Advances in nano research

  • 제10권3호
  • /
  • Pages.295-312
  • /
  • 2021
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  • 2287-237X(pISSN)
  • /
  • 2287-2388(eISSN)
테크노프레스 (Techno-Press)
권호 표지
DOI QR코드

DOI QR Code

Ionic liquid coated magnetic core/shell CoFe2O4@SiO2 nanoparticles for the separation/analysis of trace gold in water sample

  • Zeng, Yanxia (Department of Chemical Engineering, Yangzhou University) ;
  • Zhu, Xiashi (Department of Chemical Engineering, Yangzhou University) ;
  • Xie, Jiliang (Institute of Marine Resource Development, Jiangsu Ocean University) ;
  • Chen, Li (Institute of Marine Resource Development, Jiangsu Ocean University)
  • 투고 : 2020.12.08
  • 심사 : 2021.02.03
  • 발행 : 2021.03.25
⟨ 이전 논문 다음 논문 ⟩

초록

A new ionic liquid functionalized magnetic silica nanoparticle was synthesized and characterized and tested as an adsorbent. The adsorbent was used for magnetic solid phase extraction on ICP-MS method. Simultaneous determination of precious metal Au has been addressed. The method is simple and fast and has been applied to standard water and surface water analysis. A new method for separation/analysis of trace precious metal Au by Magnetron Solid Phase Extraction (MSPE) combined with ICP-MS. The element to be tested is rapidly adsorbed on CoFe2O4@SiO2@[BMIM]PF6 composite nano-adsorbent and eluted with thiourea. The method has a preconcentration factor of 9.5-fold. This method has been successfully applied to the determination of gold in actual water samples. Hydrophobic Ionic Liquids (ILs) 1-butyl-3-methylimidazole hexafluorophosphate ([BMIM]PF6) coated CoFe2O4@SiO2 nanoparticles with core-shell structure to prepare magnetic solid phase extraction agent (CoFe2O4@SiO2@ILs) and establish a new method of MSPE coupled with inductively coupled plasma mass spectrometry for separation/analysis of trace gold. The results showed that trace gold was adsorbed rapidly by CoFe2O4@SiO2@[BMIM]PF6 and eluanted by thiourea. Under the optimal conditions, preconcentration factor of the proposed method was 9.5-fold. The linear range, detection limit, correlation coefficient (R) and relative standard deviation (RSD) were found to be 0.01~1000.00 ng·mL-1, 0.001 ng·mL-1, 0.9990 and 3.4% (n = 11, c = 4.5 ng·mL-1). The CoFe2O4@SiO2 nanoparticles could be used repeatedly for 8 times. This proposed method has been successfully applied to the determination of trace gold in water samples.

키워드

과제정보

This study was supported by the Postgraduate Research and Practice Innovation Program of Jiangsu Province (CXZZ13_0892, China); National Youth Science Fund Project (31300652, 41706141, China); the funding of Open subject of Jiangsu Institute of Marine Resources Development; the funding of Jiangsu Ocean University Youth Fund (kx15039, China); the funding of Practical Innovation Project for college students of Huaihai Institute of Technology (PICX132, China).

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