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A Study on Fabrication and Characterization of Inorganic Insulation Material by Hydrothermal Synthesis Method (2)

수열합성법을 이용한 무기계 단열소재 제조방법 및 특성에 관한 연구 (2)

  • Seo, Sung-Kwan (Energy & Environmental Division Korea Institute of Ceramic Eng. & Tech.) ;
  • Chu, Yong-Sik (Energy & Environmental Division Korea Institute of Ceramic Eng. & Tech.) ;
  • Lee, Jong-Kyu (Energy & Environmental Division Korea Institute of Ceramic Eng. & Tech.) ;
  • Song, Hun (Energy & Environmental Division Korea Institute of Ceramic Eng. & Tech.) ;
  • Park, Jae-Wan (Energy & Environmental Division Korea Institute of Ceramic Eng. & Tech.)
  • 서성관 (한국세라믹기술원 에너지환경소재본부) ;
  • 추용식 (한국세라믹기술원 에너지환경소재본부) ;
  • 이종규 (한국세라믹기술원 에너지환경소재본부) ;
  • 송훈 (한국세라믹기술원 에너지환경소재본부) ;
  • 박재완 (한국세라믹기술원 에너지환경소재본부)
  • Received : 2013.12.02
  • Accepted : 2013.12.17
  • Published : 2013.12.30

Abstract

The inorganic insulating material was fabricated with quartzite, ordinary portland cement(OPC), lime, anhydrous gypsum and foaming agent by hydrothermal reaction. The inorganic insulating material was fabricated by using autoclave chamber under high-temperature and high-pressure. The inorganic insulating material is a porous lightweight concrete. Because of its porous structure, properties of inorganic insulating material were light-weight and high-heat insulation property. Properties of fabricated inorganic insulating material were $0.26g/cm^3$ in specific gravity, 0.4MPa in compressive strength and 0.064W/mK in thermal conductivity. In this study, the inorganic insulating material was fabricated and analyzed at different size of quartzite/OPC, various foaming reagent and functional additives to improve the properties. Consequently, polydimethylsiloxane can improve density and thermal conductivity. Especially, polydimethylsiloxane showed excellent improvement in compressive strength.

규석, 시멘트, 생석회 및 소량의 무수석고에 알루미늄 분말과 물을 첨가 혼합하여 오토클레이브 중에서 고온 고압 증기양생으로 미네랄 하이드레이트 소재를 제조하였다. 수열 합성된 미네랄 하이드레이트 소재는 균일한 세포조직을 갖는 다공질 경량 기포 콘크리트이다. 미네랄 하이드레이트 소재의 대표적인 특성으로는 다수의 기공으로 인해 뛰어난 경량성 및 단열성능을 들 수 있다. 제조된 미네랄 하이드레이트 소재의 특성은 각각 밀도 $0.26g/cm^3$, 압축강도 0.4MPa, 열전도율 0.064W/mK로 나타났다. 본 연구에서는 상기의 소재 특성을 증진시키기 위하여 "기포제의 종류 및 함량, 규석 및 시멘트의 입도 조건, 기능성 첨가제 종류 및 함량"에 따른 특성 평가 및 분석을 실시하였다. 그 결과 소재의 열적 특성을 개선할 수 있었으며, 특히 기능성 첨가제인 폴리디메틸실록산 혼화제를 첨가할 경우 밀도 및 열전도율을 개선하는 동시에 탁월한 강도 증진 효과를 나타내었다.

Keywords

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