Bulletin of the Korean Chemical Society

  • 제33권5호
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  • Pages.1699-1702
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  • 2012
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  • 0253-2964(pISSN)
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  • 1229-5949(eISSN)
대한화학회 (Korean Chemical Society)
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Control of Particle Characteristics in the Preparation of TiO2 Nano Particles Assisted by Microwave

  • 투고 : 2011.12.26
  • 심사 : 2012.02.21
  • 발행 : 2012.05.20
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초록

$TiO_2$ nanostructures with various morphologies like cubes, spheres, hexahedral pillars and spherical tubes were synthesized by microwave-assisted hydrothermal process. Each structure was obtained by changing the relative concentrations of titanium tetraisoproxide (TTIP), tetrabutylammonium hydroxide (TBAH) and ethanol. Scanning electron microscopy (SEM), transmission electoron microscopy (TEM), X-ray diffraction and Brunauer-Emmett-Teller (BET) surface area analysis were used to characterize the synthesized $TiO_2$ nanostructures. From these results, it has been proved that $TiO_2$ structure could be controlled to have specific morphology, size, surface area, pore volume and pore size distribution.

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피인용 문헌

  1. Effect of the Amount of Water in the Synthesis of B-TiO2: Orange II Photodegradation vol.2014, pp.None, 2014, https://doi.org/10.1155/2014/721216
  2. TiO2 synthesized by microwave assisted solvothermal method: Experimental and theoretical evaluation vol.210, pp.1, 2012, https://doi.org/10.1016/j.jssc.2013.11.023