대한치과보철학회지 (The Journal of Korean Academy of Prosthodontics)

  • 제54권4호
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  • Pages.354-363
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  • 2016
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  • 0301-2875(pISSN)
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  • 2005-3789(eISSN)
대한치과보철학회 (The Korean Academy of Prosthodonitics)
권호 표지
DOI QR코드

DOI QR Code

나노구조 알루미나 코팅 처리가 지르코니아 도재와 레진 시멘트 사이 전단 결합강도에 미치는 영향

Influence of nano-structured alumina coating treatment on shear bond strength between zirconia ceramic and resin cement

  • 김동운 (전북대학교 치의학전문대학원 치과보철학교실 및 구강생체과학연구소) ;
  • 이정진 (전북대학교 치의학전문대학원 치과보철학교실 및 구강생체과학연구소) ;
  • 김경아 (을지대학교 의과대학 치과학교실) ;
  • 서재민 (전북대학교 치의학전문대학원 치과보철학교실 및 구강생체과학연구소)
  • Kim, Dong-Woon (Department of Prosthodontics, School of Dentistry and Institute of Oral Bio-Science, Chonbuk National University) ;
  • Lee, Jung-Jin (Department of Prosthodontics, School of Dentistry and Institute of Oral Bio-Science, Chonbuk National University) ;
  • Kim, Kyoung-A (Department of Dentistry, School of Medicine, Eulji University) ;
  • Seo, Jae-Min (Department of Prosthodontics, School of Dentistry and Institute of Oral Bio-Science, Chonbuk National University)
  • 투고 : 2016.03.05
  • 심사 : 2016.07.05
  • 발행 : 2016.10.31
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초록

목적: 본 연구는 지르코니아 도재 표면의 나노구조 알루미나 코팅이 지르코니아와 레진 시멘트와의 전단결합강도에 미치는 영향을 알아보고자 하였다. 재료 및 방법: 지르코니아 원판 80개를 표면처리방법(산화알루미늄 분사처리(A), 산화알루미늄 분사 후 Rocatec 처리(R), 연마 후 나노구조 알루미나 코팅(PC), 산화알루미늄 분사 후 나노구조 알루미나 코팅(AC))에 따라 4개의 군으로 나누었다. 알루미나 코팅은 질산 알루미늄을 가수분해시킨 용액에 침적 후 $900^{\circ}C$에서 열처리 하여 시행하였다. 지르코니아 표면 코팅은 주사전자 현미경을 이용하여 관찰하였다. 레진 블럭을 레진 시멘트를 이용하여 각 실험군의 지르코니아 표면에 합착하고 열순환처리 전, 후의 전단결합강도를 측정하였다. 결과: 알루미나 코팅을 한 지르코니아 표면은 균일하고 치밀한 나노구조 알루미나가 관찰되었다. PC, AC 군은 열순환처리 전과 후 모두 A와 R 군에 비해 현저하게 높은 전단결합 강도를 보였다. A, R 군은 열순환처리 후에 급격한 결합강도의 감소를 보였으나, PC와 AC군은 열순환처리에 의해 유의할만한 결합강도의 감소를 보이지 않았다. 결론: 지르코니아 표면에 나노구조 알루미나 코팅처리하는 것은 레진시멘트와의 결합강도를 증가시키는 방법이다.

Purpose: The aim of this study was to investigate whether the application of nano-structured alumina coating to the surface of Y-TZP could enhance the bond strength with resin cement. Materials and methods: A total of 80 zirconia plates were prepared and divided into four groups. : 1) airborne particle abrasion treatment (A) : 2) Rocatec treatment after airborne particle abrasion (R) : 3) nano-structured alumina coating treatment after polishing (PC) and 4) nano-structured alumina coating after airborne particle abrasion (AC). Alumina coating was formed by the hydrolysis of aluminium nitride (AlN) powder and heat treatment at $900^{\circ}C$. Coating patterns were observed with FE-SEM. Resin block was bonded to treated zirconia ceramics using resin cement. The shear bond strengths were measured before and after thermocycling. Results: The FE-SEM images show a dense and uniform nano-structured alumina coating structure, which enhances shear bond strength by increasing micro mechanical interlocking to resin cement. PC and AC groups showed higher shear bond strengths than A and R groups before and after thermocycling. A and R groups displayed significant drops in shear bond strength after thermocycling. However, PC and AC groups did not show any meaningful decreases in shear bond strength after thermocycling. Conclusion: Treatment of Y-TZP ceramics with nano-structured alumina coating could significantly increase their shear bond strength.

키워드

참고문헌

  1. Anusavice KJ. Recent developments in restorative dental ceramics. J Am Dent Assoc 1993;124:72-4, 76-8, 80-4.
  2. Chevalier J. What future for zirconia as a biomaterial? Biomaterials 2006;27:535-43. https://doi.org/10.1016/j.biomaterials.2005.07.034
  3. Piconi C, Maccauro G. Zirconia as a ceramic biomaterial. Biomaterials 1999;20:1-25. https://doi.org/10.1016/S0142-9612(98)00010-6
  4. Jevnikar P, Krnel K, Kocjan A, Funduk N, Kosmac T. The effect of nano-structured alumina coating on resin-bond strength to zirconia ceramics. Dent Mater 2010;26:688-96. https://doi.org/10.1016/j.dental.2010.03.013
  5. Denry I, Kelly JR. State of the art of zirconia for dental applications. Dent Mater 2008;24:299-307. https://doi.org/10.1016/j.dental.2007.05.007
  6. Della Bona A, Anusavice KJ, Shen C. Microtensile strength of composite bonded to hot-pressed ceramics. J Adhes Dent 2000;2:305-13.
  7. Della Bona A, Anusavice KJ. Microstructure, composition, and etching topography of dental ceramics. Int J Prosthodont 2002;15:159-67.
  8. Brentel AS, Ozcan M, Valandro LF, Alarca LG, Amaral R, Bottino MA. Microtensile bond strength of a resin cement to feldpathic ceramic after different etching and silanization regimens in dry and aged conditions. Dent Mater 2007;23:1323-31. https://doi.org/10.1016/j.dental.2006.11.011
  9. Ozcan M, Vallittu PK. Effect of surface conditioning methods on the bond strength of luting cement to ceramics. Dent Mater 2003;19:725-31. https://doi.org/10.1016/S0109-5641(03)00019-8
  10. Derand P, Derand T. Bond strength of luting cements to zirconium oxide ceramics. Int J Prosthodont 2000;13:131-5.
  11. Aboushelib MN, Matinlinna JP, Salameh Z, Ounsi H. Innovations in bonding to zirconia-based materials: Part I. Dent Mater 2008;24:1268-72. https://doi.org/10.1016/j.dental.2008.02.010
  12. Aboushelib MN, Mirmohamadi H, Matinlinna JP, Kukk E, Ounsi HF, Salameh Z. Innovations in bonding to zirconiabased materials. Part II: Focusing on chemical interactions. Dent Mater 2009;25:989-93. https://doi.org/10.1016/j.dental.2009.02.011
  13. Blatz MB, Sadan A, Kern M. Resin-ceramic bonding: a review of the literature. J Prosthet Dent 2003;89:268-74. https://doi.org/10.1067/mpr.2003.50
  14. Ozcan M, Kerkdijk S, Valandro LF. Comparison of resin cement adhesion to Y-TZP ceramic following manufacturers' instructions of the cements only. Clin Oral Investig 2008;12:279-82. https://doi.org/10.1007/s00784-007-0151-y
  15. Amaral R, Ozcan M, Bottino MA, Valandro LF. Microtensile bond strength of a resin cement to glass infiltrated zirconia-reinforced ceramic: the effect of surface conditioning. Dent Mater 2006;22:283-90. https://doi.org/10.1016/j.dental.2005.04.021
  16. Heikkinen TT, Lassila LV, Matinlinna JP, Vallittu PK. Effect of operating air pressure on tribochemical silica-coating. Acta Odontol Scand 2007;65:241-8. https://doi.org/10.1080/00016350701459753
  17. Ozcan M. Evaluation of alternative intra-oral repair techniques for fractured ceramic-fused-to-metal restorations. J Oral Rehabil 2003;30:194-203. https://doi.org/10.1046/j.1365-2842.2003.01037.x
  18. Valandro LF, Ozcan M, Bottino MC, Bottino MA, Scotti R, Bona AD. Bond strength of a resin cement to high-alumina and zirconiareinforced ceramics: the effect of surface conditioning. J Adhes Dent 2006;8:175-81.
  19. Xible AA, de Jesus Tavarez RR, de Araujo Cdos R, Bonachela WC. Effect of silica coating and silanization on flexural and composite-resin bond strengths of zirconia posts: An in vitro study. J Prosthet Dent 2006;95:224-9. https://doi.org/10.1016/j.prosdent.2005.12.010
  20. Bottino MA, Valandro LF, Scotti R, Buso L. Effect of surface treatments on the resin bond to zirconium-based ceramic. Int J Prosthodont 2005;18:60-5.
  21. Ural C, Kulunk T, Kulunk S, Kurt M, Baba S. Determination of resin bond strength to zirconia ceramic surface using different primers. Acta Odontol Scand 2011;69:48-53. https://doi.org/10.3109/00016357.2010.517558
  22. Mirmohammadi H, Aboushelib MN, Salameh Z, Feilzer AJ, Kleverlaan CJ. Innovations in bonding to zirconia based ceramics: Part III. Phosphate monomer resin cements. Dent Mater 2010;26:786-92. https://doi.org/10.1016/j.dental.2010.04.003
  23. Wegner SM, Gerdes W, Kern M. Effect of different artificial aging conditions on ceramic-composite bond strength. Int J Prosthodont 2002;15:267-72.
  24. Akgungor G, Sen D, Aydin M. Influence of different surface treatments on the short-term bond strength and durability between a zirconia post and a composite resin core material. J Prosthet Dent 2008;99:388-99. https://doi.org/10.1016/S0022-3913(08)60088-8
  25. Novak S, Kosmac T. Preparation of alumina ceramics from aqueous suspensions employing the hydrolysis of aluminum nitride. J Mater Res 2002;17:445-50. https://doi.org/10.1557/JMR.2002.0062
  26. Krnel K, Kocjan A, Kosmac T. A simple method for the preparation of nanostructured aluminate coatings. J Am Ceram Soc 2009;92:2451-4. https://doi.org/10.1111/j.1551-2916.2009.03236.x
  27. Zhang S, Kocjan A, Lehmann F, Kosmac T, Kern M. Influence of contamination on resin bond strength to nano-structured alumina-coated zirconia ceramic. Eur J Oral Sci 2010;118:396-403. https://doi.org/10.1111/j.1600-0722.2010.00752.x
  28. Lindgren J, Smeds J, Sjogren G. Effect of surface treatments and aging in water on bond strength to zirconia. Oper Dent 2008;33:675-81. https://doi.org/10.2341/08-12
  29. Wolfart M, Lehmann F, Wolfart S, Kern M. Durability of the resin bond strength to zirconia ceramic after using different surface conditioning methods. Dent Mater 2007;23:45-50. https://doi.org/10.1016/j.dental.2005.11.040
  30. Kern M, Wegner SM. Bonding to zirconia ceramic: adhesion methods and their durability. Dent Mater 1998;14:64-71. https://doi.org/10.1016/S0109-5641(98)00011-6
  31. Phark JH1, Duarte S Jr, Blatz M, Sadan A. An in vitro evaluation of the long-term resin bond to a new densely sintered high-purity zirconium-oxide ceramic surface. J Prosthet Dent 2009;101:29-38. https://doi.org/10.1016/S0022-3913(08)60286-3
  32. Blatz MB, Chiche G, Holst S, Sadan A. Influence of surface treatment and simulated aging on bond strengths of luting agents to zirconia. Quintessence Int 2007;38:745-53.
  33. Amaral R1, Ozcan M, Valandro LF, Balducci I, Bottino MA. Effect of conditioning methods on the microtensile bond strength of phosphate monomer-based cement on zirconia ceramic in dry and aged conditions. J Biomed Mater Res B Appl Biomater 2008;85:1-9.
  34. Ozcan M, Nijhuis H, Valandro LF. Effect of various surface conditioning methods on the adhesion of dual-cure resin cement with MDP functional monomer to zirconia after thermal aging. Dent Mater J 2008;27:99-104. https://doi.org/10.4012/dmj.27.99
  35. Ernst CP, Cohnen U, Stender E, Willershausen B. In vitro retentive strength of zirconium oxide ceramic crowns using different luting agents. J Prosthet Dent 2005;93:551-8. https://doi.org/10.1016/j.prosdent.2005.04.011
  36. Matinlinna JP, Heikkinen T, Ozcan M, Lassila LV, Vallittu PK. Evaluation of resin adhesion to zirconia ceramic using some organosilanes. Dent Mater 2006;22:824-31. https://doi.org/10.1016/j.dental.2005.11.035
  37. Luthy H, Loeffel O, Hammerle CH. Effect of thermocycling on bond strength of luting cements to zirconia ceramic. Dent Mater 2006;22:195-200. https://doi.org/10.1016/j.dental.2005.04.016
  38. Breschi L, Mazzoni A, Ruggeri A, Cadenaro M, Di Lenarda R, De Stefano Dorigo E. Dental adhesion review: aging and stability of the bonded interface. Dent Mater 2008;24:90-101. https://doi.org/10.1016/j.dental.2007.02.009
  39. Yang B, Barloi A, Kern M. Influence of air-abrasion on zirconia ceramic bonding using an adhesive composite resin. Dent Mater 2010;26:44-50. https://doi.org/10.1016/j.dental.2009.08.008
  40. Kosmac T, Oblak C, Jevnikar P, Funduk N, Marion L. The effect of surface grinding and sandblasting on flexural strength and reliability of Y-TZP zirconia ceramic. Dent Mater 1999;15:426-33. https://doi.org/10.1016/S0109-5641(99)00070-6
  41. Kosmac T, Oblak C, Jevnikar P, Funduk N, Marion L. Strength and reliability of surface treated Y-TZP dental ceramics. J Biomed Mater Res 2000;53:304-13. https://doi.org/10.1002/1097-4636(2000)53:4<304::AID-JBM4>3.0.CO;2-S
  42. Zhang Y1, Lawn BR, Malament KA, Van Thompson P, Rekow ED. Damage accumulation and fatigue life of particle-abraded ceramics. Int J Prosthodont 2006;19:442-8.
  43. Zhang Y, Lawn BR, Rekow ED, Thompson VP. Effect of sandblasting on the long-term performance of dental ceramics. J Biomed Mater Res B Appl Biomater 2004;71:381-6.

피인용 문헌

  1. Influence of nano alumina coating on the flexural bond strength between zirconia and resin cement vol.10, pp.1, 2018, https://doi.org/10.4047/jap.2018.10.1.43