• Title/Summary/Keyword: $\beta$-phase

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Manufacturing Process of the Ti-6Al-4V Billet by the Open-die Forging (자유형 단조 공정에 의한 Ti-6Al-4V 빌렛 제조기술)

  • Kim, K.J.;Choi, S.S.;Hwang, C.Y.;Kim, J.S.;Yeom, J.T.;Lee, J.S.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2006.05a
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    • pp.377-380
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    • 2006
  • Manufacturing process of Ti-6Al-4V alloy billet was investigated with FEM simulation and experimental analysis. Before the breakdown process of Ti-6Al-4V alloy ingot, FEM simulation for the breakdown processes of Ti-6Al-4V alloy ingot was used to calculate the forging load and state variables such as strain, strain rate and temperature. In order to breakdown the ingot structure and make an equiaxed structure billet, two different processes were employed for a VAR/VAR processed Ti-6Al-4V alloy ingot. Firstly, the ingot was cogged in single-phase $\beta$ field at the temperature of $1,100^{\circ}C$. In the process, the coarse and inhomogeneous structure developed by the double melting process was broken down. The second breakdown was performed by upsetting and cogging processes in $\alpha+\beta$ phase field to obtain the microstructure of fine equixed $\alpha$ structure in the matrix of transformed $\beta$. Finally, the mechanical properties of Ti-6Al-4V alloy billet made in this work were compared with those of other billet and ring product.

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Chemical Vapor Deposition of $\beta$-SiC by Pyrolysis of MTS and Effect of Excess C Sources (MTS의 열분해를 이용한 $\beta$-SiC의 화학증착 및 Excess C 공급원의 영향)

  • 최병진;박병옥;김대룡
    • Journal of the Korean Ceramic Society
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    • v.30 no.1
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    • pp.46-54
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    • 1993
  • $\beta$-SiC was chemically vapor deposited by pyrolysis of MTS+H2 gas mixture. The experiments were conducted in the temperature range of 1100~150$0^{\circ}C$ with a r.f. induction furnace under atmospheric pressure. The IR, XRD, EDS and AES analysis revealed that the free Si was always codeposited with SiC below 140$0^{\circ}C$, regardless of the total flow rate and MTS concentration, whereas $\beta$-SiC single phase was deposited at 150$0^{\circ}C$. C3H8 or CH2Cl2 as an excess C sources, was supplied with MTS in order to obtain stoichiometric SiC at low temperature. With the addition of C3H8 or CH2Cl2, the deposition rate was increased and $\beta$-SiC single phase could be deposited even at temperature as low as 110$0^{\circ}C$. In the absence of C3H8 or CH2Cl2, the microhardness of the layer was quite low (

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Analysis of the Strength Property for TiC-Mo Composites at High Temperature

  • Shin, Soon-Gi
    • Korean Journal of Materials Research
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    • v.24 no.4
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    • pp.201-206
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    • 2014
  • TiC-21 mol% Mo solid solution (${\delta}$-phase) and TiC-99 mol% Mo solid solution (${\beta}$-phase), and TiC-(80~90) mol% Mo hypo-eutectic composite were deformed by compression in a temperature range from room to 2300 K and in a strain rate range from $4.9{\times}10^{-5}$ to $6.9{\times}10^{-3}/s$. The deformation behaviors of the composites were analyzed from the strengths of the ${\delta}$- and ${\beta}$-phases. It was found that the high strength of the eutectic composite is due primarily to solution hardening of TiC by Mo, and that the ${\delta}$-phase undergoes an appreciable plastic deformation at and above 1420 K even at 0.2% plastic strain of the composite. The yield strength of the three kinds of phase up to 1420 K is quantitatively explained by the rule of mixture, where internal stresses introduced by plastic deformation are taken into account. Above 1420 K, however, the calculated yield strength was considerably larger than the measured strength. The yield stress of ${\beta}$-phase was much larger than that of pure TiC. A good linear relationship was held between the yield stress and the plastic strain rate in a double-logarithmic plot. The deformation behavior in ${\delta}$-phase was different among the three temperature ranges tested, i.e., low, intermediate and high. At an intermediate temperature, no yield drop occurred, and from the beginning the work hardening level was high. At the tested temperature, a good linear relationship was held in the double logarithmic plot of the yield stress against the plastic strain rate. The strain rate dependence of the yield stress was very weak up to 1273 K in the hypo-eutectic composite, but it became stronger as the temperature rose.

TEM Diffraction Analysis of Metastable Phases in Beta Ti Alloys (베타 티타늄합금의 준 안정상 TEM 회절도형 분석)

  • Choe, Byung Hak;Shim, Jong Heon;Kim, Seung Eon;Hyun, Yong Taek;Park, Chan Hee;Kang, Joo-Hee;Lee, Yong Tai;Kim, Young Ouk
    • Korean Journal of Materials Research
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    • v.25 no.8
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    • pp.403-409
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    • 2015
  • Metastable phase characteristics of beta Ti alloys were investigated to consider the relationship of the microstructure and diffraction pattern in TEM. TEM analysis showed that the microstructure was mottled as a modulated structure, and the diffraction pattern was composed of spot streaks between the main spots of a stable beta phase with a specific lattice relationship. The modulated structure may be induced by short distance slip or atom movement during a very short interval of solution treated and quenched (STQ) materials. The athermal ${\omega}$ phase, which could be precipitated at low temperature aging, is also analysed by the metastable phase. The metastable phases including athermal ${\omega}$ phase had a common characteristic of hardened and brittle behavior because the dislocation slip was restricted by a super lattice effect due to short distance atom movement at the metastable state.

Fabrication of Ultra Fine β-phase Ti-Nb-Sn-HA Composite by Pulse Current Activated Sintering

  • Woo, Kee-Do;Wang, Xiaopeng;Kang, Duck-Soo;Kim, Sang-Hyuk;Woo, Jeong-Nam;Park, Sang-Hoon;Liuc, Zhiguang
    • Journal of Powder Materials
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    • v.17 no.6
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    • pp.443-448
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    • 2010
  • The $\beta$ phase Ti-Nb-Sn-HA bio materials were successfully fabricated by high energy mechanical milling and pulse current activated sintering (PCAS). Ti-6Al-4V ELI alloy has been widely used as biomaterial. But the Al has been inducing Alzheimer disease and V is classified as toxic element. In this study, ultra fine sized Ti-Nb-Sn-HA powder was produced by high energy mechanical milling machine. The $\beta$ phase Ti-Nb-Sn-HA powders were obtained after 12hr milling from $\alpha$ phase. And ultra fine grain sized Ti-Nb-Sn-HA composites could be fabricated using PCAS without grain growth. After sintering, the microstructures and phase-transformation of Ti-Nb-Sn-HA biomaterials were analyzed by scanning electron microscope (SEM) and X-ray diffraction (XRD). The relative density was obtained by Archimedes principle and the hardness was measured by Vickers hardness tester. The $\beta$-Ti phase was obtained after 12h milling. As result of hardness and relative density, 12h milled Ti-Nb-Sn-HA composite has the highest values.

Induction of $\beta$-Lactamase on $\beta$-Lactam Antibiotics Resistant Bacterium ($\beta$-Lactam계 항생물질 내성균주의 $\beta$-Lactamase 생산의 유도)

  • 조경순;정영기
    • Journal of Life Science
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    • v.8 no.6
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    • pp.723-728
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    • 1998
  • Bacillus subtilis J105, high resistant bacteria against $\beta$-lactam antibiotics, become higher resistant through induction of $\beta$--lactamase in the presence of $\beta$--lactam antibiotics. When there is no antibiotics in medium, the production of resistance-inductive $\beta$--lactamase reached its plateau 15 hours later. But when there is ampicillin (500$\mu\textrm{g}$/$m\ell$) in medium, the production of enzyme reached its plateau 25 hours later since cultivating bacteria, whereas it is found that enzyme 2,900 units/$m\ell$ about 20 times as much as compared with not-presence of antibiotics was actived. In addition, as the result of MIC comparing applying ampicillin-treated and non-treated strain MIC of ampicillin-treated strain is about 2~27 times higher. It is considered that this strain induce $\beta$--lactamase production by ampicil-lin-treatment, then increasing it resistance. It is found that this resistant strain induce $\beta$--lactamase production against cephalosporin antibiotics as well as peni-cillin. As the result of examining the time of adding antibiotics for each phase of growth, it is concluded that logarith-mic phase is the most effective. As the aboves, it is suggested that this strain is a peculia strain that its resistance is induced high by various $\beta$--lactam antibiotics.

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Characteristics of Tensile Strength and Corrosion Resistance of Lead- free Brass Containing 1 wt.% of Bi (1 wt.% Bi 함유 무연황동의 인장강도와 내식특성에 대한 연구)

  • Joo, Y.S.;Lee, S.B.;Kim, S.Y.;Joo, C.S.;Jung, B.H.
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.3
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    • pp.133-139
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    • 2011
  • This study has been investigated for tensile properties with lead-free brass containing 1 wt.% of Bi. And also characteristic of corrosion resistance was analyzed by polarization test. An increase of tempering temperature was found to tend to decrease tensile strength, and percentage of elongation was shown to be the lowest value at $300^{\circ}C$. On the other hand, the elongation was increased with an increase of tempering temperature after $300^{\circ}C$. The change of mechanical properties was closely related with the content and shape of acicular Witmanst$\ddot{a}$tten ${\alpha}$ formed at the interface of ${\beta}$ phase as well as in ${\beta}$ phase. Tensile strength had a tendency to be decreased with an increase of test temperature. The elongation was shown to be the lowest value at around $300^{\circ}C$, while it began to increase as test temperature rose after $300^{\circ}C$. It might be speculated that the reason that elongation was decreased was found to form bismuth film at the interface of ${\alpha}/{\beta}$ phase leading to be easily brittle when loaded by tensile stress. The lead-free brass containing 1 wt.% of Bi had similar characteristic of corrosion resistance with a free-cutting brass with 3.4 wt. % of Pb in spite of higher fraction of ${\beta}$ phase.

Effects of Ti Addition on Microstructure and Mechanical Properties of Mg-xAl-yZn Magnesium Alloys by Thixomolding Process (Thixomolding 공정으로 제조된 Mg-xAl-yZn계 마그네슘 합금의 미세조직과 기계적 물성에 미치는 Ti 첨가 영향)

  • Park, Sung-Hyun;Jang, Ho-Seung;Lee, Ji-Ho;Park, No-Jin;Oh, Myung-Hoon
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.4
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    • pp.168-174
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    • 2019
  • The microstructural features and relative room temperature mechanical properties were investigated in various compositions of Mg-xAl-yZn alloys by thxiomolding process. The microstructure was composed of ${\alpha}$-Mg particles and mixture of ${\alpha}$-Mg and ${\beta}-Mg_{17}Al_{12}$ eutectic phase. The amount of ${\beta}-Mg_{17}Al_{12}$ eutectic phase in mixture was increased with increasing Al and Zn contents without grain refinement. After adding Ti content, however, the morphology of ${\beta}-Mg_{17}Al_{12}$ eutectic phase transformed from net-like to discontinuous shape and the average grain size reduced. To determine the relationship between microstructural features and their mechanical properties, a tensile test was performed at room temperature. As a result, it was found that the mechanical properties were improved in all of Ti contained alloys due to increased elongation and the mechanisms are discussed in terms of microstructural evolution.

Genotypic Variation of Rapid Canopy Closure and Its Relationship with Yield of Rice (벼 조기초관폐쇄성의 품종 변이 및 수량과의 관계)

  • Fu, Jin-Dong;Lee, Byun-Woo
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.53 no.2
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    • pp.137-143
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    • 2008
  • Rapid canopy closure (RCC) is one of the physiological attributes that may enhance genetic yield potential of rice (Oryza sativa L.) in a growing season. Crop growth before canopy closure could be described by an exponential equation of $y\;=\;{\alpha}{\cdot}{\exp}({\beta}{\cdot}t)$ where $\alpha$ is the crop leaf area index (LAI) or shoot dry weight (DW), t is the thermal time, $\beta$ is the LAI or DW at the beginning of the exponential growth and is the relative growth rate of LAI ($m^2m^{-2}^{\circ}C^{-1}$) or DW($gg^{-2}^{\circ}C^{-1}$). Field experiment using 22 cultivars revealed that the exponential growth phase before canopy closure can be divided into two sections; an earlier section during which crop dry weight and LAI of varieties are highly dependent on $\alpha$ and a second section where crop dry weight and LAI are highly dependent on $\beta$. Grain weight had significantly positive correlation with $\alpha$ parameter and dry weight and LAI during early exponential phase. The parameter $\beta$ of the exponential growth curve had positive and significant correlation with the LAI and dry weight during the late exponential growth phase, grain number per unit area, and grain yield. There was genotypic difference for RCC parameters, $\alpha$ and $\beta$, indicating the possibility of genetic improvement for these traits.

EVOLUTION OF SUNSPOTS BASED ON VECTOR MAGNETOGRAM AND $H\beta$ FILTERGRAM OBSERVATION

  • LEE SANG WOO;YUN HONG SIK;MOON YONG JAE;WANG JIA LONG
    • Journal of The Korean Astronomical Society
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    • v.29 no.1
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    • pp.9-18
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    • 1996
  • We have analyzed vector magnetograms and $H\beta$ filtergrams of two sunspot groups, one in a growing phase and the other in a decaying phase. In this study, the temporal evolution of their magnetic morphology has been investigated in association with solar activity. The morphological variations of the growing and decaying phase of these sunspots revealed in detail the coalescence of small spots into a large spot and the fragmentation of a large spot into many small spots, respectively. Numerous small flares were detected in the spot group during the decaying phase. This seems to be intimately associated with the shearing motions of many spots with different polarities created by fragmentation of a large sunspot. The magnetic flux and the average shear angle are found to be substantially reduced during the decaying phase, especially in the course of the flarings. This implies that the decaying phase of the sunspot is, to some degree, involved with magnetic field cancellation. The growing spot group has not shown any large activities, but numerous small spots have grown into a typical bipolar sunspot.

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