한국환경보건학회지 (Journal of Environmental Health Sciences)

  • 제37권1호
  • /
  • Pages.57-63
  • /
  • 2011
  • /
  • 1738-4087(pISSN)
  • /
  • 2233-8616(eISSN)
한국환경보건학회 (Korean Society of Environmental Health)
권호 표지
DOI QR코드

DOI QR Code

청석면 분석 정도관리용 표준시료 개발 및 평가

Development and Validation of Crocidolite Quality Control Samples for Proficiency Analytical Testing

  • 이지현 (용인대학교 환경보건학과) ;
  • 김은영 (용인대학교 환경보건학과) ;
  • 노수진 (용인대학교 환경보건학과) ;
  • 박용진 (용인대학교 환경보건학과) ;
  • 정지연 (용인대학교 환경보건학과)
  • Lee, Ji-Hyun (Department of Environmental Health, Yongin University) ;
  • Kim, Eun-Young (Department of Environmental Health, Yongin University) ;
  • Noh, Su-Jin (Department of Environmental Health, Yongin University) ;
  • Park, Yong-Jin (Department of Environmental Health, Yongin University) ;
  • Jeong, Jee-Yeon (Department of Environmental Health, Yongin University)
  • 투고 : 2011.01.12
  • 심사 : 2011.02.14
  • 발행 : 2011.02.28
PDF 다운로드
⟨ 이전 논문 다음 논문 ⟩

초록

Crocidolite quality control (QC) sampling created by the wet generation method has been validated by validation tests such as the accuracy, precision, and storage tests. For this study we designed and developed a manufacturing apparatus and standard operating procedure for making these QC samples. The most important step in the procedure of making QC samples was the stage eliminating static electricity in asbestos fibers. This static electricity hampers the fibers clog functioning. In accuracy and precision tests by phase contrast microscopy analysis, the difference between the reference values and the studied values was at maximum 17.8%. This satisfies the AIHA proficiency analytical test criteria for asbestos. We could confirm the nearly even distribution of crocidolite fibers on the membrane filter. Also, there was no loss of fibers in the storage test after the one month.

키워드

참고문헌

  1. Hammar, S. P. : The pathologic features of asbestos-induced disease in Asbestos. Taylor & Francis, New York, 2006.
  2. Ahn, Y. S. and Kang, S. K. : Asbestos-related occupational cancers compensated under the industrial accident compensation insurance in Korea. Industrial Health, 47(2), 113-122, 2009. https://doi.org/10.2486/indhealth.47.113
  3. Ministry of Labor : Ministry of labor notice 2008-16; Occupational exposure standard for physical and chemical agents. Ministry of Labor, 2008.
  4. Ministry of Labor : Workplace measurement methods for hazardous chemicals. Ministry of Labor, 2009.
  5. Ministry of Environment : Official measurement methods for indoor air quality. Ministry of Environment, 2004.
  6. US National Institute for Occupational Safety and Health : NIOSH method 7400 in NIOSH Manual of analytical methods. 4th ed., US National Institute for Occupational Safety and Health, 1994.
  7. UK Health and Safety Executive : Method 39/4 in method for the determination of hazardous substances. UK Health and Safety Executive, 1995.
  8. Schlect, P. C. and Stanley, A. S. : Performance of asbestos fiber counting laboratories in the NIOSH proficiency analytical testing program. American Industrial Hygiene Association Journal, 56, 480-489, 1986.
  9. Timbrell, V., Skidmore, J. W., Hyett, A. W. and Wagner, J. C. : Exposure chambers for inhalation experiments with standard reference samples of asbestos of the International Union Against Cancer (UICC). Aerosol Science, 1, 215-223, 1970. https://doi.org/10.1016/0021-8502(70)90035-2
  10. Skogstad, A., Eduard, W. and Huser, P. O. : A laboratory method for generation of replicate fiber samples of asbestos fibers in air. Applied Occupational and Environmental Hygiene, 57, 741-745, 1996.
  11. Niemeyer, I. C. and Gerchman, L. L. : Preparation of asbestos filter samples for reference standard using a wet generation technique. American Industrial Hygiene Association Journal, 42, 757-759, 1981. https://doi.org/10.1080/15298668191420657
  12. US National Institute for Occupational Safety and Health : Guidelines for air sampling and analytical method development and evaluation. US National Institute for Occupational Safety and Health, Salt lake City, 1995.
  13. US Environmental Protection Agency : Guidance for method development and method validation for the RCRA program. US Environmental Protection Agency, 1992.
  14. US Environmental Protection Agency : Revised assessment of detection and quantitation approach. EPA-821-B-04-005. US Environmental Protection Agency, 2004.
  15. US Occupational Safety and Health Administration : Evaluation scheme for methods that use filters as collection medium in OSHA analytical manual. 2nd ed., US Occupational Safety and Health Administration, Salt Lake City, 1990.
  16. American Industrial Hygiene Association : Laboratory quality assurance program polices. American Industrial Hygiene Association, Fairfax, VA, 2001.
  17. Schlect, P. C. and Shulman, S. A. : Phase contrast microscopy asbestos fiber counting performance of laboratories in the proficiency analytical testing program. American Industrial Hygiene Association Journal, 56, 480-489, 1995. https://doi.org/10.1080/15428119591016908
  18. Lee, K. W., Yoon, C. S., Han, J. K., Yoon, M. J., Jung, S. J., Lee, J. H., Lee, I. S. and Park, D. W. : Development of asbestos qulity control samples for proficiency analytical testing: evaluation of amosite and chrysotile quality control samples. Journal of Korean Society of Occupational and Environmental Hygiene, 19(3), 288-296, 2009.