• Title/Summary/Keyword: $\mu$ synthesis

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Fabrication and Mechanical Properties of A356/SiCp Manufactured by Gas-Particle Co-injection Method (가스-입자 동시주입법에 의한 A356/SiCp 복합재료의 제조 및 기계적 특성)

  • Lee, Jung-Mu;Kang, Suk-Bong;Eum, Chil-Yong;Lim, Cha-Yong
    • Journal of Korea Foundry Society
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    • v.21 no.1
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    • pp.33-40
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    • 2001
  • Among the many techniques available to synthesis metal matrix composites, liquid phase processing, especially, conventional casting process such as stir-casting process is particularly attractive for their simplicity, economy and flexibility, In the present study, A356/20%SiCp composites were fabricated by gas-particle co-injection method. The gas-particle co-injection method is a modified stir-casting method and the corporation of particle could be improved by acceleration of particles due to rotation of impeller and gas purging. The microstructures and mechanical properties such as tensile properties and resistance to wear of fabricated materials were examined. Further, the particle injection mechanism in gas-particle co-injection method was discussed.

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Effects of Ganoderma lucidum on the IL-1, TNF and IL-12 Gene Expression of Macrophages (영지버섯이 탐식세포의 IL-1, TNF 및 IL-12 유전자 발현에 미치는 영향)

  • 배지현
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.26 no.5
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    • pp.978-982
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    • 1997
  • In order to investigate the immunomodulatory mechanism of Ganoderma lucidum, the effects of protein-bound polysacchride of Ganoderma lucidum on the proliferation and cytokine gene expression of mouse peritoneal macrophages was studied. In the macrophage proliferation assay using the BrdU labeling reagent, the GLA component extracted from Ganoderma lucidum or GLB from the bud of Ganoderma lucidum were added to the medium at the concentration of 0 to 256ug/ml. DNA synthesis of the macrophage was increased at 16ug/ml of GLA and 64ug/ml of GLB, respectively. In the reverse transcription polymerase chain reaction(RT-PCR), the cytokine(TNF, IL-1, and IL-12) gene and $\beta$-actin expression were also analyzed. 20$\mu\textrm{g}$/ml of either GLA or GLB increased TNF and IL-1 expression of the macrophages.

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Synthesis of Ultrafine TaC Powders Using Tantalum Oxalate Solution (수산 탄탈륨 용액을 이용한 초미립 TaC 분말의 합성)

  • Kwon, Dae-Hwan;Hong, Seong-Hyeon;Kim, Byoung-Kee
    • Korean Journal of Materials Research
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    • v.13 no.12
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    • pp.806-811
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    • 2003
  • Ultrafine TaC powders were synthesised by spray drying using tantalum oxalate solution. The spray dried powders were spherical shape and less than 30 $\mu\textrm{m}$ in size. The powders calcined at 500 and X$700^{\circ}C$ showed amorphous structures and $Ta_2$$O_{5}$ phase was obtained by calcining at $700^{\circ}C$. The particle size and shape remains constant after calcination. The calcined spherical powders were composed of an agglomerate of primary particles under 50 nm in size. The complete formation of TaC could be achieved by heat treatment at $1050^{\circ}C$ for 6 hrs. The observed size of TaC powders by TEM was less than 200 nm.

ZnO Nanowires Fabricated by Pulsed Laser Deposition using Gold Catalyst (PLD-Furnace로 증착시킨 금촉매를 이용한 ZnO 나노와이어 합성)

  • Son, Hyo-Jeong;Jeon, Kyung-Ah;Lee, Sang-Yeol
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.5-6
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    • 2005
  • ZnO nanowlres (NWs) were fabricated using Au as catalyst for a method combining laser ablation cluster formation and vapor-liquid-solid (VLS) growth. The target used in synthesis was pure ZnO ceramics. Two different substrates were used; (0001)-oriented sapphires and Au-coated sapphires. The Au thin film was deposited by thermal evaporation and the thickness was about 50 ${\AA}$. ZnO NWs were only formed in case of that used catalyst metal. Field effect scanning electron microscopic (FESEM) investigation showed that the average diameter of ZnO NWs was about 70 nm and the typical lengths varied from $3{\sim}4{\mu}m$.

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Synthesis of diamond at low pressure (저압력에서의 다이아몬드 함성)

  • Park, Sang-Hyun;Park, Jae-Yoon;Koo, Hyo-Geun;Kim, Kyoung-Hwan
    • Proceedings of the KIEE Conference
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    • 1999.11d
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    • pp.870-872
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    • 1999
  • The particles were deposited on silicon wafers at low pressure:1[torr] from $CH_4-H_2$ mixed gas by using RF plasma CVD, and were investigated by SEM and Raman spectroscopy. The results are as following; Diamond particles were synthesized under $CH_4/H_2$ concentration of 1[%], however amorphous cabon particles were synthesized over $CH_4/H_2$ concentration of 2[%]. Growth rate of diamond particle was 2.2 times: $0.8[{\mu}m/h]$ as much as that synthesized at 25[torr].

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Synthesis and characterization of novel polyimides with diamines containing thiophene moieties

  • Yoon, Mu-Ju;Yoon, Tae-Ho
    • Rapid Communication in Photoscience
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    • v.1 no.2
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    • pp.27-29
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    • 2012
  • Noble diamine monomers containing thiophene moiety were prepared, such as 2,5'''-diamino-2, 2':5', 2'':5'', 2'''-quaterthiophene (4TDA) and 2, 5'''''-diamino-3'', 4'''-dihexyl-2,2':5', 2'':5'', 2''':5''', 2'''':5'''', 2'''''-sexithiophene (6TDA). Then, these monomers were utilized to prepare polyimides with 3,6-diphenylpromellitic dianhydride (DPPMDA), 3,6-di(4'-trifluoro-methylphenyl) pyromellitic dianhydride (6FPMDA) or 3,6-di(3',5'-bis (trifluoromethyl)phenyl) pyromellitic dianhydride (12FPMDA) via a conventional two-step process. The polyimides were characterized by FT-IR, TGA and DSC, and then subjected CV, UV-vis and PL measurements. The polyimides containing thiophene moiety exhibited high glass transition temperatures ($280{\sim}310^{\circ}C$) and excellent thermal stability (> $420^{\circ}C$) in air as well as green emission (535~586 nm).

Synthesis and Antiviral Activity of Novel 2′-Methyl and 4′-Phenyl Branched Carbocyclic Nucleosides (2′-메칠 및 4′-페닐 측쇄를 가진 새로운 카보사이클릭 뉴크레오사이드의 합성 및 항바이러스 약효검색)

  • 양선화;홍준희
    • YAKHAK HOEJI
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    • v.48 no.1
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    • pp.88-92
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    • 2004
  • In this study; a series of 2',4'-doubly branched carbocyclic nucleosides (8,9,10) were synthesized from simple acyclic ketone derivative as starting material. The installation of the 4'-quaternary carbon needed was carried out using a 〔3,3〕-sigmatropic rearrangement. In addition, the introduction of a methyl group in the 2'-position was accomplished by Grig-nard reaction. Bis-vinyl was successfully cyclized using a Grubbs' catalyst II. The natural bases (adenine, cytosine, uracil) were efficiently coupled with the use of a Pd(0) catalyst. Although all the synthesized compounds were assayed against several viruses, only cytosine analogue 9 showed weak antiviral viral activity (EC$_{50}$=45.4 $\mu$M) against CoxB3 virus.s.

A Study on the Signal Processing and Robust Control for a 3-DOF Active Vibration Isolator (3자유도 능동형 제진 시스템을 위한 신호처리 및 강인제어에 관한 연구)

  • Moon, Jun-Hee;Kim, Hwa-Soo;Pahk, Heui-Jae
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2006.05a
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    • pp.153-156
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    • 2006
  • The vibration isolation system is a system that attenuates the vibration transmitted from surroundings by using external energy supply like electricity and feedback and/or feedforward functions. Such a system needs stiff structure to make precise positioning without ripple within a certain bandwidth. So, a horizontal and rotary arrangement of the actuation module is suggested by using lever linkage. Modeling and kinematic formulation are completed and system identification is accomplished to tune the design variables accurately. The vibration isolation control is performed by mu-synthesis with the uncertainties in design variables. Low frequency signal enhancement circuit and saturation proof integration algorithm are devised to use seismic sensors for displacement control. This overall system shows good disturbance rejection performance.

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전북대학교 소재공정용 200 kW ICP(RF) 플라즈마 발생 장치 구축

  • Lee, Mi-Yeon;Kim, Jeong-Su;Choe, Chae-Hong;Kim, Min-Ho;Seo, Jun-Ho;Hong, Bong-Geun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.538-538
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    • 2012
  • 전북대학교 고온 플라즈마 응용 연구 센터는 교육과학기술부 기초연구사업 중 고가연구장비 구축사업의 일환으로 고부가가치 재료 연구 및 시험생산이 가능한 소재공정용 200kW ICP(RF) 플라즈마 발생장치를 구축하고 있다. 200 kW급 ICP (RF)형 플라즈마 발생장치는 수~수십 um 크기의 금속, 세라믹 등 고융점 원료분말 등을 수~수십 um 크기의 금속, 세라믹 등 고융점 원료 분말을 순간적으로 용해, 기화 및 분해시키고 이들 기화 또는 분해된 증기를 급랭시키는 과정에서 대량으로 초미분($<1{\mu}m$)을 합성하는 RF 플라즈마 분말 합성 시스템으로 시간당 1 kg 이상의 나노 분말의 제조가 가능하도록 설계 제작된 생산 지원용 대형 ICP(RF) 플라즈마 장치이다.

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Effect of Grain Growth Inhibitor on Sintering of Nanophase WC-10wt%Co (초미립 WC-l0wt%Co 초경 분말의 소결시 입자 성장 억제제 첨가 효과 연구)

  • 김병기
    • Journal of Powder Materials
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    • v.1 no.2
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    • pp.208-216
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    • 1994
  • A radically new approach to the in situ synthesis of the consituent phases of a composite structure has enabled the production of a new WC/Co materials with an ultrafine microstructure. The process for synthesizing nanophase WC/Co powders consists of spray drying from solution to form a homogeneous precursor powder, and thermochemical conversion of the precursor powder to the nanophase WC/Co powder. Near theoretical density of pure nanophase WC-10 wt%Co has been obtained in only 30 sec at 140$0^{\circ}C$. But WC particles were grown up very rapidly with longer sintering time to get full density. To overcome coarsening of WC particle during sintering, VC, TaC and VC/TaC were used as the grain growth inhibitor with different amount respectively. VC/TaC doped WC-10 wt%Co was shown superior hardness and TRS and microstructure was maintained ultrafine scale (average WC size is less than 0.1 ${\mu}{\textrm}{m}$).

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