• Transactions of Materials Processing
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• v.10 no.2
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• pp.137-143
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• 2001

The change of flow stress due to dynamic recrystallization during hot forming process is investigated. A series of mechanical tests has been conducted at various temperatures, and constitutive relations and recrystallization kinetics were formulated from the test results. The effect of dynamic recrystallization to the flow stress was implemented to a commercial FEM code by conditioned remapping of state variables. The datum strain of stress compensation was optimized to minimize the overestimation of forming loads. Suggested datum was formulated as an exclusive function of critical strain for recrystallizalion and validated by mechanical tests and microstructural observations.

• Transactions of Materials Processing
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• v.15 no.8 s.89
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• pp.591-596
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• 2006

Torsion testing was employed to investigate the deformation and recrystallization behavior of coarse-grained Alloy 718, and the results are compared with the compression testing results. Mechanical testing was conducted on bulk Alloy718 samples within the temperature ranges, $1000^{\circ}C{\sim}1100^{\circ}C$. The strain gradient formed in the torsion specimens resulted in a recrystallization behavior which varied along the radial direction from the center to the surface. The flow curves based on effective stress and effective strain as obtained by Fields and Backofen's isotropic deformation theory and the dynamic recrystallization within the compression tested samples and torsion tested samples are different. The different deformation and recrystallization behavior can be rationalized by the fact that the deformation in the coarse-grained torsion specimens is not uniform and thus the strain gradient within the specimens cannot be analytically predicted by FE simulation. Thus, the extent of recrystallization cannot be properly predicted by the established recrystallization equations based on compression tests.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.59-62
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• 2006

Mg alloys have drawn a huge attention in the field of transportation and consumer electronics industries since it is the lightest alloy which could be industrially applicable. Most Mg alloy components have been fabricated by casting method. However, there have been a lot of research activities on the wrought alloys and their plastic forming process recently. The deformation behavior of an AZ31 Mg alloy at the elevated temperature was examined firstly to find out the optimum plastic forming range in terms of temperature and strain rate. During high temperature deformation, AZ31 alloy is usually undergone the dynamic recrystallization which influence the deformation behavior in turn. In the present study, the effect of deformation on dynamic recrystallization of an AZ31 alloy was investigated to clarify the relation between the deformation and recrystallization. In an AZ31 alloy system, the dynamic recrystallization was found to occur continuously. Recrystallized grain size was dependent on the stress level.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2006.05a
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• pp.70-73
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• 2006

In the present study, the flow-softening behavior occurring during high temperature deformation of AZ31 Mg alloy was investigated. Flow softening of AZ31 Mg alloy was attributed to (1) thermal softening by deformation heating and (2) microstructural softening by dynamic recrystallization. Artificial neural networks method was used to derive the accurate amounts of thermal softening by deformation heating. A series of mechanical tests (High temperature compression and load relaxation tests) was conducted at various temperatures ($250^{\circ}C{\sim}500^{\circ}C$) and strain rates ($10^{-4}/s{\sim}100/s$) to formulate the recrystallization kinetics and grain size relation. The effect of DRX kinetics on microstructure evolution (fraction of recrystallization) was evaluated by the unified SRX/DRX (static recrystallization/dynamic recrystallization) approaches

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2005.05a
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• pp.266-269
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• 2005

The effect of exit temperature on the thickness of recrystallization layer during Al extrusion process was investigated. The recrystallization layer of an extruded Al alloy is an important feature of the product in a wide range of applications, particularly those within the automotive industry. The thicker recrystallized layer in the Al alloys can give rise to a number of problems including reduced fatigue resistance and orange peel during cold forming. But the interaction of extrusion process variables with the thickness of recrystallization layer is poorly understood, and there is limited information available regarding the role of the main hot extrusion variables. Using the 3650 US ton extrusion press, this paper describes the effect of the main process variables such as billet temperature, ram speed, and exit temperature on the thickness of recrystallization layer for the A6XXX Al alloy.

• Transactions of Materials Processing
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• v.10 no.1
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• pp.42-52
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• 2001

The static softening mechanisms of 304 stainless steel were studied by hot torsion test. The interrupted deformation tests were performed In the range of 900~$1100^{\circ}C$ and 5.0$\times$$10^{-2}$- 5.0$\times$$10^0$/sec. The metadynamic recrystallization (MDRX) could be distinguished from the static recrystallization (SRX). Comparison of the softening kinetics between MDRX and SRX showed that the rate of MDRX was more rapid than that of SRX for the same deformation variables. To the exact prediction of MDRX, the MDRX parameter, which could be simultaneously estimated by the interpass time and Zener-Hollomon parameter, was developed. The time lot 50% MDRX, $t_{0.5} was modeled using the deformation parameters : $t_{0.5} = 1.33\times10^{-11}$ $\.\varepsilon^{-0.41}$ D exp(230.3kJ/mol/RT) and the predicted value was very correspondent with the measurement. It was found that the static parameters such as interpass time can control the dynamic states in the several successive deformation process.

• Korean Journal of Metals and Materials
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• v.47 no.6
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• pp.356-362
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• 2009

In order to vary the primary recrystallization textures, AA 1050 sheets were cold rolled in two different manners. Differences in cold rolling schedule gave rise to the formation of different cold rolling textures also leading to the formation of different primary recrystallization textures. Upon annealing for grain growth, changes in microstructure and texture hardly occurred in the sample depicting Cube recrystallization texture, while grain growth was accompanied with the development {001}<100> Cube texture in the sample displaying a recrystallization texture comprising of weak rolling texture components. The selective growth of Cube oriented grains is attributed to the high mobility of their grain boundaries.

• Korean Journal of Materials Research
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• v.26 no.12
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• pp.688-695
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• 2016

Recrystallization behavior has been investigated for commercial purity AA1050 (99.5wt%Al) and high purity 3N Al (99.9wt% Al). Samples were cold rolled with 90% of thickness reduction and were annealed isothermally at 290, 315, and 350o C for various times until complete recrystallization was achieved. Hardness measurement and Electron Backscatter Diffraction(EBSD) analyses, combined with Grain Orientation Spread(GOS), were employed to investigate the recrystallization behavior. EBSD analysis combined with GOS were distinctly revealed to be a more useful method to determine the recrystallization fraction and to characterize the recrystallization kinetics. As the annealing temperature increased, recrystallization in AA1050 accelerated more than that process did in Al 3N. Both AA1050 and Al 3N showed the same temperature dependence of the n value of the Johnson-Mehl-Avrami-Kolmogorov equation(JMAK equation), i.e., n values increased as annealing temperature increased. Activation energy of recrystallization in AA1050 is about 176 kJ/mol, which is comparable with the activation energy of grain boundary migration in cold-rolled AA1050. This value is somewhat higher than the activation energy of recrystallization in Al 3N.

• Food Science and Biotechnology
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• v.15 no.2
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• pp.196-201
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• 2006

Freeze concentration of milk was carried out thorough the controlled recrystallization of ice in a multi-stage freeze concentrator. Artificial temperature control was used to induce ice recrystallization via a heat and cold shock process. In each stage of freeze concentration, the recrystallization time was fixed at 1, 2, 4, and 8 hr to compare the solute concentrate, yield, Brix, ice crystal size, and freezing point at each experimental condition. Higher concentrations of milk solids were seen with increased durations of recrystallization time, and a maximum total solids in the final product of 32.7% was obtained with a ripening time of 8 hr in a second stage process. Milk solid yield decreased according to the solute concentration and recrystallization time. The results of Brix and ice crystal size showed a positive correlation with recrystallizaiton time. These results suggest the possibility of freeze concentration being of practical use in the dairy industry.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 1999.08a
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• pp.320-326
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• 1999

In the present investigation, recrystallization occurring during hot rolling of thick steel plate was predicted. The thermo-mechanical history of a material point was traced by the finite element method and the recrystallization was predicted by the Sellars equations. The investigation was performed for 4 different cases; two different pass schedules in conventional rolling and two different pass schedules in controller rolling. Variations of temperature, strain, strain rate and grain size were compared with each other. It was found out that the difference of grain size through thickness was more distinctive in the cases of controller rolling.