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Spark Plasma Sintering of Fe-TiC Composite Powders

Fe-TiC 복합재료분말의 방전플라즈마소결

  • Lee, Yong-Heui (School of Materials Science and Engineering, University of Ulsan) ;
  • Hyunh, Xuan-Khoa (School of Materials Science and Engineering, University of Ulsan) ;
  • Kim, Ji Soon (School of Materials Science and Engineering, University of Ulsan)
  • 이용희 (울산대학교 첨단소재공학부) ;
  • ;
  • 김지순 (울산대학교 첨단소재공학부)
  • Received : 2014.10.10
  • Accepted : 2014.10.21
  • Published : 2014.10.28

Abstract

Fe-TiC composite powder was fabricated by high-energy milling of powder mixture of (Fe, TiC) and (FeO, $TiH_2$, C) as starting materials, respectively. The latter one was heat-treated for reaction synthesis of TiC phase after milling. Both powders were spark-plasma sintered at various temperatures of $680-1070^{\circ}C$ for 10 min. with sintering pressure of 70 MPa and the heating rate of $50^{\circ}C/min$. under vacuum of 0.133 Pa. Density and hardness of the sintered compact was investigated. Fe-TiC composite fabricated from (FeO, $TiH_2$, C) as starting materials showed better sintered properties. It seems to be resulted from ultra-fine TiC particle size and its uniform distribution in Fe-matrix compared to the simply mixed (Fe, TiC) powder.

Keywords

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