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편백나무 잎 추출물 함유 크림의 안정성 평가

Stability Test for the Cream Containing Chamaecyparis Obtusa Leaf Extract

  • 임명선 (서울과학기술대학교 정밀화학과, 나노바이오화장품연구실 화장품종합기술연구소) ;
  • 이동숙 (서울과학기술대학교 정밀화학과, 나노바이오화장품연구실 화장품종합기술연구소) ;
  • 권순식 (서울과학기술대학교 정밀화학과, 나노바이오화장품연구실 화장품종합기술연구소) ;
  • 박수남 (서울과학기술대학교 정밀화학과, 나노바이오화장품연구실 화장품종합기술연구소)
  • Lim, Myoung-Sun (Department of Fine Chemistry, Nanobiocosmetic laboratory, Cosmetic R&D Center, Seoul National University of Science and Technology) ;
  • Lee, Dong-Sook (Department of Fine Chemistry, Nanobiocosmetic laboratory, Cosmetic R&D Center, Seoul National University of Science and Technology) ;
  • Kwon, Soon-Sik (Department of Fine Chemistry, Nanobiocosmetic laboratory, Cosmetic R&D Center, Seoul National University of Science and Technology) ;
  • Park, Soo-Nam (Department of Fine Chemistry, Nanobiocosmetic laboratory, Cosmetic R&D Center, Seoul National University of Science and Technology)
  • 투고 : 2012.04.11
  • 심사 : 2012.06.18
  • 발행 : 2012.06.30

초록

본 연구에서는 편백나무 잎 추출물의 에틸아세테이트 분획을 함유한 크림의 안정성을 평가하였다. 다양한 저장 온도($4^{\circ}C$, $25^{\circ}C$, $37^{\circ}C$$45^{\circ}C$) 및 태양광선에의 노출 하에서 12주 동안 추출물 함유 크림의 pH, 점도 및 흡광도 변화를 측정하였다. 위에서 언급된 온도별 저장조건에서 추출물이 함유되어 있지 않은 대조군 크림은 pH 변화가 거의 없었다. 추출물 함유 크림의 경우는 $4^{\circ}C$$25^{\circ}C$에서 pH가 평균 0.11 감소하였고, $37^{\circ}C$, $45^{\circ}C$ 저장과 태양광선 노출 시는 각각 0.55, 0.84 및 0.59 감소하였다. 온도별 저장 조건에서 12주 후 추출물 함유 크림과 대조군 크림의 점도를 측정하였다. 추출물 함유 크림은 초기 점도보다 평균 2,404 cPs 감소를 나타내었고, 대조군은 평균 1,296 cPs 감소하였다. $45^{\circ}C$ 조건에서 대조군은 12주 후 점도가 1,915 cPs로 감소되었지만, 동일 조건에서 추출물 함유 크림의 점도는 3,810 cPs 감소하였다. 12주 동안 $4^{\circ}C{\sim}37^{\circ}C$에서 추출물 함유 크림의 흡광도 변화는 거의 없었다. 반면에 $45^{\circ}C$ 저장과 태양광선 노출시킨 경우는 흡광도는 각각 32.5 % 및 35.2 % 감소하였다. 크림으로부터 추출물을 용출시킨 에탄올 용액을 태양광선에 직접 노출시켰을 때 4주 만에 흡광도가 54.8 %감소한 것에 비해서는 작은 감소를 나타낸다. 이는 추출물크림이 크림 내에서 비교적 안정화되어 있음을 나타낸다. 추출물 함유 크림과 대조군 크림은 12주 동안 동일한 실험 조건에서 변취나 변색이 나타나지 않았으며, 크리밍이나 응집과 같은 현상은 관찰되지 않았다. 이러한 결과들로부터 편백나무 잎 추출물을 함유한 크림이 비교적 안정함을 확인하였다. 하지만, 추출물 함유 크림을 장기간 저장할 때 안정성은 아직 확실치는 않으며, 추출물을 화장품에 응용하기 위해서는 더 많은 연구가 필요하다고 사료된다.

In this study, the stability of cream containing the ethyl acetate fraction of C. obtusa leaf extract was evaluated. The pH, viscosity, and absorbance were measured under the 4 different temperatures (4, 25, 37 and $45^{\circ}C$) and under the sun light during the 12 weeks. The control cream without containing the extract did not show pH change under the different temperatures mentioned above. However, the pH of the cream with the extract was decreased 0.11 at $4^{\circ}C$ and $25^{\circ}C$. Under the $37^{\circ}C$, $45^{\circ}C$ and sun light condition, the pH was decreased 0.55, 0.84 and 0.59, respectively. After treating the cream for 12 weeks under the different temperatures, the viscosity was measured for the cream containing the extract and control cream. The values were decreased by 2,404 cPs in average compared to the initial value for the former and control cream were decreased by 1,296 cPs in average for the latter. On the other hand, the viscosity of control cream treated under the $45^{\circ}C$ for 12 weeks was decreased (1,915 cPs) relative to the cream containing the extract, which showed 3,810 cPs decrease in viscosity. The cream containing the extract did not show absorbance change at $4^{\circ}C{\sim}37^{\circ}C$ for 12 weeks. Instead, the absorbance of the cream treated under $45^{\circ}C$ and sun light condition was decreased 32.5 % and 35.2 %, respectively. This decrease in absorbance is relatively small compared to the 54.8 % decrease of the extract sampled from the cream using ethanol solution. This indicates that the extract is stabilized in the cream. In addition, any change in color or smell was not observed through 12 weeks of the experimental time period. Also physical changes as creaming and cohesion were not shown. The results show that the cream containing C. obtusa leaf extract was relatively stable. However, it is concluded that it is still not clear in the stability of the cream containing the extract when it is stored for a long time. Accordingly, it is suggested that further study is needed for the application of the extract to cosmetics.

키워드

참고문헌

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