복합체 박막 내 미세구조의 전기장 하에서의 거동)

  • Bae, Joonwon
    • Applied Chemistry for Engineering
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    • v.28 no.3
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    • pp.290-293
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    • 2017
  • In this study, the fundamental behavior of microdomains in block copolymer/nanoparticle composite thin films was examined. In this experiment, polystyrene-b-poly(2-vinylpyridine) block copolymer and CdSe nanoparticles having a noncentrosymmetric property were employed. Composite hybrid thin films were produced by a spin coating method, and changes in the internal structure of composite thin films were monitored mainly by transmission electron microscopy. In summary, nanoparticles resided inside the thin film relatively intact, however, the block copolymer microdomains rotated parallel to the electric field direction. This study will be very helpful for future research activities regarding behaviors of heterogeneous composite materials under external fields.