• Title/Summary/Keyword: $\beta-Ti$ 합금

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Biocompatibility of Ti-8Ta-3Nb alloy with fetal rat calvarial cells (백서 태자 두개관세포에서 Ti-8Ta-3Nb 합금의 생체적합성)

  • Cho, In-Goo;Cui, De-Zhe;Kim, Young-Joon;Lee, Kyung-Ku;Lee, Doh-Jae
    • Journal of Periodontal and Implant Science
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    • v.36 no.4
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    • pp.849-861
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    • 2006
  • 타이타늄은 기계적 특성이 우수하고 생체적합성이 뛰어나 의료용 장비의 주 재료로 사용되고 있으며 타이타늄 보다 기계적 특성이 더 우수한 타이타늄 합금들(주로 Ti-6Al-4V와 Ti-6Al-7Nb 합금)도 개발되어 치과와 의료용 임플란트로 사용되고 있다. 그러나 타이타늄 합금 성분들 중 알루미늄 (aluminum)과 바나디움(vanadium)은 인체에 노출되면 세포손상과 신경계에 문제를 일으킬 수 있다. 따라서 인체에 독성이 없으면서 기계적 성질과 생체적합성이 우수한 타이타늄 합금의 개발이 필요하다. 최근 인체에 독성이 없는 성분들이 함유된 새로운 ${\beta}$ - 형태의 타이타늄 합금들이 개발되고 있는데, ${\beta}$ - 타이타늄 합금은 그 기계적 성질이 기존의 ${\alpha}+{\beta}$ 타이타늄 합금에 비해 우수하다고 알려져 있다. 최근 새로운 ${\beta}$ - 타이타늄 합금이 전남대학교 부설 타이타늄 연구소에서 개발되었다. 이 연구는 새로 개발된 ${\beta}$ - 타이타늄 합금의 생채 적합성을 세포 증식도, 알카리 인산 분해 효소 활성과 유전자 증폭을 통해 알아보고자 하였다. 그 결과는 다음과 같다; 1. Titanium-6aluminum-4vanadium (Ti-6Al-4V) 합금 표면애서의 세포 증식율은 Titanium-Titanium8Tantalum-3Niobium (Ti-8Ta-3Nb) 합금과 순수 타이타늄 표면에 비해 유의하게 낮았다(p<0.00l). Ti-8Ta-3Nb 합금 표면에서의 증식도는 순수 타이타늄 표면과 유사하였다. 2. Ti-8Ta-3Nb 합금과 순수 타이타늄에서 배양된 세포이 알카리 인산 분해 효소의 활성도는 Ti-6Al-4V 합금에서의 것보다 유의하게 높았다 (p<0.001). 3. 유전자 증폭 분석 결과, Ti-8Ta-3Nb 합금과 순수 타이타늄에서 collagen type I과 bone sialoprotein mRNA 가 유사한 수준으로 발현되었다. 이상의 결과는 생체 적합성 측면에서 Ti-8Ta-3Nb 합금과 순수 타이타늄의 차이가 없음을 보여주며 따라서 Ti-8Ta-3Nb 합금이 의학 및 치의학 영역에서 새로운 임프란트 재료로 사용될 수 있음을 의미한다.

Effect of multi-layered HA/Ti coating on biological Ti-30Ta-xNb alloys (생체용 Ti-30Ta-xNb 합금의 HA/Ti 복합코팅의 영향)

  • Jeong, Yong-Hun;Choe, Han-Cheol;Go, Yeong-Mu
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2007.11a
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    • pp.51-51
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    • 2007
  • 기존에 있는 Ti 합금의 여러 가지 단점을 보완하기 위해 골과의 탄성계수 차이를 줄이고 독성이 없는 Ta, Nb와 같은 ${\beta}$형 안정화 원소를 Ti 와 합금하여 Ti-30Ta-(3${\sim}$15wt%)Nb 합금을 제조하여 RF-magnetron sputter를 이용하여 Ti/HA 복합코팅을 하여 코팅된 합금의 전기화학적 특성을 조사하였다.

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Characteristics of Brazing of Eyewear Frame Ti Alloy with Electric Resistance (전기저항을 이용한 안경테용 Ti 합금의 땜질 특성)

  • Park, Jeong-Sik;Lee, Jeong-Yeong
    • Journal of Korean Ophthalmic Optics Society
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    • v.12 no.4
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    • pp.15-18
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    • 2007
  • Titanum and its alloys have been used as the important materials of eyewear frame because of its light weight, mechanical strength and corrosion resistance. This study investigated the characteristics of P-Ti and ${\beta}$-Ti alloys in accordance with joining conditions by electric resistance brazing. Hardness of P-Ti and ${\beta}$-Ti has been reduced because of an increase of grain size by the growth of brazing time. Hardness reduction and reduction area by grain growth were largely appeared in P-Ti than ${\beta}$-Ti.

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Study for Fatigue Crack Propagation Behavior of Ti-alloy (Ti 합금의 피로 특성 고찰)

  • 정화일;조규종
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 1997.10a
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    • pp.786-789
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    • 1997
  • Ti-6Al-4V has been used widely in biomedical field. But because of its toxicity, the ${\beta}$ stabilizing element, V, in Ti-6Al-4V has been replaced by Nb, Ta. Ti-10Ta-10Nb has been developed for biomedical applications. The fatigue crack propagation behavior of Ti-alloy(Ti-10Ta-10Nb) was investigated, in comparison with that of pure Ti. In order to better understand the fundamental fatigue behavior of Ti-10Ta-10Nb, rotating bending fatigue tests have been carried out. Ti-10Ta-10Nb has a better fatigue strength than pure Ti. In this paper, fatigue life has been predicted with Nisitani's equation of the fatigue crack propagation that can be established by measuring fatigue crack growth rates.

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High Temperature Compressive Deformation Behavior of Ti-6Al-2Sn-4Zr-6Mo Alloy (Ti-6Al-2Sn-4Zr-6Mo 합금의 고온압축 변형거동)

  • Hyun, Yong-Taek;Lee, Yong-Tai;Lee, Chan-Gyu
    • Korean Journal of Materials Research
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    • v.11 no.2
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    • pp.82-87
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    • 2001
  • The hot deformation behavior of Ti-6Al-2Sn-4Zr-6Mo(Ti6246) alloy was investigated in both the $\alpha$+$\beta$ and $\beta$-phase fields by conducting compression tests over a strain rate range of $10^{-3}s^{-1}$ to $10^0s^{-1}$. The flow stress was increased with increasing strain rate and decreasing test temperature. The flow curves obtained at temperatures below 90$0^{\circ}C$ exhibited a flow softening. However, in the $\beta$-phase field, above 95$0^{\circ}C$, the flow stress increased monotonically with plastic strain approaching steady state values. Constitutive equations for the dependence of flow stress on strain, strain rate, and temperature were developed through the analysis of the flow curves.

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The Characteristics of Ultrasonic Signals for Detecting Micro-Defects in Ti-6Al-4V Alloy (Ti-6Al-4V 합금의 내부 미소결함에 따른 초음파 신호 특성 연구)

  • Choi, Sang-Woo;Lee, Joon-Hyun;Kubota, M.;Murakami, Y.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.21 no.6
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    • pp.591-597
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    • 2001
  • Ti alloy is used for essential parts of aircraft for high temperature environment. Although Ti alloy has excellent performance in regard to mechanical properties, it is difficult ot find fatigue cracks by nondestructive ultrasonic inspection due to its two-phase microstructure, which consists of hard alpha and beta phases. Sound energy reflected from microstructural features in the component produces a background inspection noise which is seen even when no defects are present. This noise can inhibit the detection of critical internal defects such as pores cracks or inclusions. To obtain fundamental data on ultrasonic inspection of Ti alloy, ultrasonic testing was performed using a specimen with small drill holes and ultrasonic wave propagation velocites were measured.

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A Study on the Characteristics for High Frequency Induction Heating of Ti Alloy Groove Wire (안경테용 Ti 합금 홈선의 고주파유도가열처리에 따른 특성 변화에 관한 연구)

  • Park, Jeong-Sik;Jang, Woo-Yeong;Lee, Jeong-Yeong
    • Journal of Korean Ophthalmic Optics Society
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    • v.12 no.3
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    • pp.55-58
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    • 2007
  • Titanum and its alloys have been used as the important materials of eyewear frame due to its light weight, mechanical strength and corrosion resistance. This study investigates hardness and microstructures of titanum alloy groove wires in according with heating time by high frequency induction heating. Because of increase of grain size by the growth of heating time, hardness of ${\beta}-Ti$ has reduced. Hardness of Ti-325 reduced until 2 sec and rapidly increased at 3 sec by high frequency induction heating. It is observed that hardness of Ti-325 reduces by the increase of the grain size until 2 sec and suddenly increased by the development of the detailed ${\alpha}+{\beta}$ lamella at 3 sec.

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Study on the mechanical Properties of Ti-8Ta-3Nb Alloys for Biomaterials (생체재료용 Ti-8Ta-3Nb 합금의 물성변화 고찰)

  • 이경원;반재삼;유영선;조규종
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.1374-1377
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    • 2003
  • Ti-8Ta-3Nb is made for biomaterial. The experimental speciments are as-cast Ti-8Ta-3Nb and Ti-8Ta-3Nb swaged. The solution treatment in the range 760-96$0^{\circ}C$have been carried out. The microstructural investigations have been carried out on the specimens after the solution treatment. and the hardness have been measured. And the specific heat and the dilatometer of Ti-8Ta-3Nb swaged have been measured. From the result, the $\beta$ transus of the alloy was determined to be 880-86$0^{\circ}C$.

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