DOI QR코드

DOI QR Code

A Study on Dye Variation Extracted from Dyed Textile with Gardenia degraded at HIgh temperature after X-ray Irradiation

X-선 조사 후 고온 열화된 치자 염직물에서 추출한 색소 변이 연구

  • Da Young Youn (Department of Heritage Conservation and Restoration, Graduate School of Cultural Heritage, Korea National University of Cultural Heritage) ;
  • Hae Jin Park (Institute of Preventive Conservation for Cultural Heritage, Korea National University of Cultural Heritage) ;
  • Se Eun Park (Department of Heritage Conservation and Restoration, Graduate School of Cultural Heritage, Korea National University of Cultural Heritage) ;
  • Seon Hong Heo (Department of Heritage Conservation and Restoration, Graduate School of Cultural Heritage, Korea National University of Cultural Heritage) ;
  • Su Bin Lim (Department of Conservation Science, University of Science and Technology, Korea National University of Cultural Heritage, Korea National University of Cultural Heritage) ;
  • Yong Jae Chung (Department of Heritage Conservation and Restoration, Graduate School of Cultural Heritage, Korea National University of Cultural Heritage)
  • 윤다영 (한국전통문화대학교 문화유산전문대학원 문화재수리기술학과) ;
  • 박혜진 (한국전통문화대학교 문화유산예방보존연구소) ;
  • 박세은 (한국전통문화대학교 문화유산전문대학원 문화재수리기술학과) ;
  • 허선홍 (한국전통문화대학교 문화유산전문대학원 문화재수리기술학과) ;
  • 임수빈 (한국전통문화대학교 기술과학대학 문화재보존과학과) ;
  • 정용재 (한국전통문화대학교 문화유산전문대학원 문화재수리기술학과)
  • Received : 2024.03.15
  • Accepted : 2024.03.20
  • Published : 2024.03.31

Abstract

This study explores the effects of X-ray irradiation for biological control and high-temperature degradation on dye stability in dyed textiles with Gardenia. To evaluate this study, optimal extraction solvents for these textiles were identified by comparing them with a crocin standard solution. Extraction using pyridine closely matched crocin. The study then assessed the stability of X-ray irradiation and high-temperature degradation on these textiles. Transparent yellow dyes were observed in all samples. Color differences were found to increase at higher irradiation doses and longer degradation periods. While UV spectroscopy spectra showed broadening and lowering trends with higher irradiation doses and longer degradation periods, suggesting a reduction in colorant transition, mass spectrometry revealed minimal chemical changes. In conclusion, both X-ray irradiation and high-temperature degradation induced spectral changes without complete dye decomposition. Major colorants were consistently detected.

Keywords

Acknowledgement

이 논문은 문화재청의 문화유산 스마트 보존·활용 기술 개발의 지원을 받아 수행된 연구임(동산문화재 재해·재난 대응 응급 보존처리를 위한 방사선 활용 훈증 대체기술 개발, 사업번호: 2023A01D07-001, 기여율: 100%)

References

  1. Moon EB. 2012. Korea traditional color. AG book. 230. 
  2. The National Folk Museum of Korea. 2005. Identification of natural fiber & fur. 11-13. 
  3. Ahmed HE, Darwish SS. 2012. Effect of museum conditions on historical dyed silk fabric with madder dye. Journal of Polymers and the Environment 20:596-606. https://doi.org/10.1007/s10924-012-0421-x. 
  4. Park HJ, Choi JS, Hong CY, Lee NR, Youn DY, OH SM and Chung YJ. 2022. Changes of physico-chemical properties of the raw and degummed silk under the wet conditions by gamma-ray irradiation, Journal of Radiation Industry 16(3):261-269. https://doi.org/10.23042/radin.2022.16.3.261. 
  5. IAEA. 2017. Users of ionizing research for tangilble cultural heritage conservation. 
  6. IAEA. 2009. Nuclear techniques for preservation of cultural heritage artefacts. 
  7. Kim JK, Song BS, Kim JH, Park JH, Byun EB and Lee JW. 2013. Sterilization characteristics of ionizing irradiation and its industrial application. Journal of Korea Musculoskelet Transplant Society 13(2):49-57. 
  8. Oh SM, Park HJ, Choi JS, Lee NR, and Chung YJ. 2022. Variation in colourants of the dyes by gamma-ray irradiation, Journal of Conservation Science 38(6):595-607. https://doi.org/10.12654/JCS.2022.38.6.03. 
  9. Cortella L, Albino C, Tran Q and Froment K. 2020. 50 years of French experience in using gamma rays as a tool for cultural heritage remedial conservation. Radiation Physics and Chemistry 171:108726. https://doi.org/10.1016/j.radphyschem.2020.108726. 
  10. Yao W, Liu Z, Yi H, and Wang J. 2011. Structure and mechanical property of silk fiber under gamma radiation. Advance Material Research 175-176:85-89. https://doi.org/10.4028/www.scientific.net/AMR.175-176.85. 
  11. Vujcic I, Masic S, Medic M, Milicevic B and Dramicanin M. The influence of gamma irradiation on the color change of wool, linen, silk, and cotton fabrics used in cultural heritage artifacts. Radiation Physics and Chemistry 156:307-313. https://doi.org/10.1016/j.radphyschem.2018.12.001. 
  12. Vailanou L, Karapanagiotis I and Chryssoulakis Y. 2009. Comparison of extracdtion methods for the analysis of natural dyes in historical textiles by high-performace liquid chromatography. Analytical and Bioanalytical Chemistry 395:2175-2189. https://doi.org/10.1007/s00216-009-3137-6. 
  13. Laursen R. Mouri. C. 2021. Pseudoindirubin: a marker Woad-dyed textiles?. Dyes in History and Archaeology 33/34. 
  14. Han J, Wanrooij J, Bommel M and Quye A. 2017. Characterisation of chemical components for identifying historical chinese textile dyes by ultra high performance liquid chromatography-photodiode array-electro spray ionisation mass spectrometer. Journal of Chromatography A. 1479:87-96. https://doi.org/10.1016/j.chroma.2016.11.044. 
  15. Wouters J, Ceily M, Grzywacz and Claro A. 2010. Markers for identification of faded Safflower (Carthamus thictorius L.) colorants by HPLC-PDA-MS. Studies in Conservation 55:186-203. https://doi.org/10.1179/sic.2010.55.3.18610.1179/sic.2010.55.3.186. 
  16. Oh SM. 2022. Analysis of dyes in textiles dyed with Sappan Wood and Indigo using Surface-enhace Raman Spectroscopy (SERS) [master's thesis]. Korea National University of Cultrual Heritage. 
  17. Ahn CS. 2011. Analysis of Amur cork tree extract and dyed silk upon thermal degradation treatment. Journal of the Korean Society of clothing and Textiles 35(10):1228-1241. https://doi.org/10.5850/JKSCT.2011.35.10.1228. 
  18. Kim JS. 2023. A study on the impacts and challenges of climate change anad conservation of paper and textile heritage. Journal of the Society of Cultural Heritage Disaster Prevention 8(2):113-126.