• 제목/요약/키워드: ${\chi}$ phase

Search Result 391, Processing Time 0.025 seconds

Preparation of $ZrO_2-CaO$ fiber by using a chemical solution process

  • Hwang, Kyu-Seog;Jeon, Young-Sun;Kim, Sang-Bok;Kim, Chi-Kyun;Oh, Jeong-Sun;An, Jun-Hyung;Kim, Byung-Hoon
    • Journal of the Korean Crystal Growth and Crystal Technology
    • /
    • v.13 no.6
    • /
    • pp.267-271
    • /
    • 2003
  • In this work, chemical solution derived Ca-doped zirconia fiber has been prepared by using calcium- and zirconium-naphthenate. Fibrous $ZrO_2$-CaO was drawn from a sticky mixture. Dried gel fibers were finally annealed at $1000^{\circ}C$ for 1 h in argon. 91 mol%$ZrO_2$-9 mol%CaO fiber consisted of tetragonal, monoclinic and $CaZrO_3$ phases after annealing at $1000^{\circ}C$. On the other hand, samples annealed at $500^{\circ}C$ consisted of almost tetragonal single phase. Homogeneous fibers surface at $500^{\circ}C$ became rougher after $1000^{\circ}C$-annealing. The sample annealed at $1000^{\circ}C$ with relatively rough surface structure showed a high Calcium phocphate forming ability.

A Combined Rietveld Refinement on the Crystal Structure of a Magnetoelectric Aurivillius Phase $Bi_5Ti_3FeO_{15}$ Using Neutron and X-ray Powder Diffractions

  • Ko, Tae-Gyung;Jun, Chang-Ho;Lee, Jeong-Soo
    • The Korean Journal of Ceramics
    • /
    • v.5 no.4
    • /
    • pp.341-347
    • /
    • 1999
  • An ambiguity on the correct room temperature structure of $Bi_5Ti_3FeO_{15}$ was resolved using a combined Rietveld refinement of neutron and X-ray diffraction. The structure of this compound has been reported to have a space group of F2mm (adopting 2-fold rotation symmetry along the c-axis) or A21am. However, our diffraction, study reveals that some reflections would violate F-centering and confirm that the belong to $A2_1$am. Out refinement with the space group of $A2_1$am converged at $R_p=6.85%, R_wp=9.23%$ and $\chi^2$=1.66 for an isotropic temperature model with 85 variables. The lattice constants are a=5.4677(1) $\AA$, b=5.4396(1) $\AA$, and c=41.2475(8)$\AA$. In structure, Ti/Fe atoms at the oxygen octahedral sites of the perovskite unit are completely disordered, resulting in that these atoms are transparent in neutron diffraction. The octahedra of the perovskite unit are relatively displaced along the a-axis against the Bi atoms, which contribute as a major component to the spontaneous polarization of $Bi_5Ti_3FeO_{15}$.

  • PDF

A New Integrated Software Development Environment Based on SDL, MSC, and CHILL for Large-scale Switching Systems

  • Lee, Dong-Gill;Lee, Joon-Kyung;Choi, Wan;Lee, Byung-Sun;Han, Chi-Moon
    • ETRI Journal
    • /
    • v.18 no.4
    • /
    • pp.265-286
    • /
    • 1997
  • This paper presents a new software development environment that supports an integrated methodology for covering all phases of software development and gives integrated methods with tools for ITUT (Telecommunication Standardization Section of the International Telecommunication Union) languages. The design of the environment to improve software productivity and quality is based on five main concepts: 1) formal specifications based on SDL (Specification and Description Language) and MSC (Message Sequence Charts) in the design phase, 2) verification and validation of those designs by tools, 3) automatic code generation and a safe separate compilation scheme based on CHILL (CCITT High-Level Language) to facilitate programming-in-the-many and programming-in-the-large. 4) debugging of distributed real-time concurrent CHILL programs, and 5) simulation of application software for integrated testing on the host machine based on CHILL. The application results of the environment compared with other approaches show that the productivity is increased by 19 % because of decreasing implementation and testing cost, and the quality is increased by 83 % because of the formal specifications with its static and dynamic checking facilities.

  • PDF

Design and Implementation of Beam Steering System Based on Rotman lens and its Real-Time Display Device of Beam Receiving (로트만 렌즈를 이용한 빔 조향 시스템과 실시간 빔 수신표시 장치의 설계 및 구현)

  • Kim, In-Ryeol;ahn, Chi-Hyung;Oh, Soon-Soo
    • Journal of the Institute of Electronics and Information Engineers
    • /
    • v.53 no.5
    • /
    • pp.37-46
    • /
    • 2016
  • In this paper, we propose the beam-steering system using Rotman lens antenna operating at 2.442GHz which is to replace an expensive phase shifter. The overall system consists of the transmission antennas, Rotman lens and switch box. Setting the initial design conditions, it was designed and fabricated satisfying the requirements. From the result tested in the anechoic chamber, it was found that the beam can be steered using Rotman lens in the anechoic chamber. We also visually checked the beam-steering by turning on the LED of the rectenna showing the real-time beam receiving.

Numerical Study on Spontaneous Combustion in Coal Stockpile (저탄장에서의 석탄 자연발화에 관한 수치 해석적 연구)

  • HONG, JINPYO;KIM, JAEKWAN;CHI, JUNHWA;PARK, SUKWOON;SEO, DONGGYUN;LEE, JINHYANG
    • Transactions of the Korean hydrogen and new energy society
    • /
    • v.28 no.6
    • /
    • pp.721-728
    • /
    • 2017
  • In this work, an one-dimensional analysis on spontaneous combustion in a coal stockpile was conducted using a commercial software $gPROMS^{(R)}$ based on assumption suggested by Arioy and Akgun. According to them, it is assumed that there is temperature difference between the surface of coal particle and the gas surrounded around the particle, and it is also assumed that the velocity of the gas is constant and thus oxygen is fed to the stockpile with same velocity. The higher temperature zone is formed to the surface of the coal stockpile at the initial phase and it became deepen as time is taken. Finally it was found that the temperature difference between coal particle and the gas was calculated as $57^{\circ}C$ and spontaneous combustion have not been occurred during 6 months since coal was piled in the stock.

Preload effects on behaviour of FRP confined concrete: Experiment, mechanism and modified model

  • Cao, Vui Van
    • Advances in concrete construction
    • /
    • v.9 no.6
    • /
    • pp.597-610
    • /
    • 2020
  • Stress-strain models of fibre reinforced polymer (FRP) confined concrete have been widely investigated; however, the existing load which is always supported by structures during the retrofitting phase, namely 'preload', has been neglected. Thus, preload effects should be clarified, providing insightful information for FRP retrofitting of structures with preload conditions. Towards this aim, experiments were performed for 27 cylinder concrete specimens with the diameter 150 mm and the height 300 mm. Three specimens were used to test the compressive strength of concrete to compute the preloads 20%, 30% and 40% of the average strength of these specimens. Other 24 specimens were divided into 2 groups; each group included 4 subgroups. Four subgroups were subjected to the above preloads and no preload, and were then wrapped by 2 FRP layers. Similar designation is applied to group 2, but wrapped by 3 FRP layers. All specimens were tested under axial compression to failure. Explosive failure is found to be the characteristic of specimens wrapped by FRP. Experimental results indicated that the preload decreases 12-13% the elastic and second stiffness of concrete specimens wrapped by 2 FRP layers. The stiffness reduction can be mitigated by the increase of FRP layers. Preload negligibly reduces the ultimate force and unclearly affects the ultimate displacement probably due to complicated cracks developed in concrete. A mechanism of preload effects is presented in the paper. Finally, to take into account preload effects, a modification of the widely used model of un-preload FRP confined concrete is proposed and the modified model demonstrated with a reasonable accuracy.

Ultrasonic Images Enhancement of the SS Reference Specimen and the Reference Calibration Block for NPPs by the Combining Bases of Support for Spatial Frequency (공간주파수대역에서 기저대역 확장을 통한 원전 대비시험편과 대비 보정 시험편의 초음파 영상 개선)

  • Park, Chi-Seung;Kim, Seon-Jin
    • Korean Journal of Materials Research
    • /
    • v.13 no.10
    • /
    • pp.651-657
    • /
    • 2003
  • Ultrasonic microscope has been used to detect the defects on surface or inner solid. Conventionally, it has used at a single operating frequency. The resolution and quality of the measured images are determined by a characteristic of the transducer of the ultrasonic microscope. The conventional ultrasonic microscope has been used envelope detector to detect the amplitude of reflected signal, but the changes in amplitude is not sensitive enough for specimen with microstructure that in phase. In this paper, we have studied multi-frequency depth resolution enhancement with ultrasonic reflection microscope for the reflectors of a stainless steel reference specimen and a reference calibration block to be used as the material in nuclear power plants for ISI, PSI. Increased depth resolution can be obtained by taking two, three-dimensional images at more that one frequency and numerically combining the results. As results of the experiment, we could get enhanced images with the rate of contrast in proportion and high quality signal distribution for the image to the changing rate of depth for the reflectors of the two kinds of specimens.

Dipeptide (Tyr-Ile) Acting as an Inhibitor of Angiotensin-I-Converting Enzyme (ACE) from the Hydrolysate of Jellyfish Nemopilema nomurai

  • Kim, Yeon-Kye;Lim, Chi-Won;Yeun, So-Mi;Lee, Moon-Hee;Moon, Ho-Sung;Cho, Hyeon-Ah;Yoon, Na-Young;Yoon, Ho-Dong;Park, Hee-Yeon;Lee, Doo-Seog
    • Fisheries and Aquatic Sciences
    • /
    • v.14 no.4
    • /
    • pp.283-288
    • /
    • 2011
  • The jellyfish Nemopilema nomurai was hydrolyzed with papain and a novel dipeptide purified via ultrafiltration, gel filtration chromatography with Sephadex LH-20, and reverse phase chromatography using $C_{18}$ and $C_{12}$ columns. The IR, 1H NMR, 13C NMR, and MS spectrometer analyses showed that the dipeptide comprised tyrosine-isoleucine (Tyr-Ile). The $IC_{50}$ and $K_i$ values were $6.56{\pm}1.12$ and $3.10{\pm}0.28\;{\mu}M$, respectively, indicating competitive inhibition of angiotensin-I-converting enzyme (ACE). As a novel ACE-inhibitory active peptide, Tyr-Ile may have potential for use in antihypertensive therapy.

Effect of Rhamnolipids on Degradation of Anthracene by Two Newly Isolated Strains, Sphingomonas sp. 12A and Pseudomonas sp. 12B

  • Cui, Chang-Zheng;Zeng, Chi;Wan, Xia;Chen, Dong;Zhang, Jia-Yao;Shen, Ping
    • Journal of Microbiology and Biotechnology
    • /
    • v.18 no.1
    • /
    • pp.63-66
    • /
    • 2008
  • Anthracene is a PAH that is not readily degraded, plus its degradation mechanism is still not clear. Thus, two strains of anthracene-degrading bacteria were isolated from long-term petroleum-polluted soil and identified as Sphingomonas sp. 12A and Pseudomonas sp. 12B by a 16S rRNA sequence analysis. To further enhance the anthracene-degrading ability of the two strains, the biosurfactants produced by Pseudomonas aeruginosa $W_3$ were used, which were characterized as rhamnolipids. It was found that these rhamnolipids dramatically increased the solubility of anthracene, and a reverse-phase HPLC assay showed that the anthracene degradation percentage after 18 days with Pseudomonas sp. 12B was significantly enhanced from 34% to 52%. Interestingly, their effect on the degradation by Sphingomonas sp. 12A was much less, from 35% to 39%. Further study revealed that Sphingomonas sp. 12A also degraded the rhamnolipids, which may have hampered the effect of the rhamnolipids on the anthracene degradation.

Effect of Intercritical Annealing on the Dynamic Strain Aging(DSA) and Toughness of SA106 Gr.C Piping Steel

  • Lee, Joo-Suk;Kim, In-Sup;Park, Chi-Yong;Kim, Jin-Weon
    • Nuclear Engineering and Technology
    • /
    • v.32 no.1
    • /
    • pp.77-87
    • /
    • 2000
  • It is reported that the toughness and safety margins of the SA106 Gr.C main steam line piping steel is reduced due to dynamic strain aging (DSA) at the reactor operating temperature for Leak-Before-Break (LBB) application. In this study, intercritical annealing in two-phase ($\alpha$+${\gamma}$)region was performed to investigate the possibility of improving the toughness and reducing DSA susceptibility. The manifestations of DSA were still observed in the tensile tests of the annealed specimens. However, the ductility loss caused by DSA was smaller than that in the as-received material. Furthermore, the intercritical annealing was able to increase the Charpy impact toughness by 1.5 times compared to as-received. With the heat treatment, we could obtain microstructural changes such as the cleaner retained ferrite, increased ferrite content and somewhat finer grain size. It is considered that the reduced DSA was induced by cleaner retained ferrite, which in turn resulted in higher impact toughness in addition to the general toughening due to finer grain sizes and increased ferrite content.

  • PDF