DOI QR코드

DOI QR Code

Fabrication of Biaxially Textured Ni Tapes from Ni Powder Compact Rods

분말 성형체로부터 양축정렬 집합조직을 갖는 니켈 테이프의 제조

  • 이동욱 (한국원자력연구소 원자력 재료기술 개발부) ;
  • 지봉기 (한국원자력연구소 원자력 재료기술 개발부) ;
  • 주진호 (성균관대학교 금속재료공학부) ;
  • 김찬중 (한국원자력연구소 원자력 재료기술 개발부)
  • Published : 2003.08.01

Abstract

Biaxially textured Ni tapes were fabricated by a cold working and recrystallization heat treatment processes from powder compact rods. The processing parameters associated with the cube texture formation in Ni tapes were systematically investigated by using X-ray diffraction and pole-figure analysis. The Ni powder used in this study was 5 $\mu$m in size and 99.99% in purity. To find the optimum sintering temperature, tensile tests were performed for Ni rods sintered at various temperatures. The Ni rods sintered at 100$0^{\circ}C$ showed poor elongation and low fracture strength, while the Wi rods sintered above 100$0^{\circ}C$ revealed good mechanical properties. The higher elongation and fracture strength of the Ni rods sintered at higher temperatures than 100$0^{\circ}C$ are attributed to the full densification of the sintered rods. The sintered Ni rods were cold-rolled with 5% reduction to the final thickness of 100 $\mu$m and then annealed for development of rube texture in rolled Ni tapes. The annealed Ni tapes depicted strong cube texture with FWHM(full-width at half-maximum) of in-plane and out-of-plane in the range of 8$^{\circ}$ to 10$^{\circ}$. The NiO deposited on the Ni tapes by MOCVD process showed good epitaxy with FWHM=10$^{\circ}$, which indicates that the Ni tapes can be used as a substrate for YBCO coated conductors.

Keywords

References

  1. Appl. Phys. Lett. v.69 A.Goyal;D.P.Norton;J.D.Budai;M.Paranthaman;E.D.Specht;D.M.Kroeger;D.K.Christen;Q.He;B.Saffian;F.A.List;D.F.Lee;P.M.Martin;C.E.Klabunde;E.Hatfield;V.K.Silkka https://doi.org/10.1063/1.117179
  2. US patent No. 5,741,377 A.Goyal;J.D.Budai;D.M.Kroeger;D.P.Norton;E.D.Specht;D.K.Christen
  3. Appl. Phys. Lett. v.60 Y.Iijima;N.Tanabe;O.Kohno;Y.Ikeno https://doi.org/10.1063/1.106514
  4. J. Appl. Phys. v.74 Y.Iijima;K.Onabe;N.Futaki;N.Sadakata;K.O.Kohno https://doi.org/10.1063/1.354801
  5. Appl. Phys. Lett. v.67 X.D.Wu;S.R.Foltyn;P.N.Arendt;W.R.Blumenthal;I.H.Campbell;J.D.Cotton;J.Y.Coutler;W.L.Helts;M.P.Maley;H.F.Safar;J.L.Smith https://doi.org/10.1063/1.114559
  6. Proceedings of the 16th International Cryogenic Engineering Conference and International Cryogenic Material Confernece K.Hasegawa;N.Yoshida;K.Fujino;H.Mukai;K.Hayashi;K.Sata;T.Ohkuma;S.Honjyo;H.Ishii;T.Hara
  7. Mater. Sci. and Eng. B v.56 D.P.Norton;C.Park;C.Prouteau;D.K.Christen;M.F.Chisholm;J.D.Budai;S.J.Pennycook;A.Goyal;E.Y.Sun;D.F.Lee;D.M.Kroeger;E.Specht;M.Paranthaman;N.D.Browning https://doi.org/10.1016/S0921-5107(98)00230-X
  8. Supercon. Sci. and Technol. v.13 T.A.Gladstone;J.C.Moore;B.M.Henry;S.Speller;C.J.Salter;A.J.Wilkinson;C.R.M.Grovenor https://doi.org/10.1088/0953-2048/13/9/319
  9. Supercon. Sci. and Technol. v.14 S. Pi ol;J.Diaz;M.Segarra;F.Espiell https://doi.org/10.1088/0953-2048/14/1/303
  10. Structure of Metals(3rd ed.) C.S.Barett;T.B.Masalski
  11. Acta Mater. v.49 B. De Boer;J.Eickemeyer;N.Reger;L.Fernandez;G.R.;J.Richter;B.Holzapfel;L.Schultz;W.Prusseit;P.Berberich https://doi.org/10.1016/S1359-6454(01)00041-6
  12. Supercon. Sci. and Technol. v.14 J.Eickemeyer;D.Selbmann;R.Opitz;B. De Boer;B.Holzapfel;L.Schultz;U.Miller https://doi.org/10.1088/0953-2048/14/3/306
  13. Standard Test Methods for Tension Testing of Metallic Materials ASTM
  14. Mater. Sci. and Eng. v.A238 R.D.Doherty;D.A.Hughes;F.J.Humphreys;J.J.Jonas;D. Juul Jensen;M.E.Kassner;W.E.King;T.R.McNelley;H.J.McQueen;A.D.Rollett
  15. Mech. Sci. v.42 Dong Nyung Lee https://doi.org/10.1016/S0020-7403(99)00095-8
  16. Directional Properties of Materials H.J.Bunge
  17. Supercond. Sci. Technol. v.11 E.D.Specht;A.Goyal;D.F.Lee;F.A.List;D.M.Kroeger;M.Paranthaman;R.K.Williams;D.K.Christen https://doi.org/10.1088/0953-2048/11/10/009
  18. Physica C v.351 Tomonori Watanabe;Kaname Matsumoto;Toshihiko Maeda;Toru Tanigawa;Izumi Hirabayashi