• Title/Summary/Keyword: ${\sigma}$-Phase

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Relationship Between Properties Degradation and Critical Aging Time of Super Austenitic and Duplex Stainless Steels

  • S. H. Choi;Y. R. Yoo;S. Y. Won;G. B. Kim;Y. S. Kim
    • Corrosion Science and Technology
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    • v.22 no.5
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    • pp.330-340
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    • 2023
  • The objective of this study was to analyze effects of aging time on property degradation of super austenitic stainless steel of PRE 52.8 and super duplex stainless steel of PRE 48.7. To analyze corrosion properties based on aging time, a critical pitting temperature test was performed in a solution of 6% FeCl3 + 1% HCl and an anodic polarization test was performed in deaerated 0.5N HCl + 1N NaCl solution at a temperature of 50 ℃. Surface hardness was measured to analyze mechanical properties. It was found that corrosion properties and mechanical properties deteriorated rapidly as aging time increased. Critical pitting temperature had the most effect on critical aging time at which property changes occurred rapidly, followed by pitting potential and hardness. This trend was found to be closely related to the fraction of sigma phase. Rate of sigma phase formation was found to be significantly faster in duplex stainless steel than in austenitic stainless steel.

Stress analysis of the CR lens using the chrome conversion (Chrome 변환을 이용한 CR 렌즈의 미세응력 시각화)

  • Kim, Yong-Geun
    • Journal of Korean Ophthalmic Optics Society
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    • v.10 no.1
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    • pp.9-15
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    • 2005
  • The polariscope to measure the microscopic stress in CR lens consists of light source polarizer, model, polarizer, CCD, computer, chrome conversion orderly and the principal-stressed difference, (${\sigma}_1-{\sigma}_2$) and the fringe order n were measured by analyzing two components of light wave $E_1$ and $E_2$ following each polarizer's steps. The two-dimensional model could be determined from the fact that the optical axes of sample concide with the principal-stress directions. The bi-refringence acted to a light wave and the phase retardation were in proportion to the principal-stressed difference(${\sigma}_1-{\sigma}_2$) and the intensity of final light wave was proportioned to $sin2({\Delta}/2)$ and when ${\Delta}/2=n{\pi}$ (n=0, 1, 2, ${\ldots}$) the extinction occurs. Photoelastic's image by microscopic stress could analyzed using chrome conversion, and the image showed clearly.

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Partial Purification of Factors for Differential Transcription of the rrnD Promoters for Ribosomal RNA Synthesis in Streptomyces coelicolor

  • Hahn, Mi-Young;Roe, Jung-Hye
    • Journal of Microbiology
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    • v.45 no.6
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    • pp.534-540
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    • 2007
  • The Streptomyces coelicolor A3(2) genome contains six operons (rrnA to F) for ribosomal RNA synthesis. Transcription from rrnD occurs from four promoters (p1 to p4). We found that transcripts from the p1 and p3 promoters were most abundant in vivo in the early exponential phase. However, at later phases of exponential and stationary growth, transcripts from the p1 promoter decreased drastically, with the p3 and p4 transcripts constituting the major forms. Partially purified RNA polymerase supported transcription from the p3 and p4 promoters, whereas pure reconstituted RNA polymerase with core enzyme (E) and the major vegetative sigma factor ${\sigma}^{HrdB}$ ($E{\cdot}{\sigma}^{HrdB}$) did not. In order to assess any potential requirement for additional factor(s) that allow transcription from the p3 and p4 promoters, we fractionated a partially purified RNA polymerase preparation by denaturing gel filtration chromatography. We found that transcription from the p3 and p4 promoters required factor(s) of about 30-35 kDa in addition to RNAP holoenzyme ($E{\cdot}{\sigma}^{HrdB}$). Therefore, transcription from the p3 and p4 promoters, which contain a consensus -10 region but no -35 for ${\sigma}^{HrdB}$ recognition, are likely to be regulated by transcription factor(s) that modulate RNA polymerase holoenzyme activity in S. coelicolor.

Effect of Heat Treatment on the Microstructural Evolution of Pt-aluminide Coated Ni-based Superalloy (Pt-Aluminide로 코팅된 초내열합금의 열처리에 따른 미세조직변화)

  • Joo, D.;Park, S.H.;Jung, Y.G.;Lee, K.H.;Kim, C.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.19 no.2
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    • pp.103-108
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    • 2006
  • Microstructural evolution of Pt-aluminide coated Ni-based superalloy has been investigated with ductilization heat treatment. The Pt coat was prepared on the superalloy and then aluminide coating was conducted using a pack cementation process. Samples were heat-treated at $1050^{\circ}C$ for 2 hrs and the microstructure and element analysis were preformed. A various precipitated compounds were observed within the coating layer and the diffusion region in the Pt-aluminide coating and heat treatment, indicating that the bi-phase compounds of $PtAl_2$ and NiAl were performed during the Pt-aluminide coating, whereas $M_{23}C_6$, MC, $Ni_3Al$ and ${\sigma}$ phases were precipitated in the inter-diffusion region. The bi-phase compounds of $PtAl_2$ and NiAl were transformed into the single phase compound of $PtAl_2$ with the heat treatment, increasing the amount of carbide and ${\sigma}$ phase.

Performance Analysis of OFDM Communication System with the IQ Imbalance and Phase Noise (IQ Imbalance와 위상 잡음을 고려한 OFDM 통신 시스템의 성능 분석)

  • Kim, Sang-Kyun;Ryu, Heung-Gyoon;Kang, Byung-Su;Lee, Kwang-Chun
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.18 no.7
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    • pp.757-765
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    • 2007
  • OFDM system is an excellent high speed transmission method but it is seriously sensitive to the phase noise and IQ imbalance. Therefore, in this paper, we analyze the communication performance of the OFDM communication system with IQ imbalance and phase noise. Phase noise's variance can be calculated by integral calculus of phase noise power spectrum. From simulation results, it can be shown that the BER performances show different change according to the phase noise variance and IQ imbalance amount. When amplitude imbalance is ${\varepsilon}$=0.2; 0.3; 0.4 and phase imbalance is ${\phi}=10^0$, and distribution of phase noise is ${\sigma}^2=0.012$, BER is degraded by 2.88 dB, 3.61 dB, 4.09 dB in $10^{-5}$ in the respect of the SNR penalty.

A Study on Effect of PWHT on Mechanical Properties of Overlaid Weld Metal in Duplex Stainless Clad Vessel (이상 스테인리스 Clad강 육성 용접부의 기계적 성질에 미치는 후열처리의 영향에 관한 연구)

  • Seo Chang Gyo;Kim Yeong Il;Seong Hui Jun;Kim Dae Sun
    • Proceedings of the KWS Conference
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    • v.43
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    • pp.174-176
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    • 2004
  • The duplex stainless clad vessel with 38m & over thickness shall be performed to PWHT based on the ASME code. In this case, it is well-known that precipitators such as carbides and sigma($\sigma$) phase are formed at gram boundary between ferrite and austenite phase. Therefore, a weld test for simulating this situation has been planned and performed by 3309LMo71-1 for barrier layer and E2209Tl-1 for 2nd & over layer and then carried out to investigate the overlaid weld metal. Based on the test results, it could be concluded that PWHT should be carried out after the completion of 1st(barrier) layer and then 2 & over layer should be applied.

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Development of a hybrid sensor chip for power line phase measurement (전력선 위상 측정을 위한 하이브리드 센서 칩 개발)

  • Kim, Byoung-Il;Hong, Keun-Pyo;Hwang, Jin-Yong;Ahn, Byoung-Sun;Chang, Tae-Gyu
    • Proceedings of the KIEE Conference
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    • 2005.10b
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    • pp.436-438
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    • 2005
  • 본 논문에서는 전력선 위상 측정을 위해 A/D 변환기 및 위상계측 연산장치를 집적한 하이브리드 센서칩의 구현 기법을 제시하였다. 개발한 위상계측 연산장치는 recursive sliding-DFT에 기반하였으며 곱셈기의 시분할 공유 구조를 사용하여 칩의 구현 면적을 최소화 하였다. 60Hz의 전력선 신호를 중심주파수로 하는 AD 변환장치는 sigma-delta ADC를 기반으로 하여 8-bit 정밀도를 제공하며 아날로그부의 구현을 최소화하도륵 설계하였다. 설계한 하이브리드 센서칩은 컴퓨터 시뮬레이션 및 FPGA 구현을 통해 동작을 검증하였으며, 검증 완료후 $0.35{\mu}m$ CMOS 공정기술로 구현하였다. 전력선 위상을 측정하기 위해 구현된 4채널 하이브리드 센서 칩의 설계면적은 $5{\times}5m^2$ 의 약 20%정도를 차지하였다.

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Microstructures and characteristics of friction stir welded 304 stainless steel (304 스테인레스강 FSW부의 조직 및 특성)

  • ;Yutaka S. Sato;Hiroyuki Kokawa;Kazutaka Okamoto;Satoshi Hirano;Masahisa Inagaki
    • Proceedings of the KWS Conference
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    • 2004.05a
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    • pp.156-158
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    • 2004
  • The microstructural evolution in a 304 stainless steel weld during FSW was examined. The SZ and TMAZ showed typical dynamically recrystallized and recovered microstructures, respectively, The microstructural observation revealed that sigma phase was formed at the advancing side of the stir zone. A possibility was suggested that the rapid formation of the sigma phase is related to the transformation of austenite to delta-ferrite in the stir zone, from introduction of high strain and dynamic recrystallization during FSW.

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Fast Ambiguity Resolution using Galileo Multiple Frequency Carrier Phase Measurement

  • Ji, Shengyue;Chen, Wu;Zhao, Chunmei;Ding, Xiaoli;Chen, Yongqi
    • Proceedings of the Korean Institute of Navigation and Port Research Conference
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    • v.1
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    • pp.179-184
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    • 2006
  • Rapid and high-precision positioning with a Global Navigation Satellite System (GNSS) is feasible only when very precise carrier-phase observations can be used. There are two kinds of mathematical models for ambiguity resolution. The first one is based on both pseudorange and carrier phase measurements, and the observation equations are of full rank. The second one is only based on carrier phase measurement, which is a rank-defect model. Though the former is more commonly used, the latter has its own advantage, that is, ambiguity resolution will be freed from the effects of pseudorange multipath. Galileo will be operational. One of the important differences between Galileo and current GPS is that Galileo will provide signals in four frequency bands. With more carrier-phase data available, frequency combinations with long equivalent wavelength can be formed, so Galileo will provide more opportunities for fast and reliable ambiguity resolution than current GPS. This paper tries to investigate phase only fast ambiguity resolution performance with four Galileo frequencies for short baseline. Cascading Ambiguity Resolution (CAR) method with selected optimal frequency combinations and LAMBDA method are used and compared. To validate the resolution, two tests are used and compared. The first one is a ratio test. The second one is lower bound success-rate test. The simulation test results show that, with LAMBDA method, whether with ratio test or lower bound success rate validation criteria, ambiguity can be fixed in several seconds, 8 seconds at most even when 1 sigma of carrier phase noise is 12 mm. While with CAR method, at least about half minute is required even when 1 sigma of carrier phase noise is 3 mm. It shows that LAMBDA method performs obviously better than CAR method.

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Computer simulation of the effects of anisotropic grain boundary energy on grain growth in 2-D (이방성 결정립 계면에너지의 2차원 결정립 성장에 미치는 효과에 대한 컴퓨터 모사)

  • Kim, Shin-Woo
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.22 no.4
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    • pp.178-182
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    • 2012
  • The grain growth is very important because of its great influence on the various materials properties. Therefore, in this study, the effects of anisotropic grain boundary energy on grain growth in 2-D have been investigated with a large scale phase field simulation model on PC. A $2000{\times}2000$ grid system and the initial number of grains of about 73,000 were used in the computer simulation. The anisotropic ratio of grain boundary energy, ${\sigma}_{max}/{\sigma}_{min}$, has been varied from 1 to 3. As the anisotropy increased, the grain growth exponent, n, increased from 2.05 to 2.37. The grain size distribution showed a central plateau in the isotropic case, and was changed into no central plateau and the increasing population of very small grains in the anisotropic case, resulting from slowly disappearing grains. Finally, simulated microstructures were compared according to anisotropy.